WO2019151002A1 - Beverage and method for imparting milk flavor to beverage - Google Patents
Beverage and method for imparting milk flavor to beverage Download PDFInfo
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- WO2019151002A1 WO2019151002A1 PCT/JP2019/001577 JP2019001577W WO2019151002A1 WO 2019151002 A1 WO2019151002 A1 WO 2019151002A1 JP 2019001577 W JP2019001577 W JP 2019001577W WO 2019151002 A1 WO2019151002 A1 WO 2019151002A1
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- beverage
- acid
- milk
- milk flavor
- whey
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
Definitions
- the present invention relates to a beverage and a method for imparting a milk flavor to a beverage.
- Patent Document 1 describes a milk flavored beverage characterized by containing whey minerals and sweeteners, and substantially free of proteins and fats and oils.
- Patent Document 2 discloses a milk flavored beverage containing milk, milk protein stabilizer and water, having a non-fat milk solid content of 0.15 to 0.4% by mass and a pH of 4.0 or less. Have been described.
- the milk flavor drink specifically described in Patent Document 1 does not contain an acid, and the pH is considered to be near neutral.
- a beverage having a pH near neutral needs to be sufficiently sterilized (heated) for sale in the market. Therefore, it can be considered that an appropriate acid is added to lower the pH and relax the sterilization conditions.
- a certain amount of acid for example, citric acid, which is the most typical acid in the beverage field, was added to the milk flavored drink specifically described in Patent Document 1 to lower the pH. In this case, there is a problem that the milk flavor is lowered.
- the milk flavored beverage described in Patent Document 2 is cloudy because it contains a certain amount of milk protein.
- beverages called “flavored water” and the like that have a high transparency and have a flavor and flavor. Therefore, there was room for improvement in terms of transparency.
- an object of the present invention is to provide a beverage having a good milk flavor and high transparency even at a low pH.
- Whey minerals Including one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid, A beverage having a pH of less than 4.6 is provided.
- a method for imparting a milk flavor to a beverage wherein the beverage is obtained by adding at least one whey mineral and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid to the beverage.
- the beverage of this embodiment contains whey minerals and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid, and has a pH of less than 4.6.
- one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid, and gluconic acid are also referred to as “specific acids”.
- Whey mineral The beverage of this embodiment contains whey minerals.
- Whey minerals are known in the food and beverage industry as one of the food additives. Whey minerals are sometimes called whey minerals or whey salts.
- Whey minerals are generally produced by removing protein and lactose as much as possible from milk or whey. For this reason, generally, milk ash (mineral) is contained at a high concentration, and the proportion of ash in the solid is extremely high. And the mineral composition becomes a ratio close
- the ash content in the solid content of the whey mineral is, for example, 30% by mass or more, and specifically 50% by mass or more. A higher ash content is preferred.
- whey minerals can be obtained by using milk or whey as a raw material to remove proteins and lactose by membrane separation and / or ion exchange, cooling, and the like.
- the whey when whey is used as a raw material, the whey is not particularly limited, whey obtained as a by-product when producing cheese using milk, whey obtained as a by-product during casein production, Examples thereof include whey obtained by ultrafiltration of milk.
- examples of the membrane separation method include microfiltration membrane separation, ultrafiltration membrane separation, nanofiltration membrane separation, reverse osmosis membrane separation, and dialysis membrane separation.
- examples of the ion exchange method include electrodialysis membrane separation using a cation exchange membrane method and an anion exchange membrane method, and a method using an ion exchange resin.
- the whey mineral obtained by the above production method may remain in a liquid state, but may be concentrated and / or dried in terms of storage and handling.
- concentration method include a vacuum concentration method using an evaporator.
- drying method a generally used method such as spray drying or freeze drying can be appropriately selected.
- whey mineral for example, a commercial product of ADEKA (trade name: Milku Mineral L10, P10, etc.) may be used.
- the concentration (addition amount) of the whey mineral in the beverage is not particularly limited, but the amount of the solid content (component other than water) of the whey mineral is usually 0.1 to 2 g / L, preferably 0.1 to The amount is 1.5 g / L, more preferably 0.1 to 1 g / L, and still more preferably 0.2 to 0.8 g / L. By setting this amount, an appropriate milk flavor can be obtained.
- the concentration of potassium (K + ) that is particularly abundant as ash is set to the concentration of whey mineral. Can be used as an estimation index.
- the potassium concentration in the beverage is typically 1.5 mg / 100 mL or more, preferably 2.0 mg / 100 mL or more, more preferably 2.5 to 55 mg / 100 mL,
- the dose is preferably 2.6 to 45 mg / 100 mL, particularly preferably 2.6 to 30 mg / 100 mL, and most preferably 5 to 25 mg / 100 mL.
- the potassium concentration here is a density
- the potassium concentration in the beverage can be determined, for example, by analysis by atomic absorption spectrophotometry. Or it can also obtain
- the beverage of this embodiment includes one or more acids (specific acids) selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid.
- specific acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid.
- the sourness of these acids makes it difficult to disturb the milky taste of whey minerals and / or easily matches the milky taste, and as a result, a good milky taste can be obtained even at low pH. it is conceivable that.
- phosphoric acid has a weak aftertaste and does not interfere with the aftertaste (kokumi) of whey minerals, it is considered that phosphoric acid does not interfere with the milk flavor.
- tartaric acid has a weak persistent acidity like citric acid, it does not interfere with the aftertaste (kokumi) due to whey minerals and is considered to have good compatibility with milk flavor.
- the specific acid lactic acid or gluconic acid is preferable, and gluconic acid is particularly preferable.
- the milk flavor can be “enhanced” more than when no specific acid is used. This is also shown in the examples described later.
- Lactic acid may be contained in raw milk in a small amount, and is compatible with whey minerals. Therefore, it is presumed that it is easy to feel that the human taste is closer to the milk flavor.
- Gluconic acid also has a complex taste. This complex taste expresses the “richness” of milk, and as a result, it is presumed that the milk flavor is enhanced.
- the beverage of this embodiment may contain only one type of specific acid or may contain two or more types of specific acid.
- the combination of the specific acids is not particularly limited. For example, it is preferable to use a combination of gluconic acid and lactic acid. It is considered that this combined use can further enhance the milk flavor.
- the content of the specific acid in the beverage is not particularly limited, but is usually 0.01 to 2 g / L, preferably 0.05 to 1 g / L, more preferably 0.07 to 0.5 g / L, and still more preferably 0.08 to 0.3 g / L.
- the amount of the specific acid it is considered that the milk flavor can be further enhanced while the pH of the beverage is less than 4.6.
- the milk flavor can be further enhanced by adjusting the quantitative ratio between the whey mineral and the specific acid.
- the mass ratio of the whey mineral content in the beverage to the specific acid content in the beverage that is, the whey mineral content (mass) in the beverage / specific acid content (The value of (mass) is, for example, 0.3 to 10, preferably 0.5 to 10, more preferably 0.5 to 8, and still more preferably 1.5 to 6.5.
- it is preferably 0.5 to 4, and more preferably 0.5 to 1.5.
- “content of whey mineral” means the amount of solid content (components other than moisture) of whey mineral.
- the drink of this embodiment contains a plant extract as one aspect
- a plant extract in the beverage, it is possible to relieve the after-effect of sweetness, which is effective in improving the dryness.
- Plant extract is obtained by immersing plant raw materials in water or an organic solvent such as alcohol (typically ethanol) or a mixed solvent such as water and ethanol to extract components and distilling off the solvent. It is. Although it does not specifically limit as a plant raw material of a plant extract, Teas, coffee, cocoa, seeds, vegetables, a fruit, an herb, a spice, a seaweed etc. can be mentioned. In the beverage of this embodiment, it is preferable to use a plant extract made from tea, coffee, or herb as a plant material from the viewpoint of compatibility with milk flavor. That is, the beverage of this embodiment preferably contains one or more plant extracts selected from the group consisting of tea extracts, coffee extracts, and herbal extracts.
