WO2016201706A1 - Plant molecular purification technique integration system - Google Patents
Plant molecular purification technique integration system Download PDFInfo
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- WO2016201706A1 WO2016201706A1 PCT/CN2015/081985 CN2015081985W WO2016201706A1 WO 2016201706 A1 WO2016201706 A1 WO 2016201706A1 CN 2015081985 W CN2015081985 W CN 2015081985W WO 2016201706 A1 WO2016201706 A1 WO 2016201706A1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/18—Extraction of water soluble tea constituents
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- the invention relates to a plant extract producing device, and more particularly to a plant molecular purification technology integrated system.
- the separation and extraction technology of plant active ingredients is a strategic high-tech. An important direction is the development and production of high-efficiency separation and purification technology, separation of active ingredients from natural plants, formation of new products with high added value, and improvement. Resource utilization.
- the active ingredients contained in plants are the material basis for determining plant characteristics. Plants use solar energy as an energy source to form a variety of active ingredients through a series of life activities, which determine the morphological characteristics and utilization value of plants. The coordination and unification of the active ingredients in plants determines the quality of the plants and the value of drinking. In the final analysis, the active ingredients of plants are substances that determine the various characteristics of plants.
- the existing technical methods for extracting active ingredients of plants include: (1) hot water extraction, high temperature water as a solvent, destroying the active ingredients of the plants, and reducing the quality of the extract. (2) Chemical solvent extraction, the chemical substance remains in the extract, which reduces the quality of the extract. (3) Countercurrent extraction, extraction with water at a temperature of 80-90 degrees, the composition is destroyed, for example, under high temperature for a long time, the oxidation loss rate of the active ingredient will increase, affecting the quality of the extract. (4) Microwave extraction, with residual chemical solvents, high temperature destroys the active ingredients, and reduces the quality of the extract. (5) Supercritical extraction, low extraction efficiency, and mainly used to extract plant essential oils.
- the present invention firstly provides an integrated system for plant molecular purification technology, which comprises a material pulverizing module, a high pressure fluid extraction module and a centrifugal module which are sequentially connected; and a primary separation module, a stage separation module and a three-stage membrane separation module, wherein the centrifugal module is simultaneously connected to the first-stage separation module, the second-stage separation module and the third-stage separation module, and the first-stage separation module, the second-stage separation module and the third-stage separation module are mutually connected
- the primary separation module is connected to the primary purification module and the primary recombination module
- the secondary separation module is connected to the secondary purification module and the secondary recombination module
- the tertiary separation module is connected with three a level purification module and a three-stage recombination module, wherein the first-level reorganization module, the two-group reorganization module, and the third-level reorganization module are simultaneously
- the primary separation module comprises a ceramic membrane having a membrane pore size of 0.8-1.2 ⁇ m.
- the secondary separation module comprises a ceramic membrane having a membrane pore size of 0.1-0.5 ⁇ m.
- the three-stage separation module includes a ceramic membrane having a membrane pore diameter of 4 to 50 nm.
- the material pulverizing module comprises a high-speed tissue masher for splitting the material and a universal pulverizer for pulverizing the material to 50-80 mesh.
- the high-pressure fluid extraction module includes an extraction tank equipped with a high-speed agitator connected to a pressure pump, and the pressurized pump pressurizes purified water as a solvent and delivers it to the extraction tank.
- the pressure is set to 25 MPa to 75 MPa.
- the centrifugal module includes a centrifuge having a rotational speed of 3800 or more.
- the purification module includes an organic nanofiltration membrane.
- the recombination module comprises a concentrator and a vacuum dryer, and the filtrate after the nanofiltration purification is first concentrated and then dried and recrystallized.
- the quantitative compounding module comprises a feeding device and a stirring device.
- the integrated system of the invention can realize pipeline, intelligent and reduce labor.
- the integrated system of the present invention has a reasonable structure setting, and the production time is reduced by the cooperation of the respective modules.
- the active components of the plant can be completely separated and extracted, and the molecular foods of different tastes can be assembled.
- FIG. 1 is a schematic diagram of an integrated system for plant molecular purification technology of the present invention.
- the method of use of the device of the present invention is as follows:
- the plant is first placed in a material pulverizing module, and is broken into a powder of 50-80 mesh by a material pulverizing module, and then input into a high-pressure fluid extraction module through a conveyor belt, and the extract is conveyed to a centrifugal module through a pipe through a pipe, and solidified by a centrifuge.
