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WO2011142553A2 - Method for analyzing internal density of material by using x-ray computed tomography - Google Patents

Method for analyzing internal density of material by using x-ray computed tomography Download PDF

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Publication number
WO2011142553A2
WO2011142553A2 PCT/KR2011/003370 KR2011003370W WO2011142553A2 WO 2011142553 A2 WO2011142553 A2 WO 2011142553A2 KR 2011003370 W KR2011003370 W KR 2011003370W WO 2011142553 A2 WO2011142553 A2 WO 2011142553A2
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ray
density
analyzed
specimens
standard
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PCT/KR2011/003370
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French (fr)
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WO2011142553A9 (en
WO2011142553A3 (en
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Jae Yeol Lee
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Agency For Defense Development
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Priority to JP2013510017A priority Critical patent/JP5508598B2/en
Priority to US13/697,220 priority patent/US9025724B2/en
Publication of WO2011142553A2 publication Critical patent/WO2011142553A2/en
Publication of WO2011142553A3 publication Critical patent/WO2011142553A3/en
Publication of WO2011142553A9 publication Critical patent/WO2011142553A9/en

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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
    • G01N9/24—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by observing the transmission of wave or particle radiation through the material
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
    • G01N23/04—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material
    • G01N23/046—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material using tomography, e.g. computed tomography [CT]
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00—Investigating materials by wave or particle radiation
    • G01N2223/40—Imaging
    • G01N2223/419—Imaging computed tomograph