- tea extracts examples include green tea extract, black tea extract, oolong tea extract, hoji tea extract, pu-erh tea extract, mate tea extract, gymnema tea extract, dokudami tea extract, and other tea extracts that are generally regarded as favorite beverages. it can.
- the coffee extract may be an extract made from raw beans, or an extract made from roasted beans.
- herbal extracts include thyme extract, sage extract, rosemary extract, oregano extract, basil extract, mint extract and the like.
- the content is not particularly limited, but is usually 0.01 to 1 g / L, preferably 0.03 to 0.5 g / L, more preferably 0.05 to 0.2 g / L. It is. By setting it as this amount, it is possible to achieve both a good milk flavor and dryness at a high level.
- the beverage of this embodiment preferably contains a sweetener for improving palatability.
- a sweetener for improving palatability.
- known sweeteners can be used.
- sugars such as sucrose (sugar), glucose, granulated sugar, fructose, lactose, maltose, fructose, glucose liquid sugar, etc.
- low sweetness sweeteners such as xylitol and D-sorbitol, thaumatin, stevia extract, glycyrrhizin diacid
- high-intensity sweeteners such as sodium, acesulfame potassium, sucralose, aspartame, saccharin, neotame, and saccharin sodium.
- saccharides are preferable from the viewpoint of natural milk flavor, and sucrose (sugar) or fructose is more preferable.
- only 1 type may be used for a sweetener and it may use 2 or more types together.
- the content of the sweetener in the beverage is not particularly limited, but in the case of sugar, it is usually 10 to 200 g / L, preferably 20 to 100 g / L, more preferably 30 to 80 g / L. is there. It can be considered that a good palatability improvement effect can be obtained by setting this amount.
- the beverage of this embodiment contains a pH adjuster.
- a pH adjusting agent By including a pH adjusting agent, it is possible to obtain merits such as easy pH fine adjustment, and suppression of pH fluctuation during production or distribution of beverages.
- the pH adjuster include organic acid salts. More specifically, a sodium salt of carboxylic acid, a potassium salt of carboxylic acid, and the like can be given. In terms of suppressing the influence on taste as much as possible, when the organic acid that is the base of the organic acid salt is a polybasic acid, it is preferable that all carboxyl groups are neutralized.
- the beverage according to the present embodiment it is preferable to include the above-mentioned salt of a specific acid (such as sodium salt or potassium salt) as a pH adjuster.
- a specific acid such as sodium salt or potassium salt
- trisodium citrate can also be preferably used as a pH adjuster.
- the beverage of this embodiment may contain a fragrance for adjusting the milk flavor and other purposes.
- flavor which a drink can contain is not specifically limited, A well-known fragrance
- a milk flavor can be further enhanced by using a milk flavor.
- milk flavoring fragrances include fragrances containing aroma components characteristic of milk components such as lactones and short chain fatty acids.
- the beverage of this embodiment may contain various components other than those described above.
- the taste may be adjusted with salt.
- it may contain fruit juice, various nutritional components, coloring agents, diluents, antioxidants, thickening stabilizers and the like.
- the beverage contains substantially no colorant or a small amount (for example, 0.01 g / L or less).
- the pH of the beverage of this embodiment is less than 4.6.
- the pH is preferably 3.6 to 4.5, more preferably 3.7 to 4.2.
- the pH is preferably less than 4.6 from the viewpoint of production cost, flavor maintenance, browning suppression, and the like.
- the pH can be measured by using a commercially available pH meter.
- the pH can be adjusted, for example, by changing the amount of the specific acid or using a pH adjuster.
- the acidity of the beverage of this embodiment (the amount of acid contained in the beverage) is not particularly limited, but the milk flavor can be further enhanced by adjusting the acidity to an appropriate acidity.
- the upper limit is preferably 0.04% or less, more preferably 0. It is less than 03%, more preferably 0.025% or less, and particularly preferably 0.02% or less.
- the citric acidity is specifically determined by titration using the following procedure using a phenolphthalein indicator and sodium hydroxide.
- (1) Weigh accurately 5 to 15 g of beverage in a 200 mL Erlenmeyer flask and dilute to about 50 ml with water.
- (2) Add a few drops of 1% phenolphthalein indicator to the diluted beverage and stir.
- (3) While stirring the diluted beverage solution in the Erlenmeyer flask with a magnetic stirrer, 0.1M sodium hydroxide placed in a 25 mL burette is dropped into the beverage solution, and a titration test is performed.
- Citric acidity (%) A ⁇ f ⁇ (100 / W) ⁇ 0.0064 (Formula 1)
- A is the titration amount (mL) of 0.1 M sodium hydroxide solution
- f is the titer of 0.1 M sodium hydroxide solution
- W is the mass (g) of the beverage sample.
- the value of “0.0064” multiplied in (Equation 1) refers to the mass (g) of anhydrous citric acid corresponding to 1 mL of 0.1 M sodium hydroxide solution.
- a hydrogen ion concentration meter may be used instead of the phenolphthalein indicator.
- the end point of the titration test is when the pH of the beverage solution in the Erlenmeyer flask becomes 8.1.
- the beverage of this embodiment has a low content of acid components other than the specific acid (typically citric acid), or substantially does not contain any acid component other than the specific acid.
- the concentration of citric acid in the beverage of this embodiment is preferably 0 to 15 mg / 100 ml, more preferably 0 to 10 mg / 100 ml, and even more preferably 0.
- the concentration of citric acid can be determined by organic acid analysis by high performance liquid chromatography (HPLC), and the mass of citric acid used as a raw material. And the mass of citrate (excluding the mass corresponding to the counter cation).
- HPLC high performance liquid chromatography
- the beverage of the present embodiment contains an acid component other than the specific acid for some purpose. As long as a good milk flavor is felt, the beverage of this embodiment does not exclude the inclusion of an acid component other than the specific acid.
- the beverage of this embodiment can have high transparency.
- the absorbance at a wavelength of 650 nm of the beverage of the present embodiment is preferably 0.06 or less, more preferably 0.04 or less, and still more preferably 0.01 or less.
- the light absorbency in wavelength 420nm becomes like this.
- it is 0.1 or less, More preferably, it is 0.05 or less, More preferably, it is 0.01 or less.
- the light absorbency in this specification is a value measured by putting a beverage in a quartz cell having an optical path length of 1 cm.
- the beverage of this embodiment has a low protein content.
- the content of the protein contained in the beverage of this embodiment is, for example, 0 to 0.2 g / L, preferably 0 to 0.05 g / L, more preferably 0 to 0.03 g / L. .
- the Brix value of the beverage of the present embodiment is preferably 1 to 20 °, more preferably 2 to 10 °, and further preferably 2 to 8 ° from the viewpoint of improving the palatability of the beverage.
- the Brix value can be adjusted, for example, by the amount of the above-mentioned sweetener, the amount of other various components, and the like.
- the beverage of this embodiment can be obtained by uniformly mixing whey minerals, a specific acid, and if necessary other components in water according to a conventional method.
- the beverage of the present embodiment may be a container-packed beverage that has been heat-sterilized and packed in a container.
- the container at this time include a plastic bottle, an aluminum can, a steel can, a paper pack, a chilled cup, and a bottle.
- the container is preferably transparent, and specifically, a plastic bottle or an uncolored bottle is preferable.
- a container is a PET bottle from viewpoints, such as a handleability, distribution
- the beverage according to the present embodiment has a pH of less than 4.6, so that the conditions for heat sterilization can be moderated.
- the heat sterilization condition may be, for example, instantaneous sterilization at 90 to 135 ° C. or sterilization for 30 seconds.
- ⁇ Method for imparting milk flavor to beverages> there is a method for imparting a milk flavor to a beverage in addition to the beverage itself. Specifically, as an embodiment of the present invention, at least one whey mineral and one or more acids (specific acids) selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid are included in the beverage. There is a method for imparting a milk flavor to a beverage, in which a beverage is obtained by adding the above.
- the “whey mineral”, “specific acid”, and other components used in this method of imparting milk flavor are as described above in ⁇ Beverage>.
- the pH of the beverage finally obtained by this milk flavor imparting method is preferably less than 4.6.
- a more favorable milk flavor can be provided.
