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WO2019153885A1 - Support de génération de fumée de cigarette permettant un chauffage électrique sans combustion et son procédé de préparation - Google Patents

Support de génération de fumée de cigarette permettant un chauffage électrique sans combustion et son procédé de préparation Download PDF

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Publication number
WO2019153885A1
WO2019153885A1 PCT/CN2018/121179 CN2018121179W WO2019153885A1 WO 2019153885 A1 WO2019153885 A1 WO 2019153885A1 CN 2018121179 W CN2018121179 W CN 2018121179W WO 2019153885 A1 WO2019153885 A1 WO 2019153885A1
Authority
WO
WIPO (PCT)
Prior art keywords
aerosol
tobacco
stems
generating carrier
preparation
Prior art date
Application number
PCT/CN2018/121179
Other languages
English (en)
Chinese (zh)
Inventor
潘雪松
郑松明
Original Assignee
上海聚华科技股份有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 上海聚华科技股份有限公司 filed Critical 上海聚华科技股份有限公司
Publication of WO2019153885A1 publication Critical patent/WO2019153885A1/fr

Links

Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/241—Extraction of specific substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products

Definitions

  • the invention relates to the field of electronic cigarettes, in particular to a cigarette aerosol generating carrier for electrically heating non-combustion mode and a preparation method thereof.
  • the present invention provides a cigarette aerosol generating carrier for electrically heating non-combustion and a method of preparing the same to better solve the above-mentioned problems.
  • An aerosol aerosol generating carrier for electrically heating non-combustion, the cigarette aerosol generating carrier is heated when electrically heated to generate an aerosol, the cigarette aerosol generating carrier comprising a reconstituted stem,
  • the reconstituted cut stem is a reconstituted cut stem formed by removing the protein, polysaccharide, and nitrate substance from the tobacco stem by extracting and then filling the tobacco stem with a predetermined aroma substance.
  • the reconstituted stem of the cigarette aerosol generating carrier is electrically heated at a temperature ranging from 200 to 380 degrees Celsius to generate an aerosol.
  • the reconstituted stem wire further includes an aerosol, and the aerosol specifically includes one or a combination of a polyol, an ester of a polyol, a polymer, and a long carbon chain monohydric alcohol.
  • the aroma substances include one or a combination of an essential tobacco essential oil, a volatile natural product essential oil, a molecular distillation product of tobacco, and a volatile food flavor.
  • the materials prepared in steps 5.1 and 5.2 are fed through a feeding device, and the materials are sufficiently uniform through the extrusion homogenization process, and the water is equilibrated in a constant temperature and humidity process, and then packaged for use.
  • the extraction step in the step 5.1 specifically includes the following specific steps of removing or reducing the protein: adding phosphoric acid in the mixture of the solvent and the tobacco stem, and then placing the mixture in an ultra-high pressure container for a predetermined time.
  • the mixture in the ultrahigh pressure vessel is simultaneously ultrasonicated for a predetermined period of time.
  • the aerosol comprises one or a combination of a polyol, an ester of a polyol, a polymer, a long carbon chain monohydric alcohol.
  • the aroma substances include one or a combination of an essential tobacco essential oil, a volatile natural product essential oil, a molecular distillation product of tobacco, and a volatile food flavor.
  • the present invention also provides an aerosol-generating carrier for electric heating, the aerosol-generating carrier comprising a reconstituted stem, the re-cut stem is extracted by a general stem, and the protein and sugar in the original stem are removed. The reconstructed stems formed by the predetermined aroma substances are backfilled.
  • the reconstituted stem wire further includes an aerosol, and the aerosol specifically includes one or a combination of a polyol, an ester of a polyol, a polymer, and a long carbon chain monohydric alcohol.
  • the aroma substances include one or a combination of an essential tobacco essential oil, a volatile natural product essential oil, a molecular distillation product of tobacco, and a volatile food flavor.
  • the invention also provides a preparation method of an aerosol generating carrier for electric heating, comprising the following steps:
  • the cigarette aerosol generating carrier of the invention is suitable for heating at an electric heating temperature in the range of 200-380 degrees Celsius.
  • the composition of the aerosol generating carrier includes a special reconstruction.