Definitions

  • the present invention relates to a method for analyzing internal density of material by using x-ray computed tomography, and more specifically, to a method for analyzing internal density of material by using x-ray computed tomography by which inside of material can be analyzed quantitatively by using an x-ray tomography image.
  • the intensity of x-ray which has transmitted a material is detected by radiating x-ray to the material placed between an x-ray generator and an x-ray detector.
  • x-ray tomography computed tomography By reconstructing, through a computer, the intensities of the x-rays which have been shot while rotating the material, a distribution of x-ray absorption inside the material cross-section can be obtained, which is called x-ray tomography computed tomography.
  • the x-ray tomography is a typical non-destructive method of analyzing material, the absorption coefficient of the x-ray being known as a function of density of the material.
  • An x-ray tomography image is a result obtained by converting the difference among absorption coefficients to a shaded image, which can be decoded by trained staffs.
  • the method resorts to a qualitative decision through a naked eye, which can include errors due to the experience and subjective feeling of a person and has limitation in its reproducibility.
  • US Patent No. 5,774,520 provides method of obtaining clear x-ray tomography image by using a single gamma ray excluding scattering, but just show the density difference as the difference between absorption coefficients failing to provide actual quantitative density distribution.
  • the present invention has been designed to solve the above mentioned problems and aims to provide a method for analyzing internal density of material by using x-ray computed tomography by which inside of material can be analyzed quantitatively by using an x-ray tomography image.
  • the method for analyzing internal density of material by using X-ray computed tomography comprises the steps of: a) installing a cylinder-shaped jig between an x-ray generator and an x-ray detector, b) inserting a material to be analyzed and a plurality of standard specimens whose densities are known into the inside of the cylinder-shaped jig, c) performing X-ray computed tomography while rotating the cylinder-shaped jig through 360°, and d) calculating the internal density of distribution of the material to be analyzed by using the X-ray intensities shown in the x-ray tomography image.
  • the number of standard specimens in step b) is preferably 3-20.
  • the standard specimens preferably have homogeneous internal density.
  • the standard specimens preferably have all different internal densities.
  • the standard specimens comprise specimens with density higher than the material to be analyzed and specimens with density lower than the material to be analyzed.
  • step d) the calculation of internal density distribution of the material to be analyzed is performed based on the density of the standard specimens and the X-ray intensity in the region of standard specimens present at the X-ray tomography image by using the following formula:
  • X is an X-ray intensity at one region inside the material to be analyzed
  • D(X) is the density at the region
  • Di is the density of each standard specimen
  • Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen
  • DM is the average of all the Di
  • AM is the average of all Ai
  • N is the number of standard specimens.
  • X-ray tomography image is converted to the image showing the internal density distribution of the material, improving the qualitative decision by naked eye by providing quantitative decision method.
  • Fig. 1 shows the process of performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
  • Fig. 2 shows the construction of the apparatus for use in performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
  • Fig. 3 shows the X-ray tomography image obtained by the method of the present invention of analyzing the internal density of material by using X-ray tomography.
  • Fig. 4 shows the result of quantitative analysis of the internal density of material obtained by the method of the present invention of analyzing the internal density of material by using X-ray tomography.
  • Fig. 1 shows the process of performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
  • a cylinder-shaped jig 30 is installed between an X-ray generator 10 and an X-ray detector 11, as shown in Fig. 2 (step S101).
  • the jig 30 has the structure into which the material 20 to be analyzed and standard specimens 21, 22, 23 can be inserted, and the outer surface of the jig 30 has preferably cylinder shape without edge since the presence of edge can generate unnecessary noise to the X-ray tomography image due to refraction and diffraction from the edge.
  • step S102 After installing the jig 30, the material 20 to be analyzed and a plurality of standard specimens 21, 22, 23, whose densities are known are inserted into the inside of the cylinder-shaped jig 30 (step S102).
  • X-ray computed tomography is performed while rotating the cylinder-shaped jig 30 through 360° by rotating the turn table 12 supporting the jig 30(step S103).
  • the internal density of distribution of the material 20 to be analyzed is calculated by using the X-ray intensities shown in the x-ray tomography image as shown in Fig. 3(step S104).
  • the number of standard specimens 21, 22, 23 in step S102 is preferably 3-20.
  • the standard specimens 21, 22, 23 preferably have homogeneous internal density.
  • the standard specimens 21, 22, 23 preferably have all different internal densities.
  • the standard specimens 21, 22, 23 comprise specimens with density higher than the material 20 to be analyzed and specimens with density lower than the material to be analyzed.
  • step S104 the calculation of internal density distribution of the material 20 to be analyzed is performed based on the density of the standard specimens 21, 22, 23 and the X-ray intensity in the region of standard specimens present at the X-ray tomography image by using the following mathematical formula:
  • X is an X-ray intensity at one region inside the material to be analyzed
  • D(X) is the density at the region
  • Di is the density of each standard specimen
  • Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen
  • DM is the average of all the Di
  • AM is the average of all Ai
  • N is the number of standard specimens.
  • the X-ray 40 generated by the X-ray generator 10 passes through the jig 30 containing the material to be analyzed 20 and the standard specimens 21, 22, 23, and reaches the X-ray detector 11. At this stage, the X-ray absorption coefficients depend on the density of the region through which the X-ray 40 passes, and these differences in transmission intensities are recorded on the X-ray detector 11.
  • the jig 30, the material 20 to be analyzed and the standard specimens 21, 22, 23 rotate through 360° as the turn table 12 is rotated. As the turn table 12 rotates a certain amount of angle, X-ray is radiated again, so that the differences in the intensity of the X-ray resulting from the difference in absorption coefficients are recorded.
  • Fig. 3 shows the X-ray tomography image of internal cross section of the material obtained by reconstructing the X-ray intensities of the images.
  • the image of the material to be analyzed 20 At the center of the jig 30 is the image of the material to be analyzed 20, and on the periphery is the image of the standard specimens 21, 22, 23.
  • the standard specimens 21, 22, 23 are provided as a reference for analyzing the density of the material to be analyzed 20, and are not limited to specific materials. In other words, any material including metal, ceramics or plastic can be used, but a single material with homogeneous internal density is preferable. The reason is that the change in the density of the standard specimens 21, 22, 23, which is a basis for the analysis, result in the change in the analysis result of the material to be analyzed 20.
  • each standard specimen 21, 22, 23 should be different, and preferably comprises specimens with density higher than the material 20 to be analyzed and specimens with density lower than the material to be analyzed. The reason is that the reliability in the correlation between the X-ray intensity and density becomes higher as the density of the material 20 to be analyzed is within the density distribution of the standard specimens 21, 22, 23.
  • the number of standard specimens 21, 22, 23 is variable, but preferably is 3-20. When the number of the standard specimens is less than 3, it is too small for the reference of exact density, and when the number of the standard specimens is more than 20, the time for analysis becomes longer with little increase in accuracy.
  • the internal density of the material 20 to be analyzed can be calculated quantitatively by using the above mathematical formula, where Di is the density of standard specimens 21, 22, 23, and Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen.
  • Fig. 4 shows the result of quantitative analysis of the internal density D(X) of material obtained by applying the above formula to every region inside the material 20 to be analyzed.
  • the internal density of the material 20 to be analyzed is in the range of 5.3-1.8g/cm2.
  • the region represented by red color is normal region 50 inside the material with high density, and the region represented by blue color is defective region 51 with low density, which results from the crack of the material or generation of air bubbles.
  • X-ray tomography image is converted to the image showing the internal density distribution of the material, improving the qualitative decision by naked eye by providing quantitative decision method.