- Examples of the method of adjusting the pH of the beverage to less than 4.6 include a method of adjusting the addition amount of the specific acid and using a pH adjuster.
- Brix value A value measured at 20 ° C. using a sugar refractometer (RX-5000 ⁇ , Atago Co., Ltd.).
- PH Value measured with GST-5741C manufactured by Toa DKK Corporation.
- Citric acidity A value measured by the titration method described above.
- Citric acid concentration A value calculated from these components contained in the raw material and the amount of raw material used.
- Preliminary test A beverage containing whey minerals but not acid was prepared as a “standard” for evaluation. Specifically, beverages were prepared by uniformly mixing each component described in “Control Example” in Table 1 in water, and the resulting beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained. And 5 subjects took this drink. Various numerical values were measured / calculated.
- the strength of the acidity of the beverage of this control example was set to the reference point “4 points” in the seven-step evaluation from the following 1 point to 7 points in each subject.
- an embodiment comprising whey minerals and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid, and having a pH of less than 4.6. It was confirmed that the beverages 1 to 4 had a milk flavor (good milk feeling, good milk taste) similar to the control example. In addition, the beverages of Examples 1 to 4 had better milk flavor (good milk feeling, good milk taste) than beverages containing citric acid or malic acid as acids (Comparative Examples 1 and 2). It was.
- the sourness of the beverages of Examples 1 to 4 was suppressed as compared with the beverages of Comparative Examples 1 and 2. This suggests that the beverages of Examples 1 to 4 not only did not inhibit the milk flavor due to the acidity, but also improved the thirstability over citric acid.
- the ease of drinking of the beverages of Examples 1 to 4 was the same as or better than the beverage of the comparative example. It can be seen that the ease of drinking tends to be improved by using phosphoric acid, tartaric acid, lactic acid or gluconic acid as the acid.
- Example 3 using lactic acid as the specific acid and Example 4 using gluconic acid
- the milk feeling and richness were significantly improved as compared with the control example.
- the milk flavor can be “enhanced” more than when no acid is used.
- the amount of whey mineral itself is preferably about 0.2 to 0.8 g / L (in the amount of potassium, 5.3 to 21.). 4 mg / 100 mL).
- Example 1 in the control example 7 points evaluation (1 to 7 points) with 4 points as reference points.
- Various numerical values were measured / calculated. Table 4 shows the average values of various numerical values and the scores of five people. For milk flavor (good milk feeling), good aftertaste and ease of drinking, the larger the number, the better the result. As for the strength of the sweetness pull-back, the smaller the value, the better the result (the effect of improving the thirst is high).
- Example 11 Each component described in Table 5 as “Example 11” was uniformly mixed in water to prepare a beverage, and the resulting beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained.
- the milk flavor good milk feeling, good milk taste
- ease of drinking and sourness when ingesting this packaged beverage five panelists were given the above I.S.
- a 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example).
- Various numerical values were measured / calculated. Table 5 shows the average values of various numerical values and the scores of five people.
- milk flavor good milk feeling, good milk taste
- ease of drinking the larger the number, the better the result.
- About sourness intensity it shows that it is so favorable that a numerical value is small.
- the amount of phosphoric acid is considerably higher (compared to the amount of whey minerals), and even if the beverage has a relatively large citric acidity of about 0.03%, the ease of drinking is better than the control example.
- the acidity was equivalent to that of the control example.
- the amount of phosphoric acid was considerably large, the decrease in milk flavor (good milk feeling and good milk taste) was suppressed to only 0.2 points compared to the control example. That is, it was confirmed that a sufficient milk flavor can be felt.
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Abstract
Description
例えば、特許文献1には、乳清ミネラルと、甘味料とを含み、タンパク質及び油脂を実質的に含まないことを特徴とする乳風味飲料が記載されている。
また、特許文献2には、乳、乳蛋白質の安定化剤及び水を含み、無脂乳固形分量が0.15~0.4質量%で、pHが4.0以下である乳風味飲料が記載されている。 In the field of beverages, various studies have been made on milk-flavored beverages.
For example, Patent Document 1 describes a milk flavored beverage characterized by containing whey minerals and sweeteners, and substantially free of proteins and fats and oils.
Patent Document 2 discloses a milk flavored beverage containing milk, milk protein stabilizer and water, having a non-fat milk solid content of 0.15 to 0.4% by mass and a pH of 4.0 or less. Have been described.
しかし、これら従来の乳風味飲料については、以下の点で改良の余地があった。 As described above, various studies have been made on milk-flavored beverages.
However, these conventional milk flavor drinks have room for improvement in the following points.
pHが中性付近の飲料は、市場での販売のためには十分な殺菌(加熱)を行う必要がある。よって、適当な酸を加えてpHを下げ、殺菌条件を緩和することが考えられる。
しかし、本発明者の検討によれば、特許文献1に具体的に記載された乳風味飲料に、酸、例えば飲料分野で最も代表的な酸であるクエン酸を一定量加えてpHを下げた場合、乳風味が低下するという問題がある。 The milk flavor drink specifically described in Patent Document 1 does not contain an acid, and the pH is considered to be near neutral.
A beverage having a pH near neutral needs to be sufficiently sterilized (heated) for sale in the market. Therefore, it can be considered that an appropriate acid is added to lower the pH and relax the sterilization conditions.
However, according to the study of the present inventor, a certain amount of acid, for example, citric acid, which is the most typical acid in the beverage field, was added to the milk flavored drink specifically described in Patent Document 1 to lower the pH. In this case, there is a problem that the milk flavor is lowered.
乳清ミネラルと、
リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸とを含み、
pHが4.6未満である飲料
が提供される。 According to the present invention,
Whey minerals,
Including one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid,
A beverage having a pH of less than 4.6 is provided.
飲料に、少なくとも、乳清ミネラルと、リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸とを添加して飲料を得る、飲料への乳風味付与方法
が提供される。 Moreover, according to the present invention,
A method for imparting a milk flavor to a beverage, wherein the beverage is obtained by adding at least one whey mineral and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid to the beverage. Is provided.
本明細書中、数値範囲の説明における「a~b」との表記は、特に断らない限り、a以上b以下のことを表す。例えば、「1~5質量%」とは「1質量%以上5質量%以下」の意である。 Hereinafter, embodiments of the present invention will be described in detail.
In the present specification, the notation “a to b” in the description of numerical ranges represents a to b inclusive unless otherwise specified. For example, “1-5 mass%” means “1 mass% or more and 5 mass% or less”.
本実施形態の飲料は、乳清ミネラルと、リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸とを含み、pHが4.6未満である。
なお、以下では、「リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸」を、「特定酸」とも表記する。 <Beverage>
The beverage of this embodiment contains whey minerals and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid, and has a pH of less than 4.6.
In the following, “one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid, and gluconic acid” are also referred to as “specific acids”.
また、本発明者の知見によれば、特定酸の酸味は、いずれも、クエン酸などの飲料分野で使用される他の酸の酸味に比べて、乳清ミネラルによる乳風味を邪魔しづらく、かつ/または、乳風味とマッチしやすく、結果として低pHであっても飲用者が良好な乳風味を感じられるものと推定される。
「透明で低pHであるにもかかわらず、良好な乳風味が感じられる」という意外性は、本実施形態の飲料独自のものである。 In this drink, transparency can be increased by using whey minerals in order to give a milk flavor.
Further, according to the knowledge of the present inventor, the acidity of the specific acid is less likely to disturb the milky taste due to whey minerals than the acidity of other acids used in the beverage field such as citric acid, And / or it is estimated that it is easy to match the milk flavor, and as a result, the drinker can feel a good milk flavor even at a low pH.
The surprising property that “a good milk flavor is felt despite being transparent and low pH” is unique to the beverage of the present embodiment.
本実施形態の飲料は、乳清ミネラルを含む。乳清ミネラルは、食品添加物の1つとして、食品・飲料業界で知られたものである。乳清ミネラルは、ホエイミネラルまたはホエイソルトと呼ばれることもある。 [Whey mineral]
The beverage of this embodiment contains whey minerals. Whey minerals are known in the food and beverage industry as one of the food additives. Whey minerals are sometimes called whey minerals or whey salts.