- the liquid is layered, the liquid layer is taken, and three different separation modules are selected according to the requirements.
- the module After separation, the module is subjected to nanofiltration purification to remove heavy metals and pesticide residues, and then the reconstituted module is used to obtain the concentrated powder obtained by different membrane pore size filtration, according to the seeking
- the different concentrated powders are added to the feeding device in a certain proportion, and the molecular components of the plant active ingredient are obtained by the mixing device of the quantitative assembling module, mixing and blending, and finally packaging.
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Abstract
Disclosed is an integration device for the extraction and purification of plant molecules, comprising: a material pulverizing module, a high pressure fluid extraction module and a centrifugation module, which are connected in sequence, and also comprising a first stage membrane separation and purification module, a second stage membrane separation and purification module and a third stage membrane separation and purification module. The centrifugation module simultaneously connects to the first stage membrane separation and purification module, the second stage membrane separation and purification module and the third stage membrane separation and purification module, and simultaneously connects to a quantitative blending module. By integrating production devices for the extraction and purification of plant molecules and through the coordination of each module, plant monomer components or combined components of various grades can be quantitatively blended.
Description
本发明涉及一种植物提取物的生产装置，更具体地，涉及一种植物分子纯化技术集成系统。The invention relates to a plant extract producing device, and more particularly to a plant molecular purification technology integrated system.
植物有效成分的分离提取技术是战略性的高新技术，一个重要方向是通过高效分离纯化技术集成及装备的开发与生产，从天然植物中分离有效成分，形成高附加值的新产品，并可提高资源利用率。The separation and extraction technology of plant active ingredients is a strategic high-tech. An important direction is the development and production of high-efficiency separation and purification technology, separation of active ingredients from natural plants, formation of new products with high added value, and improvement. Resource utilization.
植物中所含的有效成分，是决定植物特性的物质基础。植物以太阳能为能源，通过一系列的生命活动过程形成各种各样的有效成分，决定了植物形形色色的形态特征及利用价值。植物中有效成分的协调统一，确定了植物品质优劣及饮用价值。归根结底，植物的有效成分是决定植物各种特征的物质。The active ingredients contained in plants are the material basis for determining plant characteristics. Plants use solar energy as an energy source to form a variety of active ingredients through a series of life activities, which determine the morphological characteristics and utilization value of plants. The coordination and unification of the active ingredients in plants determines the quality of the plants and the value of drinking. In the final analysis, the active ingredients of plants are substances that determine the various characteristics of plants.
国内外科学研究证明，植物有效成分功能显著，更比人工合成健康有益。植物有效成分的功能包括：清除人体自由基和提高免疫力、抗氧化、抗衰老、抗辐射、抗癌和降血脂等等功能。因此，植物的功能性成分已被广泛的应用于医药、保健和食品等领域，且具有巨大的潜在市场。综合开发植物的功能性成分，是促进人类健康和解决我国中低档植物出路的有效途径。Scientific research at home and abroad has proved that the active ingredients of plants are significant and more beneficial than synthetic health. The functions of plant active ingredients include: removing free radicals from the body and improving immunity, anti-oxidation, anti-aging, anti-radiation, anti-cancer and blood fat reduction. Therefore, the functional components of plants have been widely used in the fields of medicine, health care and food, and have a huge potential market. Comprehensive development of functional components of plants is an effective way to promote human health and solve the path of low- and medium-grade plants in China.
现有提取植物有效成分的技术方式有：(1)热水浸提，高温水作为溶剂，破坏了植物的有效成分，使提取物的品质降低。(2)化学溶剂提取，提取物中有化学物质的残留，降低了提取物的品质。(3)逆流提取，用温度在80-90度的水提取，成分被破坏，例如高温长时间条件下，有效成分的氧化损失率将增加，影响了提取物的品质。(4)微波提取，有化学溶剂的残留，还有高温破坏了有效成分，降低了提取物的品质。(5)超临界提取，提取效率低，并主要用于提取植物精油。(6)冷冻干燥，效果良好，但成本太高，而且只是其中的一部分低温，不能保证整个提取过程的有效成分损失。(7)喷雾干燥，150度以上，高温破坏成分完整，影响产品的品质。The existing technical methods for extracting active ingredients of plants include: (1) hot water extraction, high temperature water as a solvent, destroying the active ingredients of the plants, and reducing the quality of the extract. (2) Chemical solvent extraction, the chemical substance remains in the extract, which reduces the quality of the extract. (3) Countercurrent extraction, extraction with water at a temperature of 80-90 degrees, the composition is destroyed, for example, under high temperature for a long time, the oxidation loss rate of the active ingredient will increase, affecting the quality of the extract. (4) Microwave extraction, with residual chemical solvents, high temperature destroys the active ingredients, and reduces the quality of the extract. (5) Supercritical extraction, low extraction efficiency, and mainly used to extract plant essential oils. (6) Freeze-drying, the effect is good, but the cost is too high, and only a part of the low temperature, can not guarantee the loss of the active ingredient of the whole extraction process. (7) Spray drying, 150 degrees or more, high temperature damage components are intact, affecting the quality of the product.