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Abstract

Disclosed is a method for analyzing internal density of material by using X-ray computed tomography, comprising the steps of installing a cylinder-shaped jig between an x-ray generator and an x-ray detector, inserting a material to be analyzed and a plurality of standard specimens whose densities are known into the inside of the cylinder-shaped jig, performing X-ray computed tomography while rotating the cylinder-shaped jig through 360°, and calculating the internal density of distribution of the material to be analyzed by using the X-ray intensities shown in the x-ray tomography image. By using the method of the present invention, X-ray tomography image is converted to the image showing the internal density distribution of the material, improving the qualitative decision by naked eye by providing quantitative decision method.

Description

METHOD FOR ANALYZING INTERNAL DENSITY OF MATERIAL BY USING X-RAY COMPUTED TOMOGRAPHY
The present invention relates to a method for analyzing internal density of material by using x-ray computed tomography, and more specifically, to a method for analyzing internal density of material by using x-ray computed tomography by which inside of material can be analyzed quantitatively by using an x-ray tomography image.
The intensity of x-ray which has transmitted a material is detected by radiating x-ray to the material placed between an x-ray generator and an x-ray detector. By reconstructing, through a computer, the intensities of the x-rays which have been shot while rotating the material, a distribution of x-ray absorption inside the material cross-section can be obtained, which is called x-ray tomography computed tomography.
The x-ray tomography is a typical non-destructive method of analyzing material, the absorption coefficient of the x-ray being known as a function of density of the material. An x-ray tomography image is a result obtained by converting the difference among absorption coefficients to a shaded image, which can be decoded by trained staffs. The method, however, resorts to a qualitative decision through a naked eye, which can include errors due to the experience and subjective feeling of a person and has limitation in its reproducibility.
US Patent No. 5,774,520 provides method of obtaining clear x-ray tomography image by using a single gamma ray excluding scattering, but just show the density difference as the difference between absorption coefficients failing to provide actual quantitative density distribution.
The present invention has been designed to solve the above mentioned problems and aims to provide a method for analyzing internal density of material by using x-ray computed tomography by which inside of material can be analyzed quantitatively by using an x-ray tomography image.
In order to obtain the object of the present invention, the method for analyzing internal density of material by using X-ray computed tomography comprises the steps of: a) installing a cylinder-shaped jig between an x-ray generator and an x-ray detector, b) inserting a material to be analyzed and a plurality of standard specimens whose densities are known into the inside of the cylinder-shaped jig, c) performing X-ray computed tomography while rotating the cylinder-shaped jig through 360°, and d) calculating the internal density of distribution of the material to be analyzed by using the X-ray intensities shown in the x-ray tomography image.
The number of standard specimens in step b) is preferably 3-20.
Also the standard specimens preferably have homogeneous internal density.
Also the standard specimens preferably have all different internal densities.
Also preferably, the standard specimens comprise specimens with density higher than the material to be analyzed and specimens with density lower than the material to be analyzed.
In the step d), the calculation of internal density distribution of the material to be analyzed is performed based on the density of the standard specimens and the X-ray intensity in the region of standard specimens present at the X-ray tomography image by using the following formula:
Figure PCTKR2011003370-appb-I000001
, where X is an X-ray intensity at one region inside the material to be analyzed, D(X) is the density at the region, Di is the density of each standard specimen, Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen, DM is the average of all the Di, AM is the average of all Ai, and N is the number of standard specimens.
By using the method of the present invention, X-ray tomography image is converted to the image showing the internal density distribution of the material, improving the qualitative decision by naked eye by providing quantitative decision method.
Fig. 1 shows the process of performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
Fig. 2 shows the construction of the apparatus for use in performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
Fig. 3 shows the X-ray tomography image obtained by the method of the present invention of analyzing the internal density of material by using X-ray tomography.
Fig. 4 shows the result of quantitative analysis of the internal density of material obtained by the method of the present invention of analyzing the internal density of material by using X-ray tomography.
Now, the present invention will be described in more detail with reference to the attached drawings.
Fig. 1 shows the process of performing the method of the present invention of analyzing the internal density of material by using X-ray tomography.
Referring to Fig. 1, according to the method of the present invention of analyzing the internal density of material by using X-ray tomography, a cylinder-shaped jig 30 is installed between an X-ray generator 10 and an X-ray detector 11, as shown in Fig. 2 (step S101). The jig 30 has the structure into which the material 20 to be analyzed and standard specimens 21, 22, 23 can be inserted, and the outer surface of the jig 30 has preferably cylinder shape without edge since the presence of edge can generate unnecessary noise to the X-ray tomography image due to refraction and diffraction from the edge.