乳清ミネラルの固形分に占める灰分含量は、例えば30質量%以上であり、具体的には50質量%以上である。灰分含量は高いほうが好ましい。 Whey minerals are generally produced by removing protein and lactose as much as possible from milk or whey. For this reason, generally, milk ash (mineral) is contained at a high concentration, and the proportion of ash in the solid is extremely high. And the mineral composition becomes a ratio close | similar to the mineral composition in the milk or whey used as a raw material.
The ash content in the solid content of the whey mineral is, for example, 30% by mass or more, and specifically 50% by mass or more. A higher ash content is preferred.
上記製造方法において、原料として乳清を用いる場合、その乳清は特に限定されず、乳を使用してチーズを製造する際に副産物として得られるホエイ、カゼイン製造の際に副産物として得られるホエイ、乳を限外濾過することによって得られるホエイなどを挙げることができる。
上記製造方法において、膜分離の方法としては、精密濾過膜分離、限外濾過膜分離、ナノ濾過膜分離、逆浸透膜分離、透析膜分離等を挙げることができる。
上記製造方法において、イオン交換の方法としては、陽イオン交換膜法や陰イオン交換膜法を用いる電気透析膜分離や、イオン交換樹脂による方法等を挙げることができる。 As a specific method for producing whey minerals, whey minerals can be obtained by using milk or whey as a raw material to remove proteins and lactose by membrane separation and / or ion exchange, cooling, and the like.
In the above production method, when whey is used as a raw material, the whey is not particularly limited, whey obtained as a by-product when producing cheese using milk, whey obtained as a by-product during casein production, Examples thereof include whey obtained by ultrafiltration of milk.
In the above production method, examples of the membrane separation method include microfiltration membrane separation, ultrafiltration membrane separation, nanofiltration membrane separation, reverse osmosis membrane separation, and dialysis membrane separation.
In the above production method, examples of the ion exchange method include electrodialysis membrane separation using a cation exchange membrane method and an anion exchange membrane method, and a method using an ion exchange resin.
飲料中のカリウム濃度は、例えば、原子吸光光度法による分析で求めることができる。または、飲料の原材料中のカリウム濃度と、原材料の使用量とから、計算により求めることもできる。 In addition, the potassium concentration here is a density | concentration of the total potassium contained not only in the potassium derived from a whey mineral but in a drink.
The potassium concentration in the beverage can be determined, for example, by analysis by atomic absorption spectrophotometry. Or it can also obtain | require by calculation from the potassium concentration in the raw material of a drink, and the usage-amount of a raw material.
本実施形態の飲料は、リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸(特定酸)を含む。前述したが、これらの酸による酸味は、乳清ミネラルによる乳風味を邪魔しづらく、かつ/または、乳風味とマッチしやすく、その結果として、低pHであっても良好な乳風味が得られると考えられる。 [Specific acid]
The beverage of this embodiment includes one or more acids (specific acids) selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid. As described above, the sourness of these acids makes it difficult to disturb the milky taste of whey minerals and / or easily matches the milky taste, and as a result, a good milky taste can be obtained even at low pH. it is conceivable that.
乳酸は、生乳に若干量含まれていることもあり、乳清ミネラルとの相性がよい。よって、人間の味覚において、より乳風味に近いと感じやすいものと推測される。
また、グルコン酸には複雑味がある。この複雑味が、乳の「コク」を表現し、結果、乳風味が高められるものと推測される。 The reason why the milk flavor can be “enhanced” can be explained as follows although it is speculated.
Lactic acid may be contained in raw milk in a small amount, and is compatible with whey minerals. Therefore, it is presumed that it is easy to feel that the human taste is closer to the milk flavor.
Gluconic acid also has a complex taste. This complex taste expresses the “richness” of milk, and as a result, it is presumed that the milk flavor is enhanced.
本実施形態の飲料においては、乳清ミネラルと特定酸との量比を調整することで、乳風味を一層高めることができる。また、飲みやすさの一層の向上なども期待しうる。
具体的には、飲料中の特定酸の含有量に対する、飲料中の乳清ミネラルの含有量の質量比(つまり、飲料中の、乳清ミネラルの含有量(質量)/特定酸の含有量(質量)の値)が、例えば0.3~10であり、好ましくは0.5~10であり、より好ましくは0.5~8であり、さらに好ましくは1.5~6.5である。特にまた、飲みやすさも向上させる観点からは、好ましくは0.5~4であり、より好ましくは0.5~1.5である。なお、ここでの「乳清ミネラルの含有量」は、乳清ミネラルの固形分(水分以外の成分)の量の意である。 [Quantity ratio between whey mineral and specified acid]
In the beverage of the present embodiment, the milk flavor can be further enhanced by adjusting the quantitative ratio between the whey mineral and the specific acid. In addition, further improvement in ease of drinking can be expected.
Specifically, the mass ratio of the whey mineral content in the beverage to the specific acid content in the beverage (that is, the whey mineral content (mass) in the beverage / specific acid content ( The value of (mass) is, for example, 0.3 to 10, preferably 0.5 to 10, more preferably 0.5 to 8, and still more preferably 1.5 to 6.5. In particular, from the viewpoint of improving ease of drinking, it is preferably 0.5 to 4, and more preferably 0.5 to 1.5. Here, “content of whey mineral” means the amount of solid content (components other than moisture) of whey mineral.
本実施形態の飲料は、一態様として、植物エキスを含むことが好ましい。飲料が植物エキスを含むことで、甘さの後引きを和らげることができ、止渇性の向上等に効果的である。 [Plant extract]
It is preferable that the drink of this embodiment contains a plant extract as one aspect | mode. By including a plant extract in the beverage, it is possible to relieve the after-effect of sweetness, which is effective in improving the dryness.
植物エキスの植物原料としては、特に限定されないが、茶類、コーヒー、ココア、種実類、野菜、果実、ハーブ、スパイス、海藻などを挙げることができる。
本実施形態の飲料においては、乳風味との相性の点から、茶類、コーヒーまたはハーブを植物原料とする植物エキスを用いることが好ましい。つまり、本実施形態の飲料は、茶類エキス、コーヒーエキスおよびハーブエキスからなる群より選ばれる1種または2種以上の植物エキスを含むことが好ましい。 “Plant extract” is obtained by immersing plant raw materials in water or an organic solvent such as alcohol (typically ethanol) or a mixed solvent such as water and ethanol to extract components and distilling off the solvent. It is.
Although it does not specifically limit as a plant raw material of a plant extract, Teas, coffee, cocoa, seeds, vegetables, a fruit, an herb, a spice, a seaweed etc. can be mentioned.
In the beverage of this embodiment, it is preferable to use a plant extract made from tea, coffee, or herb as a plant material from the viewpoint of compatibility with milk flavor. That is, the beverage of this embodiment preferably contains one or more plant extracts selected from the group consisting of tea extracts, coffee extracts, and herbal extracts.
コーヒーエキスとしては、生豆を原料としたエキスでもよいし、焙煎豆を原料としたエキスでもよい。
ハーブエキスとしては、タイムエキス、セージエキス、ローズマリーエキス、オレガノエキス、バジルエキス、ミントエキスなどを挙げることができる。 Examples of tea extracts include green tea extract, black tea extract, oolong tea extract, hoji tea extract, pu-erh tea extract, mate tea extract, gymnema tea extract, dokudami tea extract, and other tea extracts that are generally regarded as favorite beverages. it can.
The coffee extract may be an extract made from raw beans, or an extract made from roasted beans.
Examples of herbal extracts include thyme extract, sage extract, rosemary extract, oregano extract, basil extract, mint extract and the like.