  • the cut stem, the special reconstructed cut stem is a reconstructed stem which is formed by extracting or removing the protein, polysaccharide and nitrate substance from the general tobacco stem silk, and then backfilling the tobacco stem silk with the predetermined aroma substance. Because the protein, polysaccharide, nitrate and other substances in the tobacco stems are heated in this temperature range of electric heating, the polysaccharide and protein will produce a scorching odor, which seriously affects the taste of the eater.
  • the nitrate in the tobacco stems is decomposed by heat to produce nitrite (amine), which will cause harm to the human body, and fundamentally avoid the possibility of partial decomposition of nitrate to produce toxic gases.
  • the aerosol generating carrier of the invention adopts a special reconstituted stem wire, which can well solve the above defects of the general tobacco stem silk during electric heating.
  • there is also a special step of removing or reducing protein adding phosphoric acid in a mixture of solvent and tobacco stem, and then placing the mixture in an ultrahigh pressure vessel for a predetermined time, The mixture in the ultrahigh pressure vessel is simultaneously ultrasonicated for a predetermined period of time.
  • the addition of phosphoric acid can acidify the protein, and the side chain reactive group of the protein binds to the phosphate group.
  • the electrostatic repulsion between the protein molecules is increased, making them mutually repellent in the food system, and being easily dispersed to be water.
  • the solvent is dissolved.
  • protein molecules in the state of ultra-high pressure (500 MPa), can be polymerized into a polymer, and the molecular mass is increased, which is advantageous for interaction with a solvent such as water, and is advantageous for dissolution in a solvent.
  • Simultaneous ultrasonic treatment can cause structural changes in protein molecules and improve the solubility of proteins in solvents such as water.
  • An aerosol aerosol generating carrier for electrically heating non-combustion, the cigarette aerosol generating carrier is heated when electrically heated to generate an aerosol, the cigarette aerosol generating carrier comprising a reconstituted stem,
  • the reconstituted cut stem is a reconstituted cut stem formed by removing the protein, polysaccharide, and nitrate substance from the tobacco stem by extracting and then filling the tobacco stem with a predetermined aroma substance.
  • the reconstituted stem yarn further comprises an aerosol
  • the specific aerosol comprises a polyol such as propylene glycol, glycerol, triethylene glycol, 1,3-butanediol; and a polyol oxime ester such as glyceryl octanoic acid Ester; polymer, such as polyethylene glycol 200, polyethylene glycol 400, etc., as well as long carbon chain monohydric alcohols, such as solanesol present in tobacco.
  • the aroma substances in the reconstituted stems include hair tobacco essential oil, volatile natural product essential oil, molecular distillation products of tobacco, such as benzyl alcohol, phenethyl alcohol, dihydrodamascone, ⁇ -ionone, dihydro kiwi Lactone, solanone, phytol, phytonone, acacia-based acetone, eugenol, eugenol, 3-oxo- ⁇ -ionol, etc.
  • Fragrance components such as geranylacetone, neophytadiene, cedartriene diol, methyl octadecyl carbonate and other tobacco distillation fractions below 300 ° C; molecular distillation of natural products; volatile food flavors (including various Flavoring components such as floral, fruity, and characteristic flavors; combinations of one or more of them.
  • the preparation method comprises the following steps:
  • blank stems preparing tobacco stems, and adopting extraction, solid-liquid separation and drying processes on the tobacco stems to remove or reduce protein, polysaccharide and nitrate substances in the tobacco stems, and complete Preparation of blank stems;
  • the extraction step specifically includes the following special steps of removing or reducing the protein: adding phosphoric acid in the mixture of the solvent and the tobacco stem, and then placing the mixture in an ultra-high pressure container (about 500 MPa) for a predetermined time.
  • the mixture in the ultrahigh pressure vessel is simultaneously ultrasonically treated for the predetermined time.
  • tobacco stems In the process of tobacco growth, tobacco stems have their own special functions - to transport nutrients to the leaves, to promote the growth of tobacco, but also to grow themselves. Because of its transmission function, its internal structure is porous and multi-channel, so its special structure and effect are formed. This feature is beyond the characteristics of ordinary natural materials.
  • the invention fully utilizes the special structure and effect of the tobacco stem material, especially after the tobacco stem is extracted and processed, not only improves the space for effectively accommodating the material, but also avoids the inherent bad atmosphere released after being heated.