目前并没有一套能够完整的将植物中的有效成分进行分离提取纯化的装置。At present, there is no complete device for separating and purifying the active ingredients in plants.
发明内容Summary of the invention
为了能够一步获得植物中有效成分，本发明首先提供一种植物分子纯化技术集成系统，其特征在于，包括依次连接的物料粉碎模块、高压流体提取模块和离心模块；还包括一级分离模块、二级分离模块和三级膜分离模块，所述的离心模块同时连接一级分离模块、二级分离模块和三级分离模块，且一级分离模块、二级分离模块和三级分离模块之间相互连接；所述的一级分离模块连接一级纯化模块和一级重组模块，所述的二级分离模块连接二级纯化模块和二级重组模块，所述的三级分离模块之后都连接有三级纯化模块和三级重组模块，所述的一级重组模块、二组重组模块和三级重组模块同时连接定量拼配模块，In order to obtain the active ingredient in the plant in one step, the present invention firstly provides an integrated system for plant molecular purification technology, which comprises a material pulverizing module, a high pressure fluid extraction module and a centrifugal module which are sequentially connected; and a primary separation module, a stage separation module and a three-stage membrane separation module, wherein the centrifugal module is simultaneously connected to the first-stage separation module, the second-stage separation module and the third-stage separation module, and the first-stage separation module, the second-stage separation module and the third-stage separation module are mutually connected The primary separation module is connected to the primary purification module and the primary recombination module, and the secondary separation module is connected to the secondary purification module and the secondary recombination module, and the tertiary separation module is connected with three a level purification module and a three-stage recombination module, wherein the first-level reorganization module, the two-group reorganization module, and the third-level reorganization module are simultaneously connected to the quantitative assembly module.
所述的一级分离模块包括膜孔径为0.8-1.2μm的陶瓷膜，The primary separation module comprises a ceramic membrane having a membrane pore size of 0.8-1.2 μm.
所述的二级分离模块包括膜孔径为0.1-0.5μm的陶瓷膜，The secondary separation module comprises a ceramic membrane having a membrane pore size of 0.1-0.5 μm.
所述的三级分离模块包括膜孔径为4-50nm的陶瓷膜。The three-stage separation module includes a ceramic membrane having a membrane pore diameter of 4 to 50 nm.
所述的物料粉碎模块包括用于将物料劈裂的高速组织捣碎机和用于将物料粉碎至50～80目的万能粉碎机。The material pulverizing module comprises a high-speed tissue masher for splitting the material and a universal pulverizer for pulverizing the material to 50-80 mesh.
所述高压流体提取模块包括配备高速搅拌器的提取罐，连接有加压泵，加压泵将纯净水作为溶剂加压后输送到提取罐。压力设置为25MPa－75MPa。
The high-pressure fluid extraction module includes an extraction tank equipped with a high-speed agitator connected to a pressure pump, and the pressurized pump pressurizes purified water as a solvent and delivers it to the extraction tank. The pressure is set to 25 MPa to 75 MPa.
所述的离心模块包括一台转速为3800以上的离心机。The centrifugal module includes a centrifuge having a rotational speed of 3800 or more.
所述的纯化模块包括有机纳滤膜。The purification module includes an organic nanofiltration membrane.
所述的重组模块包括浓缩器和真空干燥机，将经过纳滤纯化之后的滤液先进行浓缩再进行干燥重组结晶。The recombination module comprises a concentrator and a vacuum dryer, and the filtrate after the nanofiltration purification is first concentrated and then dried and recrystallized.
所述的定量拼配模块，包括加料装置和搅拌装置。The quantitative compounding module comprises a feeding device and a stirring device.