本実施形態の飲料は、嗜好性を向上させるなどのため、甘味料を含むことが好ましい。
甘味料としては、公知のものを使用することができる。例えば、ショ糖(砂糖)、ブドウ糖、グラニュー糖、果糖、乳糖、麦芽糖、果糖ブドウ糖液糖等の糖類、キシリトール、およびD-ソルビトール等の低甘味度甘味料、タウマチン、ステビア抽出物、グリチルリチン酸二ナトリウム、アセスルファムカリウム、スクラロース、アスパルテーム、サッカリン、ネオテーム、サッカリンナトリウム等の高甘味度甘味料などが挙げられる。これらの中でも、自然な乳風味という点からは、糖類が好ましく、ショ糖(砂糖)または果糖がより好ましい。また、甘味料は1種のみを用いてもよいし2種以上を併用してもよい。 [sweetener]
The beverage of this embodiment preferably contains a sweetener for improving palatability.
Known sweeteners can be used. For example, sugars such as sucrose (sugar), glucose, granulated sugar, fructose, lactose, maltose, fructose, glucose liquid sugar, etc., low sweetness sweeteners such as xylitol and D-sorbitol, thaumatin, stevia extract, glycyrrhizin diacid Examples include high-intensity sweeteners such as sodium, acesulfame potassium, sucralose, aspartame, saccharin, neotame, and saccharin sodium. Among these, saccharides are preferable from the viewpoint of natural milk flavor, and sucrose (sugar) or fructose is more preferable. Moreover, only 1 type may be used for a sweetener and it may use 2 or more types together.
本実施形態の飲料は、pH調整剤を含むことが好ましい。pH調整剤を含むことで、pHの微調整が容易となる、飲料の製造時や流通時のpH変動が抑えられる等のメリットを得ることができる。 [PH adjuster]
It is preferable that the beverage of this embodiment contains a pH adjuster. By including a pH adjusting agent, it is possible to obtain merits such as easy pH fine adjustment, and suppression of pH fluctuation during production or distribution of beverages.
なお、呈味への影響をできるだけ抑えるという点では、有機酸の塩の元となる有機酸が多塩基酸の場合は、全てのカルボキシル基が中和されていることが好ましい。 Specific examples of the pH adjuster include organic acid salts. More specifically, a sodium salt of carboxylic acid, a potassium salt of carboxylic acid, and the like can be given.
In terms of suppressing the influence on taste as much as possible, when the organic acid that is the base of the organic acid salt is a polybasic acid, it is preferable that all carboxyl groups are neutralized.
本実施形態の飲料は、乳風味の調整やその他の目的のため、香料を含んでもよい。飲料が含むことができる香料は特に限定されず、公知の香料を適宜用いることができる。例えば、乳風味の香料を用いることで、乳風味を一層引き立てられると考えられる。乳風味の香料としては、ラクトン類、短鎖脂肪酸等の乳成分に特徴的な香気成分を含む香料を挙げることができる。 [Fragrance]
The beverage of this embodiment may contain a fragrance for adjusting the milk flavor and other purposes. The fragrance | flavor which a drink can contain is not specifically limited, A well-known fragrance | flavor can be used suitably. For example, it is considered that a milk flavor can be further enhanced by using a milk flavor. Examples of milk flavoring fragrances include fragrances containing aroma components characteristic of milk components such as lactones and short chain fatty acids.
本実施形態の飲料は、上記以外の種々の成分を含んでもよい。例えば、食塩により味を調製するなどしてもよい。また、果汁、各種栄養成分、着色料、希釈剤、酸化防止剤、増粘安定剤等を含んでもよい。
ただし、透明性の観点からは、飲料は、着色料を実質的に含まないか、含むとしても少量である(例えば0.01g/L以下)ことが好ましい。 [Other ingredients]
The beverage of this embodiment may contain various components other than those described above. For example, the taste may be adjusted with salt. Further, it may contain fruit juice, various nutritional components, coloring agents, diluents, antioxidants, thickening stabilizers and the like.
However, from the viewpoint of transparency, it is preferable that the beverage contains substantially no colorant or a small amount (for example, 0.01 g / L or less).
本実施形態の飲料のpHは4.6未満である。pHは、好ましくは3.6~4.5、より好ましくは3.7~4.2である。
pHが4.6未満であることで、殺菌条件を緩和することができる。特に日本では、法令上、飲料のpHが4.6以上であると、飲料の殺菌条件を厳しくする必要がある。よって、製造コストや香味維持、褐変抑制等の観点から、pHは4.6未満であることが好ましい。また、pHが3.7以上であることで、酸味が目立ちすぎることが無く、乳風味を一層高めることができる。
なお、pHの測定は、市販のpH測定器を用いるなどして行うことができる。
pHの調整は、例えば、特定酸の量を変えることや、pH調整剤を用いることなどにより行うことができる。 [PH]
The pH of the beverage of this embodiment is less than 4.6. The pH is preferably 3.6 to 4.5, more preferably 3.7 to 4.2.
When the pH is less than 4.6, sterilization conditions can be relaxed. Particularly in Japan, it is necessary to tighten the sterilization conditions of beverages when the pH of the beverage is 4.6 or more according to the law. Therefore, the pH is preferably less than 4.6 from the viewpoint of production cost, flavor maintenance, browning suppression, and the like. Moreover, since pH is 3.7 or more, a sour taste does not stand out too much and a milk flavor can be improved further.
The pH can be measured by using a commercially available pH meter.
The pH can be adjusted, for example, by changing the amount of the specific acid or using a pH adjuster.
本実施形態の飲料の酸度(飲料に含まれている酸の量)は、特に限定されないが、適切な酸度に調整されることで、乳風味をさらに高めることができる。
具体的には、クエン酸の相当量として換算した値(本明細書では、この値を「クエン酸度」ともいう)において、上限が、好ましくは0.04%以下であり、より好ましくは0.03%未満であり、さらに好ましくは0.025%以下であり、特に好ましくは0.02%以下である。下限は特にない(典型的には0%より大きい値である)。 [Acidity (citric acidity)]
The acidity of the beverage of this embodiment (the amount of acid contained in the beverage) is not particularly limited, but the milk flavor can be further enhanced by adjusting the acidity to an appropriate acidity.
Specifically, in the value converted as the equivalent amount of citric acid (this value is also referred to as “citric acid degree” in this specification), the upper limit is preferably 0.04% or less, more preferably 0. It is less than 03%, more preferably 0.025% or less, and particularly preferably 0.02% or less. There is no particular lower limit (typically a value greater than 0%).
(1)200mL三角フラスコに対して5~15gの飲料を正確に秤量し、水を用いて50ml程度まで希釈する。
(2)希釈した上記飲料に対して1%フェノールフタレイン指示薬を数滴加えて撹拌する。
(3)三角フラスコ内の希釈飲料溶液をマグネティックスターラーで撹拌しながら、25mLビューレットに入れた0.1Mの水酸化ナトリウムを上記飲料溶液に滴下し、滴定試験を実施する。この滴定試験は、三角フラスコ内の飲料溶液の色が、30秒間赤色を持続した点を終点とする。そして、
(4)クエン酸酸度(%)の値を、滴定試験の結果に基づき、次式によって算出する。
クエン酸酸度(%)=A×f×(100/W)×0.0064 (式1)
[(式1)において、Aは、0.1M水酸化ナトリウム溶液の滴定量(mL)を、fは、0.1M水酸化ナトリウム溶液の力価を、Wは、飲料試料の質量(g)を示す。(式1)において乗算している「0.0064」という値は、1mLの0.1M水酸化ナトリウム溶液に相当する無水クエン酸の質量(g)を指す。] Here, in this specification, the citric acidity is specifically determined by titration using the following procedure using a phenolphthalein indicator and sodium hydroxide.
(1) Weigh accurately 5 to 15 g of beverage in a 200 mL Erlenmeyer flask and dilute to about 50 ml with water.
(2) Add a few drops of 1% phenolphthalein indicator to the diluted beverage and stir.
(3) While stirring the diluted beverage solution in the Erlenmeyer flask with a magnetic stirrer, 0.1M sodium hydroxide placed in a 25 mL burette is dropped into the beverage solution, and a titration test is performed. In this titration test, the end point is the point where the color of the beverage solution in the Erlenmeyer flask has remained red for 30 seconds. And
(4) The value of citric acidity (%) is calculated by the following formula based on the result of the titration test.