  • CN106723282A describes the use of porous tobacco stems to absorb the atomizing agent, thereby increasing the amount of smoke in the tobacco product, but does not consider the negative effect of the stalk ribbon on the smoking taste of the tobacco product, nor does it involve electric heating without burning. Case.
  • heating a non-combustible tobacco product requires heating the tobacco substrate to above 200 ° C to produce a nicotine-containing aerosol.
  • the tobacco matrix is continuously heated, and the protein and sugar contained in the heated body are coked as the temperature rises, giving an unpleasant scent.
  • the invention aims to provide a special reconstituted cut stem by applying the original stem material to the deficiencies of heating when not burning, and after extracting or removing the protein, polysaccharide and nitrate substance in the general tobacco stem silk, Reconstituted stems formed by backfilling the tobacco stems with a predetermined aroma substance. Because the protein, polysaccharide, nitrate and other substances in the tobacco stems are heated in this temperature range of electric heating, the polysaccharide and protein will produce a scorching odor, which seriously affects the taste of the eater.
  • nitrate in the tobacco stems is decomposed by heat to produce nitrite (amine), which will cause harm to the human body, and fundamentally avoid the possibility of partial decomposition of nitrate to produce toxic gases.
  • the cigarette aerosol generating carrier of the invention adopts a special reconstituted cut stem, which can well solve the above defects of the general tobacco stem silk during electric heating.
  • Tobacco stems include raw stems, stems, granules, and stalk powder, whether or not they are puffed, are within our range.
  • the form of the cut stem is preferred as an example. Including the following steps:
  • blank stems preparing tobacco stems, and adopting extraction, solid-liquid separation and drying processes on the tobacco stems to remove or reduce protein, polysaccharide and nitrate substances in the tobacco stems. Preparation of blank stems;
  • the materials prepared in the steps 1 and 2 are fed through a feeding device, and the material is sufficiently uniform by the extrusion homogenization process.
  • the homogenized smoke production forms a base material, and after water balance in a constant temperature and humidity process, it is packaged for use.
  • the elimination of most of the sugar can also avoid the scorching atmosphere when heating (including polysaccharide starch, pectin generated when the pectin is heated);
  • the solvent used for extraction in step 1 includes, but is not limited to, dilute mono-, di-, and triol solutions such as ethanol, propanol, propylene glycol, butanediol, glycerol, etc.;
  • a dilute solution of an organic acid such as acetic acid, citric acid, malic acid, lactic acid, etc.; also includes a suitable alkaline solution, an aqueous ammonia solution, a sodium carbonate solution, a sodium hydrogencarbonate solution, and the like.
  • the aroma components in step 2 include, but are not limited to, volatile tobacco essential oils, volatile natural product essential oils, molecular distillation products of tobacco, such as benzyl alcohol, phenethyl alcohol, dihydrodamascone, ⁇ -ionone, two Hydrogen kiwi lactone, solanone, phytol, phytonone, acacia alkaloid, eugenol, eugenol, 3-oxo- ⁇ -ionol, etc.
  • volatile tobacco essential oils such as benzyl alcohol, phenethyl alcohol, dihydrodamascone, ⁇ -ionone, two Hydrogen kiwi lactone, solanone, phytol, phytonone, acacia alkaloid, eugenol, eugenol, 3-oxo- ⁇ -ionol, etc.
  • Tobacco aroma components such as geranyl acetone, neophytadiene, cembtriene diol, methyl octadecyl carbonate, etc., tobacco distillation fractions below 300 ° C; molecular distillation of natural products; volatile food flavors (including Flavoring components such as various floral, fruity, and characteristic flavors; combinations of one or more of them.
  • Aerosols are known in the art including, but not limited to, polyols such as propylene glycol, glycerol, triethylene glycol, 1,3-butanediol; and polyol oxime esters such as glyceryl octanoic acid Ester; polymer, such as polyethylene glycol 200, polyethylene glycol 400, etc., as well as long carbon chain monohydric alcohols, such as solanesol present in tobacco.
  • polyols such as propylene glycol, glycerol, triethylene glycol, 1,3-butanediol
  • polyol oxime esters such as glyceryl octanoic acid Ester
  • polymer such as polyethylene glycol 200, polyethylene glycol 400, etc., as well as long carbon chain monohydric alcohols, such as solanesol present in tobacco.
  • Preferred aerosols are polyols or mixtures thereof.
  • the proportion of aerosol in the formation of aerosols can be adjusted between 5% and 70% according to the needs of the product.
  • the formation of the smoke production base (regardless of the carrier or the feed) is basically: deproteinization, de-sugarization, de-inorganic salt, to avoid adverse effects in the heating process.
  • the heating temperature is controlled in the range of 200 to 400 °C.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