After installing the jig 30, the material 20 to be analyzed and a plurality of standard specimens 21, 22, 23, whose densities are known are inserted into the inside of the cylinder-shaped jig 30 (step S102).
Then, X-ray computed tomography is performed while rotating the cylinder-shaped jig 30 through 360° by rotating the turn table 12 supporting the jig 30(step S103).
Finally, the internal density of distribution of the material 20 to be analyzed is calculated by using the X-ray intensities shown in the x-ray tomography image as shown in Fig. 3(step S104).
Here, the number of standard specimens 21, 22, 23 in step S102 is preferably 3-20.
Also the standard specimens 21, 22, 23 preferably have homogeneous internal density.
Also the standard specimens 21, 22, 23 preferably have all different internal densities.
Also preferably, the standard specimens 21, 22, 23 comprise specimens with density higher than the material 20 to be analyzed and specimens with density lower than the material to be analyzed.
Also, in the step S104, the calculation of internal density distribution of the material 20 to be analyzed is performed based on the density of the standard specimens 21, 22, 23 and the X-ray intensity in the region of standard specimens present at the X-ray tomography image by using the following mathematical formula:
Figure PCTKR2011003370-appb-I000002
, where X is an X-ray intensity at one region inside the material to be analyzed, D(X) is the density at the region, Di is the density of each standard specimen, Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen, DM is the average of all the Di, AM is the average of all Ai, and N is the number of standard specimens.
The above series of processes will now be described in more detail.
The X-ray 40 generated by the X-ray generator 10 passes through the jig 30 containing the material to be analyzed 20 and the standard specimens 21, 22, 23, and reaches the X-ray detector 11. At this stage, the X-ray absorption coefficients depend on the density of the region through which the X-ray 40 passes, and these differences in transmission intensities are recorded on the X-ray detector 11.
The jig 30, the material 20 to be analyzed and the standard specimens 21, 22, 23 rotate through 360° as the turn table 12 is rotated. As the turn table 12 rotates a certain amount of angle, X-ray is radiated again, so that the differences in the intensity of the X-ray resulting from the difference in absorption coefficients are recorded.
Fig. 3 shows the X-ray tomography image of internal cross section of the material obtained by reconstructing the X-ray intensities of the images. At the center of the jig 30 is the image of the material to be analyzed 20, and on the periphery is the image of the standard specimens 21, 22, 23. The standard specimens 21, 22, 23 are provided as a reference for analyzing the density of the material to be analyzed 20, and are not limited to specific materials. In other words, any material including metal, ceramics or plastic can be used, but a single material with homogeneous internal density is preferable. The reason is that the change in the density of the standard specimens 21, 22, 23, which is a basis for the analysis, result in the change in the analysis result of the material to be analyzed 20. Also, the density of each standard specimen 21, 22, 23 should be different, and preferably comprises specimens with density higher than the material 20 to be analyzed and specimens with density lower than the material to be analyzed. The reason is that the reliability in the correlation between the X-ray intensity and density becomes higher as the density of the material 20 to be analyzed is within the density distribution of the standard specimens 21, 22, 23.
The number of standard specimens 21, 22, 23 is variable, but preferably is 3-20. When the number of the standard specimens is less than 3, it is too small for the reference of exact density, and when the number of the standard specimens is more than 20, the time for analysis becomes longer with little increase in accuracy.
The internal density of the material 20 to be analyzed can be calculated quantitatively by using the above mathematical formula, where Di is the density of standard specimens 21, 22, 23, and Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen.
Fig. 4 shows the result of quantitative analysis of the internal density D(X) of material obtained by applying the above formula to every region inside the material 20 to be analyzed. In Fig. 4, the internal density of the material 20 to be analyzed is in the range of 5.3-1.8g/㎠.
The region represented by red color is normal region 50 inside the material with high density, and the region represented by blue color is defective region 51 with low density, which results from the crack of the material or generation of air bubbles.
As described above, by using the method of the present invention, X-ray tomography image is converted to the image showing the internal density distribution of the material, improving the qualitative decision by naked eye by providing quantitative decision method.
The present invention has been described in detail with reference to a preferable example. The invention, however, is not limited by the example, and it is obvious that the example can be variously modified by those skilled in the art within the scope of the present invention. Accordingly, the scope of the invention should be interpreted by the claims attached, and all technical ideas which are equivalent to the present invention should be regarded as belonging to the scope of the present invention.
Description of numerals in the drawings
10... x-ray generator 11... x-ray detector
12... turn table 20... material to be analyzed
21,22,23... standard specimen 30... jig
40... x-ray 50... normal portion inside the material to be analyzed
51... defective portion inside the material to be analyzed