Citric acidity (%) = A × f × (100 / W) × 0.0064 (Formula 1)
[In (Formula 1), A is the titration amount (mL) of 0.1 M sodium hydroxide solution, f is the titer of 0.1 M sodium hydroxide solution, and W is the mass (g) of the beverage sample. Indicates. The value of “0.0064” multiplied in (Equation 1) refers to the mass (g) of anhydrous citric acid corresponding to 1 mL of 0.1 M sodium hydroxide solution. ]
本実施形態の飲料は、良好な乳風味の観点から、特定酸以外の酸成分(代表的にはクエン酸)の含有量が少ないか、または特定酸以外の酸成分を実質的に含まないことが好ましい。
具体的には、本実施形態の飲料におけるクエン酸の濃度は、好ましくは0~15mg/100mlであり、より好ましくは0~10mg/100mlであり、さらに好ましくは0である。
なお、クエン酸(酸アニオンの状態で系中に存在するものも含む)の濃度は、高速液体クロマトグラフィー(HPLC)法による有機酸分析で求めることができるし、原料に用いたクエン酸の質量やクエン酸塩の質量(対カチオンに相当する質量は除く)から求めることもできる。
ちなみに、何らかの目的により、本実施形態の飲料が、特定酸以外の酸成分を含むことは、必ずしも排除されない。良好な乳風味が感じられる限りにおいて、本実施形態の飲料は、特定酸以外の酸成分を含むことを排除するものではない。 [Concentration of citric acid]
From the viewpoint of good milk flavor, the beverage of this embodiment has a low content of acid components other than the specific acid (typically citric acid), or substantially does not contain any acid component other than the specific acid. Is preferred.
Specifically, the concentration of citric acid in the beverage of this embodiment is preferably 0 to 15 mg / 100 ml, more preferably 0 to 10 mg / 100 ml, and even more preferably 0.
The concentration of citric acid (including those present in the system in the form of acid anions) can be determined by organic acid analysis by high performance liquid chromatography (HPLC), and the mass of citric acid used as a raw material. And the mass of citrate (excluding the mass corresponding to the counter cation).
Incidentally, it is not necessarily excluded that the beverage of the present embodiment contains an acid component other than the specific acid for some purpose. As long as a good milk flavor is felt, the beverage of this embodiment does not exclude the inclusion of an acid component other than the specific acid.
本実施形態の飲料は、前述したように、透明性を高くすることができる。
具体的には、本実施形態の飲料の波長650nmにおける吸光度が好ましくは0.06以下であり、より好ましくは0.04以下であり、さらに好ましくは0.01以下である。
また、波長420nmにおける吸光度は、好ましくは0.1以下であり、より好ましくは0.05以下であり、さらに好ましくは0.01以下である。
なお、本明細書での吸光度は、光路長1cmの石英セルに飲料を入れて測定される値である。 [transparency]
As described above, the beverage of this embodiment can have high transparency.
Specifically, the absorbance at a wavelength of 650 nm of the beverage of the present embodiment is preferably 0.06 or less, more preferably 0.04 or less, and still more preferably 0.01 or less.
Moreover, the light absorbency in wavelength 420nm becomes like this. Preferably it is 0.1 or less, More preferably, it is 0.05 or less, More preferably, it is 0.01 or less.
In addition, the light absorbency in this specification is a value measured by putting a beverage in a quartz cell having an optical path length of 1 cm.
本実施形態の飲料のBrix値は、飲料の嗜好性を向上させる観点から、好ましくは1~20°であり、より好ましくは2~10°であり、さらに好ましくは2~8°である。
Brix値は、例えば、前述の甘味料の量、その他の各種成分の量などにより調整することができる。 [Brix value]
The Brix value of the beverage of the present embodiment is preferably 1 to 20 °, more preferably 2 to 10 °, and further preferably 2 to 8 ° from the viewpoint of improving the palatability of the beverage.
The Brix value can be adjusted, for example, by the amount of the above-mentioned sweetener, the amount of other various components, and the like.
本実施形態の飲料は、乳清ミネラルと特定酸、必要に応じてその他の成分を、定法に従って水に均一に混合することで得ることができる。
本実施形態の飲料は、加熱殺菌され、容器に詰められた状態の容器詰め飲料としてもよい。このときの容器としては、ペットボトル、アルミ缶、スチール缶、紙パック、チルドカップ、瓶等が挙げられる。本実施形態の飲料の特徴の1つである「透明性」の訴求の点からは、容器は透明であることが好ましく、具体的にはペットボトルまたは無着色の瓶が好ましい。また、取扱性、流通性、携帯性等の観点から、容器はペットボトルであることが好ましい。 [Manufacturing method, container, etc.]
The beverage of this embodiment can be obtained by uniformly mixing whey minerals, a specific acid, and if necessary other components in water according to a conventional method.
The beverage of the present embodiment may be a container-packed beverage that has been heat-sterilized and packed in a container. Examples of the container at this time include a plastic bottle, an aluminum can, a steel can, a paper pack, a chilled cup, and a bottle. From the point of appeal of “transparency” which is one of the characteristics of the beverage of this embodiment, the container is preferably transparent, and specifically, a plastic bottle or an uncolored bottle is preferable. Moreover, it is preferable that a container is a PET bottle from viewpoints, such as a handleability, distribution | circulation property, and portability.
本発明の実施形態としては、飲料そのもののほか、飲料への乳風味付与方法もある。
具体的には、本発明の実施形態として、飲料に、少なくとも、乳清ミネラルと、リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸(特定酸)とを添加して飲料を得る、飲料への乳風味付与方法がある。
この乳風味付与方法で用いられる「乳清ミネラル」や「特定酸」、その他の成分などについては、上記<飲料>で説明のとおりである。 <Method for imparting milk flavor to beverages>
As an embodiment of the present invention, there is a method for imparting a milk flavor to a beverage in addition to the beverage itself.
Specifically, as an embodiment of the present invention, at least one whey mineral and one or more acids (specific acids) selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid are included in the beverage. There is a method for imparting a milk flavor to a beverage, in which a beverage is obtained by adding the above.
The “whey mineral”, “specific acid”, and other components used in this method of imparting milk flavor are as described above in <Beverage>.
I.~VII.の試験における共通事項について以下に説明しておく。 We asked five subjects to cooperate. To VII. The milk flavor and the like of beverages having various compositions were evaluated by the above test.
I. To VII. The common items in these tests are described below.
乳清ミネラルについては、株式会社ADEKAの「みるくのミネラルL10」(固形分(水分以外の成分)濃度:10質量%)を用いた。その他成分については市販品を適宜用いた。 <Ingredients>
As for the whey mineral, “Mikuru Mineral L10” (solid content (component other than moisture) concentration: 10% by mass) of ADEKA Corporation was used. Regarding other components, commercially available products were appropriately used.
・Brix値:糖用屈折計(RX-5000α、株式会社アタゴ)を用いて20℃で測定した値である。
・pH:東亜ディーケーケー社製 GST-5741Cにて測定した値である。
・クエン酸酸度:前述の滴定法により測定される値である。
・吸光度(波長420nm、650nm):飲料を光路長1cmのセルに入れて、市販の分光光度計で測定した値である。
・クエン酸濃度:原材料中に含まれるこれら成分と原材料の使用量から算出される値である。
・カリウム(K+)、カルシウム(Ca2+):原材料中に含まれるこれら成分と原材料の使用量から算出される値である。 <About various numerical values>
Brix value: A value measured at 20 ° C. using a sugar refractometer (RX-5000α, Atago Co., Ltd.).
PH: Value measured with GST-5741C manufactured by Toa DKK Corporation.
Citric acidity: A value measured by the titration method described above.
Absorbance (wavelength: 420 nm, 650 nm): A value obtained by putting a beverage in a cell having an optical path length of 1 cm and measuring with a commercially available spectrophotometer.
Citric acid concentration: A value calculated from these components contained in the raw material and the amount of raw material used.
-Potassium (K <+> ), calcium (Ca < 2+ > ): It is a value calculated from the usage-amount of these components contained in a raw material, and a raw material.
