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WO2008054560A3 - Certaines compositions de polyester qui comprennent du cyclobutanediol, du cyclohexanediméthanol, et de l'acide trans-cyclohexanedicarboxylique supérieur - Google Patents

Certaines compositions de polyester qui comprennent du cyclobutanediol, du cyclohexanediméthanol, et de l'acide trans-cyclohexanedicarboxylique supérieur Download PDF

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Publication number
WO2008054560A3
WO2008054560A3 PCT/US2007/015713 US2007015713W WO2008054560A3 WO 2008054560 A3 WO2008054560 A3 WO 2008054560A3 US 2007015713 W US2007015713 W US 2007015713W WO 2008054560 A3 WO2008054560 A3 WO 2008054560A3
Authority
WO
WIPO (PCT)
Prior art keywords
mole
cyclohexanedicarboxylic acid
acid residues
residues
cyclohexanedimethanol
Prior art date
Application number
PCT/US2007/015713
Other languages
English (en)
Other versions
WO2008054560A2 (fr
Inventor
Leslie Shane Moody
Emmett Dudley Crawford
Jeremy Richards Lizotte
Original Assignee
Eastman Chem Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/588,906 external-priority patent/US8193302B2/en
Priority claimed from US11/588,883 external-priority patent/US20070105993A1/en
Priority claimed from PCT/US2006/042292 external-priority patent/WO2007053549A1/fr
Priority claimed from US11/588,524 external-priority patent/US20100096589A1/en
Priority claimed from US11/588,527 external-priority patent/US20100087574A1/en
Priority claimed from US11/588,907 external-priority patent/US20070106054A1/en
Priority claimed from US11/588,554 external-priority patent/US20070100125A1/en
Priority claimed from PCT/US2006/041917 external-priority patent/WO2007053434A1/fr
Priority claimed from US11/588,458 external-priority patent/US20070100122A1/en
Priority claimed from US11/635,434 external-priority patent/US7737246B2/en
Priority claimed from US11/635,433 external-priority patent/US20070142511A1/en
Priority claimed from US11/706,791 external-priority patent/US20070232779A1/en
Priority claimed from US11/706,476 external-priority patent/US20070232778A1/en
Priority claimed from PCT/US2007/007632 external-priority patent/WO2007126855A1/fr
Priority claimed from PCT/US2007/010551 external-priority patent/WO2007139653A1/fr
Priority claimed from US11/773,275 external-priority patent/US8586701B2/en
Application filed by Eastman Chem Co filed Critical Eastman Chem Co
Publication of WO2008054560A2 publication Critical patent/WO2008054560A2/fr
Publication of WO2008054560A3 publication Critical patent/WO2008054560A3/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/199—Acids or hydroxy compounds containing cycloaliphatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181—Acids containing aromatic rings
    • C08G63/183—Terephthalic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C08G63/85—Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)

Abstract

Selon l'un de ses aspects, l'invention concerne des compositions de polyester comprenant au moins un polyester qui comprend : (A) un composant acide dicarboxylique comprenant : i) 70 à 100 % en moles de résidus d'acide cyclohexanedicarboxylique, ou d'un ester de celui-ci comprenant : (a) 70 à 98 % en moles de résidus d'acide trans-cyclohexanedicarboxylique, ou d'un ester de celui-ci; et (b) 2 à 30 % en moles de résidus d'acide cis-cyclohexanedicarboxylique, ou d'un ester de celui-ci; ii) 0 à 30 % en moles de résidus d'acide dicarboxylique aliphatique, autres que des résidus d'acide cyclohexanedicarboxylique, ayant jusqu'à 16 atomes de carbone, ou d'esters de celui-ci, autres que des résidus d'acide cyclohexanedicarboxylique; et iii) 0 à 10 % en moles de résidus d'acide dicarboxylique aromatique ayant jusqu'à 20 atomes de carbone; et (B) un composant glycol comprenant : i) 1 à 99 % en moles de résidus de 2,2,4,4-tétraméthyl-1,3-cyclobutanediol; et ii) 1 à 99 % en moles de résidus de 1, 4-cyclohexanediméthanol, de résidus de 1,3-cyclohexanediméthanol, de résidus de 1,2-cyclohexanediméthanol, ou d'esters de ceux-ci ou de mélanges de ceux-ci, le pourcentage en moles total du composant acide dicarboxylique étant égal à 100 % en moles; le pourcentage en moles total du composant glycol étant égal à 100 % en moles; la viscosité inhérente dudit polyester étant de 0,35 à 1,2 dl/g telle que déterminée dans du phénol/tétrachloroéthane à 60/40 (poids/poids) à une concentration de 0,5 g/100 ml à 25°C; et le polyester ayant une Tg de 60 à 155°C. Les polyesters peuvent être fabriqués sous la forme d'articles.
PCT/US2007/015713 2006-10-27 2007-07-10 Certaines compositions de polyester qui comprennent du cyclobutanediol, du cyclohexanediméthanol, et de l'acide trans-cyclohexanedicarboxylique supérieur WO2008054560A2 (fr)