Claims (6)

  1. A method for analyzing internal density of material by using X-ray computed tomography, comprising the steps of:
    a) installing a cylinder-shaped jig between an x-ray generator and an x-ray detector,
    b) inserting a material to be analyzed and a plurality of standard specimens whose densities are known into the inside of the cylinder-shaped jig,
    c) performing X-ray computed tomography while rotating the cylinder-shaped jig through 360°, and
    d) calculating the internal density of distribution of the material to be analyzed by using the X-ray intensities shown in the x-ray tomography image.
  2. The method of claim 1, wherein the number of standard specimens is 3-20.
  3. The method of claim 1, wherein the standard specimens have homogeneous internal density.
  4. The method of claim 1, wherein the standard specimens have all different internal densities.
  5. The method of claim 1, wherein the standard specimens comprise specimens with density higher than the material to be analyzed and specimens with density lower than the material to be analyzed.
  6. The method of claim 1, wherein the calculation of internal density distribution of the material to be analyzed is performed based on the density of the standard specimens and the X-ray intensity in the region of standard specimens present at the X-ray tomography image by using the following formula:
    Figure PCTKR2011003370-appb-I000003
    , where X is an X-ray intensity at one region inside the material to be analyzed, D(X) is the density at the region, Di is the density of each standard specimen, Ai is the average of X-ray intensity at the region of the X-ray tomography image corresponding to the standard specimen, DM is the average of all the Di, AM is the average of all Ai, and N is the number of standard specimens.
PCT/KR2011/003370 2010-05-13 2011-05-06 Method for analyzing internal density of material by using x-ray computed tomography WO2011142553A2 (en)

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