評価の「基準」となる、乳清ミネラルを含むが酸を含まない飲料を調合した。具体的には、表1の「対照例」に記載の各成分を水中で均一に混合して飲料を調合し、得られた飲料を95℃瞬間殺菌にて殺菌し、容器に詰めた。これにより容器詰飲料を得た。そして、この飲料を、被験者5人に飲用してもらった。また、各種数値を測定/算出した。 I. Preliminary test A beverage containing whey minerals but not acid was prepared as a “standard” for evaluation. Specifically, beverages were prepared by uniformly mixing each component described in “Control Example” in Table 1 in water, and the resulting beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained. And 5 subjects took this drink. Various numerical values were measured / calculated.
7点・・・基準と比較して、非常に良い。
6点・・・基準と比較して、良い
5点・・・基準と比較して、やや良い。
4点・・・基準
3点・・・基準と比較して、やや悪い。
2点・・・基準と比較して、悪い。
1点・・・基準と比較して、非常に悪い。 For each subject, the milk flavor (good milk feel, good milk taste) and ease of drinking of this control beverage were set as the reference point “4 points” in the 7-point evaluation from 1 point to 7 points below. did.
7 points: Very good compared to the standard.
6 points: Good compared to the standard 5 points: Slightly better than the standard.
4 points: Standard 3 points: Slightly worse than the standard.
2 points: Bad compared to the standard.
1 point: Very bad compared to the standard.
7点・・・基準と比較して、非常に強く感じる。
6点・・・基準と比較して、強く感じる
5点・・・基準と比較して、やや強く感じる。
4点・・・基準
3点・・・基準と比較して、やや弱く感じる。
2点・・・基準と比較して、弱く感じる。
1点・・・基準と比較して、非常に弱く感じる。 Moreover, the strength of the acidity of the beverage of this control example was set to the reference point “4 points” in the seven-step evaluation from the following 1 point to 7 points in each subject.
7 points ... I feel very strong compared to the standard.
6 points: feels stronger than the standard 5 points: feels slightly stronger than the standard
4 points-standard 3 points-feels slightly weaker than standard.
2 points ... Feels weaker than the standard.
1 point ... It feels very weak compared to the standard.
表2に記載の各成分を水中で均一に混合して飲料を調合し、得られた飲料を95℃瞬間殺菌にて殺菌し、容器に詰めた。これにより容器詰飲料を得た。
この容器詰飲料を摂取したときの乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさおよび酸味の強さについて、5人のパネリストに、上記I.で説明した対照例を4点とした7段階評価(1~7点)をしてもらった(対照例については表1参照)。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表2に示した。乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさについては、数字が大きいほど良好な結果であることを表す。酸味の強さについては、数値が小さいほど良好な結果であることを表す。 II. Preparation and Evaluation of Beverage Containing Whey Minerals and Specific Acids Beverages are prepared by uniformly mixing each component shown in Table 2 in water, and the resulting beverage is sterilized by instant sterilization at 95 ° C. Stuffed. Thereby, a packaged beverage was obtained.
Regarding the milk flavor (good milk feeling, good milk taste), ease of drinking and sourness when ingesting this packaged beverage, five panelists were given the above I.S. A 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example). Various numerical values were measured / calculated.
Table 2 shows the average values of various numerical values and the scores of five people. Regarding milk flavor (good milk feeling, good milk taste) and ease of drinking, the larger the number, the better the result. About sourness intensity, it shows that it is so favorable that a numerical value is small.
また、実施例1~4の飲料は、酸としてクエン酸またはリンゴ酸を含む飲料(比較例1および2)に比べて、乳風味(ミルク感の良さ、ミルクのコクの良さ)が良好であった。 As shown in Table 2, an embodiment comprising whey minerals and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid, and having a pH of less than 4.6. It was confirmed that the beverages 1 to 4 had a milk flavor (good milk feeling, good milk taste) similar to the control example.
In addition, the beverages of Examples 1 to 4 had better milk flavor (good milk feeling, good milk taste) than beverages containing citric acid or malic acid as acids (Comparative Examples 1 and 2). It was.
加えて、実施例1~4の飲料の飲みやすさについては、比較例の飲料と同等または比較例の飲料よりも良好だった。酸としてリン酸、酒石酸、乳酸またはグルコン酸を用いることで飲みやすさも向上する傾向にあることが読み取れる。 Furthermore, the sourness of the beverages of Examples 1 to 4 was suppressed as compared with the beverages of Comparative Examples 1 and 2. This suggests that the beverages of Examples 1 to 4 not only did not inhibit the milk flavor due to the acidity, but also improved the thirstability over citric acid.
In addition, the ease of drinking of the beverages of Examples 1 to 4 was the same as or better than the beverage of the comparative example. It can be seen that the ease of drinking tends to be improved by using phosphoric acid, tartaric acid, lactic acid or gluconic acid as the acid.
表3に記載の各成分を水中で均一に混合して飲料を調合し、得られた飲料を95℃瞬間殺菌にて殺菌し、容器に詰めた。これにより容器詰飲料を得た。
この容器詰飲料を摂取したときの乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさおよび酸味の強さについて、5人のパネリストに、上記I.で説明した対照例を4点とした7段階評価(1~7点)をしてもらった(対照例については表1参照)。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表3に示した。乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさについては、数字が大きいほど良好な結果であることを表す。酸味の強さについては、数値が小さいほど良好な結果であることを表す。 III. Evaluation in which the amount of whey mineral was changed Each component shown in Table 3 was uniformly mixed in water to prepare a beverage, and the resulting beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained.
Regarding the milk flavor (good milk feeling, good milk taste), ease of drinking and sourness when ingesting this packaged beverage, five panelists were given the above I.S. A 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example). Various numerical values were measured / calculated.
Table 3 shows the average of various numerical values and the scores of five people. Regarding milk flavor (good milk feeling, good milk taste) and ease of drinking, the larger the number, the better the result. About sourness intensity, it shows that it is so favorable that a numerical value is small.
また、乳風味と飲みやすさとの両立の点では、乳清ミネラルそれ自身の量(固形分換算)は、0.2~0.8g/L程度が好ましい(カリウム量では5.3~21.4mg/100mL程度)ことが読み取れる。 From Table 3, it can be seen that by appropriately increasing the amount of whey mineral, milk flavor (good milk feeling, good milk taste) is further improved.
From the viewpoint of compatibility between milk flavor and ease of drinking, the amount of whey mineral itself (in terms of solid content) is preferably about 0.2 to 0.8 g / L (in the amount of potassium, 5.3 to 21.). 4 mg / 100 mL).
表4に記載の各成分を水中で均一に混合して飲料を調合し、得られた飲料を95℃瞬間殺菌にて殺菌し、容器に詰めた。これにより容器詰飲料を得た。
この容器詰飲料を摂取したときの、乳風味(ミルク感の良さ)、後味の良さ、飲みやすさおよび甘さの後引きの強さについて、5人のパネリストに、実施例1(対照例ではないことに留意)を基準点の4点とした7段階評価(1~7点)をしてもらった。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表4に示した。乳風味(ミルク感の良さ)、後味の良さおよび飲みやすさについては、数字が大きいほど良好な結果であることを表す。甘さの後引きの強さについては、数値が小さいほど良好な結果である(止渇性の向上効果が高い)ことを表す。 IV. Evaluation of beverage using plant extract Each component shown in Table 4 was uniformly mixed in water to prepare a beverage, and the resulting beverage was sterilized by instant sterilization at 95 ° C and packed in a container. Thereby, a packaged beverage was obtained.
About the strength of the aftertaste, milky taste (good milk feeling), aftertaste, ease of drinking and sweetness when ingesting this packaged beverage, Example 1 (in the control example) 7 points evaluation (1 to 7 points) with 4 points as reference points. Various numerical values were measured / calculated.
Table 4 shows the average values of various numerical values and the scores of five people. For milk flavor (good milk feeling), good aftertaste and ease of drinking, the larger the number, the better the result. As for the strength of the sweetness pull-back, the smaller the value, the better the result (the effect of improving the thirst is high).