L'invention concerne un support de génération de fumée de cigarette permettant un chauffage électrique sans combustion, et son procédé de préparation. Le support de génération de fumée de cigarette génère de la fumée lorsqu'il est chauffé électriquement, et le support de génération de fumée de cigarette comprend des tiges recréées, qui sont formées par réduction ou élimination des substances de protéine, de polysaccharide et de nitrate dans des tiges de tabac par extraction, puis par ajout de substances aromatiques prédéterminées aux tiges de tabac.
PCT/CN2018/121179 2018-02-09 2018-12-14 Support de génération de fumée de cigarette permettant un chauffage électrique sans combustion et son procédé de préparation WO2019153885A1 (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
CN201810136240.2 2018-02-09
CN201810136240 2018-02-09
CN201810737478.0A CN109105944A (zh) 2018-02-09 2018-07-06 用于电加热不燃烧的香烟气雾产生载体及其制备方法
CN201810737478.0 2018-07-06

Publications (1)

Publication Number Publication Date
WO2019153885A1 true WO2019153885A1 (fr) 2019-08-15

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ID=64822893

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Application Number Title Priority Date Filing Date
PCT/CN2018/121179 WO2019153885A1 (fr) 2018-02-09 2018-12-14 Support de génération de fumée de cigarette permettant un chauffage électrique sans combustion et son procédé de préparation

Country Status (2)

Country Link
CN (1) CN109105944A (fr)
WO (1) WO2019153885A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110150716A (zh) * 2019-05-09 2019-08-23 安徽中烟工业有限责任公司 一种用于加热不燃烧卷烟的雾化剂及其用途
CN115135175A (zh) * 2019-12-19 2022-09-30 尤尔实验室有限公司 有机基尼古丁凝胶组合物
CN113498874A (zh) * 2021-08-11 2021-10-15 河南金瑞香精香料有限公司 一种醇类逐口释放均匀的加热卷烟制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101422276A (zh) * 2008-12-04 2009-05-06 广东省金叶烟草薄片技术开发有限公司 一种调控烟草提取或萃取物中氯、硝酸盐含量的方法
CN102920012A (zh) * 2012-09-03 2013-02-13 上海聚华科技股份有限公司 通过烟叶再造烟草梗丝的方法
CN104968225A (zh) * 2013-01-24 2015-10-07 洛艾克有限公司 用于非易燃吸烟制品的气雾剂的功能化的方法、组分和装置
CN105707970A (zh) * 2016-04-22 2016-06-29 江苏中烟工业有限责任公司 一种混合型再造梗丝的制备方法
CN106333383A (zh) * 2016-08-30 2017-01-18 湖北中烟工业有限责任公司 一种适合烤烟风味的白肋烟再造烟叶的制备方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101422276A (zh) * 2008-12-04 2009-05-06 广东省金叶烟草薄片技术开发有限公司 一种调控烟草提取或萃取物中氯、硝酸盐含量的方法
CN102920012A (zh) * 2012-09-03 2013-02-13 上海聚华科技股份有限公司 通过烟叶再造烟草梗丝的方法
CN104968225A (zh) * 2013-01-24 2015-10-07 洛艾克有限公司 用于非易燃吸烟制品的气雾剂的功能化的方法、组分和装置
CN105707970A (zh) * 2016-04-22 2016-06-29 江苏中烟工业有限责任公司 一种混合型再造梗丝的制备方法
CN106333383A (zh) * 2016-08-30 2017-01-18 湖北中烟工业有限责任公司 一种适合烤烟风味的白肋烟再造烟叶的制备方法

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