本发明具有以下优点：The invention has the following advantages:
1.本发明的集成系统可以实现管道化，智能化，减少了人工。1. The integrated system of the invention can realize pipeline, intelligent and reduce labor.
2.本发明的集成系统的结构设置合理，通过各个模块的配合，减少生产时间。2. The integrated system of the present invention has a reasonable structure setting, and the production time is reduced by the cooperation of the respective modules.
3.通过本发明的集成系统可以完整地分离提取植物有效成分，并拼配出不同口味的分子食品。3. Through the integrated system of the invention, the active components of the plant can be completely separated and extracted, and the molecular foods of different tastes can be assembled.
图1为本发明的植物分子纯化技术集成系统示意图。1 is a schematic diagram of an integrated system for plant molecular purification technology of the present invention.
下面结合附图和具体实施例进一步详细说明本发明。除非特别说明，本发明采用的试剂、设备和方法为本技术领域常规市购的试剂、设备和常规使用的方法。The invention will be further described in detail below with reference to the drawings and specific embodiments. Unless otherwise stated, the reagents, devices, and methods employed in the present invention are conventionally commercially available reagents, equipment, and methods of routine use.
本发明的装置的使用方法如下：The method of use of the device of the present invention is as follows:
先将植物放入物料粉碎模块，通过物料粉碎模块破碎成50～80目的粉末，然后通过输送带输入到高压流体提取模块，通过提取，将提取液通过管道输送到离心模块，通过离心机将固液分层，取液层，并根据需求选择三种不同的分离模块，通过分离模块之后进行纳滤纯化，去除重金属及农药残留，然后通过重组模块得到不同膜孔径过滤所得的浓缩粉，根据寻求，将不同的浓缩粉按一定的比例加入到加料装置中，通过定量拼配模块的搅拌装置，混合拼配，最后包装，即得一种植物有效成分分子食品。
The plant is first placed in a material pulverizing module, and is broken into a powder of 50-80 mesh by a material pulverizing module, and then input into a high-pressure fluid extraction module through a conveyor belt, and the extract is conveyed to a centrifugal module through a pipe through a pipe, and solidified by a centrifuge. The liquid is layered, the liquid layer is taken, and three different separation modules are selected according to the requirements. After separation, the module is subjected to nanofiltration purification to remove heavy metals and pesticide residues, and then the reconstituted module is used to obtain the concentrated powder obtained by different membrane pore size filtration, according to the seeking The different concentrated powders are added to the feeding device in a certain proportion, and the molecular components of the plant active ingredient are obtained by the mixing device of the quantitative assembling module, mixing and blending, and finally packaging.
Claims (8)
- 一种植物分子纯化技术集成系统，其特征在于，包括依次连接的物料粉碎模块、高压流体提取模块和离心模块；还包括一级分离模块、二级分离模块和三级膜分离模块，所述的离心模块同时连接一级分离模块、二级分离模块和三级分离模块，且一级分离模块、二级分离模块和三级分离模块之间相互连接；所述的一级分离模块连接一级纯化模块和一级重组模块，所述的二级分离模块连接二级纯化模块和二级重组模块，所述的三级分离模块之后都连接有三级纯化模块和三级重组模块，所述的一级重组模块、二组重组模块和三级重组模块同时连接定量拼配模块，An integrated system for plant molecular purification technology, comprising: a material pulverizing module, a high pressure fluid extraction module and a centrifugal module connected in sequence; and a primary separation module, a secondary separation module and a tertiary membrane separation module, wherein The centrifugal module is simultaneously connected to the first-stage separation module, the second-stage separation module and the third-stage separation module, and the first-stage separation module, the second-stage separation module and the third-stage separation module are connected to each other; the first-stage separation module is connected to the first-stage purification module. The module and the primary recombination module, the secondary separation module is connected to the secondary purification module and the secondary recombination module, and the third-stage separation module is connected with a three-stage purification module and a third-level recombination module, the one The level reorganization module, the second group reorganization module and the third level reorganization module are simultaneously connected to the quantitative assembly module.所述的一级分离模块包括膜孔径为0.8-1.2μm的陶瓷膜，The primary separation module comprises a ceramic membrane having a membrane pore size of 0.8-1.2 μm.所述的二级分离模块包括膜孔径为0.1-0.5μm的陶瓷膜，The secondary separation module comprises a ceramic membrane having a membrane pore size of 0.1-0.5 μm.所述的三级分离模块包括膜孔径为4-50nm的陶瓷膜。