特定酸としてリン酸を用いた追加の評価を行い、各種数値と、乳風味や飲みやすさなどとの関係を確認した。 V. Additional evaluation using phosphoric acid as a specific acid Additional evaluation using phosphoric acid as a specific acid was performed, and the relationship between various numerical values and milk flavor and ease of drinking was confirmed.
この容器詰飲料を摂取したときの乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさおよび酸味の強さについて、5人のパネリストに、上記I.で説明した対照例を4点とした7段階評価(1~7点)をしてもらった(対照例については表1参照)。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表5に示した。乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさについては、数字が大きいほど良好な結果であることを表す。酸味の強さについては、数値が小さいほど良好な結果であることを表す。 Each component described in Table 5 as “Example 11” was uniformly mixed in water to prepare a beverage, and the resulting beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained.
Regarding the milk flavor (good milk feeling, good milk taste), ease of drinking and sourness when ingesting this packaged beverage, five panelists were given the above I.S. A 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example). Various numerical values were measured / calculated.
Table 5 shows the average values of various numerical values and the scores of five people. Regarding milk flavor (good milk feeling, good milk taste) and ease of drinking, the larger the number, the better the result. About sourness intensity, it shows that it is so favorable that a numerical value is small.
また、リン酸の量がかなり多いにもかかわらず、対照例に比べて乳風味(ミルク感の良さおよびミルクのコクの良さ)の低下はわずか0.2点に抑えられていた。つまり、十分な乳風味が感じられることが確認された。 From Table 5, the amount of phosphoric acid is considerably higher (compared to the amount of whey minerals), and even if the beverage has a relatively large citric acidity of about 0.03%, the ease of drinking is better than the control example. In addition, the acidity was equivalent to that of the control example.
Moreover, although the amount of phosphoric acid was considerably large, the decrease in milk flavor (good milk feeling and good milk taste) was suppressed to only 0.2 points compared to the control example. That is, it was confirmed that a sufficient milk flavor can be felt.
特定酸として乳酸を用いた追加の評価を行い、各種数値と、乳風味や飲みやすさなどとの関係を確認した。 VI. Additional evaluation using lactic acid as a specific acid Additional evaluation using lactic acid as a specific acid was performed to confirm the relationship between various numerical values and milk flavor and ease of drinking.
この容器詰飲料を摂取したときの乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさおよび酸味の強さについて、5人のパネリストに、上記I.で説明した対照例を4点とした7段階評価(1~7点)をしてもらった(対照例については表1参照)。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表6に示した。乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさについては、数字が大きいほど良好な結果であることを表す。酸味の強さについては、数値が小さいほど良好な結果であることを表す。 Ingredients described as Examples 12 to 15 in Table 6 were uniformly mixed in water to prepare a beverage. The obtained beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained.
Regarding the milk flavor (good milk feeling, good milk taste), ease of drinking and sourness when ingesting this packaged beverage, five panelists were given the above I.S. A 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example). Various numerical values were measured / calculated.
Table 6 shows the average values of various numerical values and the scores of five people. Regarding milk flavor (good milk feeling, good milk taste) and ease of drinking, the larger the number, the better the result. About sourness intensity, it shows that it is so favorable that a numerical value is small.
結果をより詳細に分析すると、乳清ミネラルの含有量/特定酸の含有量がある程度大きいほうが、乳風味を高められる傾向にある。 According to Table 6, when lactic acid is used as the specific acid, at least in the wide range of whey mineral amount (solid content) of 0.05 to 0.8 g / L, milk flavor (good milk feeling and milk richness) It can be seen that the goodness of the milk is comparable to that of the control example or the milk flavor is better than that of the control example.
When the results are analyzed in more detail, the milk flavor tends to be enhanced when the whey mineral content / specific acid content is somewhat large.
特定酸としてグルコン酸を用いた追加の評価を行い、各種数値と、乳風味や飲みやすさなどとの関係を確認した。 VII. Additional evaluation using gluconic acid as a specific acid Additional evaluation using gluconic acid as a specific acid was performed, and the relationship between various numerical values and milk flavor and ease of drinking was confirmed.
この容器詰飲料を摂取したときの乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさおよび酸味の強さについて、5人のパネリストに、上記I.で説明した対照例を4点とした7段階評価(1~7点)をしてもらった(対照例については表1参照)。また、各種数値を測定/算出した。
各種数値および5人の評点の平均値を表7に示した。乳風味(ミルク感の良さ、ミルクのコクの良さ)、飲みやすさについては、数字が大きいほど良好な結果であることを表す。酸味の強さについては、数値が小さいほど良好な結果であることを表す。 Ingredients described as Examples 16 to 18 in Table 7 were uniformly mixed in water to prepare a beverage. The obtained beverage was sterilized by instant sterilization at 95 ° C. and packed in a container. Thereby, a packaged beverage was obtained.
Regarding the milk flavor (good milk feeling, good milk taste), ease of drinking and sourness when ingesting this packaged beverage, five panelists were given the above I.S. A 7-point evaluation (1 to 7 points) was performed with the control example described in 4 as 4 points (see Table 1 for the control example). Various numerical values were measured / calculated.
Table 7 shows the average values of various numerical values and the scores of five people. Regarding milk flavor (good milk feeling, good milk taste) and ease of drinking, the larger the number, the better the result. About sourness intensity, it shows that it is so favorable that a numerical value is small.
Claims (11)
- 乳清ミネラルと、
リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸とを含み、
pHが4.6未満である飲料。 Whey minerals,
Including one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid,
A beverage having a pH of less than 4.6. - 請求項1に記載の飲料であって、
前記酸としてグルコン酸を含む飲料。 The beverage according to claim 1,
A beverage containing gluconic acid as the acid. - 請求項1または2に記載の飲料であって、
カリウム濃度が1.5mg/100mL以上である飲料。 The beverage according to claim 1 or 2,
A beverage having a potassium concentration of 1.5 mg / 100 mL or more. - 請求項1~3のいずれか1項に記載の飲料であって、
さらに、植物エキスを含む飲料。 The beverage according to any one of claims 1 to 3,
Furthermore, beverages containing plant extracts. - 請求項1~4のいずれか1項に記載の飲料であって、
クエン酸酸度が0.04%以下である飲料。 The beverage according to any one of claims 1 to 4,
A beverage having a citric acidity of 0.04% or less. - 請求項1~5のいずれか1項に記載の飲料であって、
クエン酸の濃度が0~15mg/100mLである飲料。 The beverage according to any one of claims 1 to 5,
A beverage having a citric acid concentration of 0 to 15 mg / 100 mL. - 請求項1~6のいずれか1項に記載の飲料であって、
飲料中の前記酸の含有量に対する、飲料中の前記乳清ミネラルの含有量の質量比が、0.5~10である飲料。 The beverage according to any one of claims 1 to 6,
A beverage in which the mass ratio of the whey mineral content in the beverage to the acid content in the beverage is 0.5 to 10. - 請求項1~7のいずれか1項に記載の飲料であって、
乳風味飲料である飲料。 The beverage according to any one of claims 1 to 7,
A beverage that is a milk flavored beverage. - 請求項1~8のいずれか1項に記載の飲料であって、
波長650nmにおける吸光度が0.06以下である飲料。 The beverage according to any one of claims 1 to 8,
A beverage having an absorbance at a wavelength of 650 nm of 0.06 or less. - 飲料に、少なくとも、乳清ミネラルと、リン酸、酒石酸、乳酸及びグルコン酸からなる群より選択される1種又は2種以上の酸とを添加して飲料を得る、飲料への乳風味付与方法。 A method for imparting a milk flavor to a beverage, wherein the beverage is obtained by adding at least one whey mineral and one or more acids selected from the group consisting of phosphoric acid, tartaric acid, lactic acid and gluconic acid to the beverage. .
- 請求項10に記載の飲料への乳風味付与方法であって、
飲料のpHを4.6未満とする、飲料への乳風味付与方法。 A method for imparting milk flavor to a beverage according to claim 10,
A method for imparting milk flavor to a beverage, wherein the pH of the beverage is less than 4.6.
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