The three-stage separation module includes a ceramic membrane having a membrane pore diameter of 4 to 50 nm.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述的物料粉碎模块包括用于将物料劈裂的高速组织捣碎机和用于将物料粉碎至50～80目的万能粉碎机。The plant molecular purification technology integrated system according to claim 1, wherein the material pulverizing module comprises a high-speed tissue masher for splitting the material and pulverizing the material to 50-80 mesh. machine.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述高压流体提取模块包括配备高速搅拌器的提取罐，连接有加压泵，加压泵将纯净水作为溶剂加压后输送到提取罐。压力设置为25MPa－75MPa。The plant molecular purification technology integration system according to claim 1, wherein the high pressure fluid extraction module comprises an extraction tank equipped with a high speed agitator, and a pressure pump is connected, and the pressure pump pressurizes pure water as a solvent. Transfer to the extraction tank. The pressure is set to 25 MPa to 75 MPa.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述的离心模块包括一台转速为3800以上的离心机。The plant molecular purification technology integrated system according to claim 1, wherein the centrifugal module comprises a centrifuge having a rotational speed of 3800 or more.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述的纯化模块包括有机纳滤膜。The plant molecular purification technology integrated system according to claim 1, wherein the purification module comprises an organic nanofiltration membrane.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述的重组模块包括浓缩器和真空干燥机，将经过纳滤纯化之后的滤液先进行浓缩再进行干燥重组结晶。The plant molecular purification technology integrated system according to claim 1, wherein the recombination module comprises a concentrator and a vacuum dryer, and the filtrate after the nanofiltration purification is first concentrated and then dried and recrystallized.
- 根据权利要求1所述的植物分子纯化技术集成系统，其特征在于，所述的定量拼配模块，包括加料装置和搅拌装置。The plant molecular purification technology integration system according to claim 1, wherein the quantitative compounding module comprises a feeding device and a stirring device.
- 根据权利要求1所述的植物分子纯化技术集成系统的使用方法，其特征在于，先将植物放入物料粉碎模块，通过物料粉碎模块破碎成50～80目的粉末，然后通过输送带输入到高压流体提取模块，通过提取，将提取液通过管道输送到离心模块，通过离心机将固液分层，取液层，并根据需求选择三种不同的分离模块，通过分离模块之后进行纳滤纯化，去除重金属及农药残留，然后通过重组模块得到不同膜孔径过滤所得的浓缩粉，根据寻求，将不同的浓缩粉按一定的比例加入到加料装置中，通过定量拼配模块的搅拌装置，混合拼配，最后包装，即得一种植物有效成分分子食品。 The method for using a plant molecular purification technology integrated system according to claim 1, wherein the plant is first placed in a material pulverizing module, and is broken into a powder of 50 to 80 mesh by a material pulverizing module, and then input to a high pressure fluid through a conveyor belt. The extraction module, through extraction, transports the extract to the centrifugal module through a pipeline, stratifies the solid liquid through a centrifuge, takes a liquid layer, and selects three different separation modules according to requirements, and performs nanofiltration purification after separation of the module. Heavy metals and pesticide residues, and then obtained the concentrated powder obtained by different membrane pore size filtration through the recombination module. According to the quest, different concentrated powders are added to the feeding device in a certain proportion, and the mixing device is mixed and assembled by the quantitative assembling module. Finally packaging, that is, a plant active ingredient molecular food.
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| CN111729637A (en) * | 2020-07-24 | 2020-10-02 | 上海汇像信息技术有限公司 | Vacuum dosing system and vacuum dosing method |
| CN116943840A (en) * | 2023-08-07 | 2023-10-27 | 广州绿徽新材料研究院有限公司 | Device for high-speed three-vortex-microwave composite super-nano grinding of plant fiber powder by pressure change cavitation |
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| CN116943840A (en) * | 2023-08-07 | 2023-10-27 | 广州绿徽新材料研究院有限公司 | Device for high-speed three-vortex-microwave composite super-nano grinding of plant fiber powder by pressure change cavitation |
| CN116943840B (en) * | 2023-08-07 | 2024-04-09 | 广州绿徽新材料研究院有限公司 | Device for high-speed three-vortex-microwave composite super-nano grinding of plant fiber powder by pressure change cavitation |
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