Applications Claiming Priority (46)

Application Number Priority Date Filing Date Title
USPCT/US06/42293 2006-10-27
US11/588,883 2006-10-27
US11/588,524 US20100096589A1 (en) 2005-10-28 2006-10-27 Polyester compositions containing low amounts of cyclobutanediol and articles made therefrom
US11/588,524 2006-10-27
US11/588,906 2006-10-27
US11/588,527 US20100087574A1 (en) 2005-10-28 2006-10-27 Polyester compositions containing cyclobutanediol having a certain combination of inherent viscosity and moderate glass transition temperature and articles made therefrom
USPCT/US06/42291 2006-10-27
US11/588,907 US20070106054A1 (en) 2005-10-28 2006-10-27 Polyester compositions containing cyclobutanediol having a certain combination of inherent viscosity and high glass transition temperature and articles made therefrom
US11/588,554 US20070100125A1 (en) 2005-10-28 2006-10-27 Polyester compositions comprising minimal amounts of cyclobutanediol
PCT/US2006/041917 WO2007053434A1 (fr) 2005-10-28 2006-10-27 Compositions de polyester comprenant du cyclobutanediol et certains stabilisants thermiques et/ou des produits de reaction de ceux-ci
USPCT/US06/42069 2006-10-27
PCT/US2006/042291 WO2007053548A2 (fr) 2005-10-28 2006-10-27 Compositions de polyester comprenant des quantites minimales de cyclobutanediol
US11/588,906 US8193302B2 (en) 2005-10-28 2006-10-27 Polyester compositions which comprise cyclobutanediol and certain phosphate thermal stabilizers, and/or reaction products thereof
US11/588,554 2006-10-27
PCT/US2006/042292 WO2007053549A1 (fr) 2005-10-28 2006-10-27 Compositions de polyester contenant du cyclobutanediol qui presente une certaine combinaison d'indice logarithmique de viscosite et de temperature de transition vitreuse moderee et articles fabriques a partir de celles-ci
US11/588,527 2006-10-27
PCT/US2006/042293 WO2007053550A1 (fr) 2005-10-28 2006-10-27 Compositions de polyester contenant du cyclobutanediol qui presente une temperature de transition vitreuse elevee et articles fabriques a partir de celles-ci
US11/588,458 US20070100122A1 (en) 2005-10-28 2006-10-27 Polyester compositions containing cyclobutanediol and articles made therefrom
USPCT/US06/41917 2006-10-27
US11/588,883 US20070105993A1 (en) 2005-10-28 2006-10-27 Polyester compositions which comprise cyclobutanediol and at least one phosphorus compound
US11/588,907 2006-10-27
PCT/US2006/042069 WO2007053460A1 (fr) 2005-10-28 2006-10-27 Compositions de polyester comprenant du cyclobutanediol et au moins un compose phosphoreux
US11/588,458 2006-10-27
USPCT/US06/42292 2006-10-27
US11/635,433 US20070142511A1 (en) 2005-12-15 2006-12-07 Polyester compositions which comprise cyclobutanediol ethylene glycol, titanium, and phosphorus with improved color and manufacturing processes therefor
US11/635,434 US7737246B2 (en) 2005-12-15 2006-12-07 Polyester compositions which comprise cyclobutanediol, cyclohexanedimethanol, and ethylene glycol and manufacturing processes therefor
US11/635,434 2006-12-07
US11/635,433 2006-12-07
US11/706,791 US20070232779A1 (en) 2006-03-28 2007-02-14 Certain polyester compositions which comprise cyclohexanedimethanol, moderate cyclobutanediol, cyclohexanedimethanol, and high trans cyclohexanedicarboxylic acid
US11/706,476 US20070232778A1 (en) 2006-03-28 2007-02-14 Certain polyester compositions which comprise cyclobutanediol, cyclohexanedimethanol, and high trans-cyclohexanedicarboxylic acid
US11/706,476 2007-02-14
US11/706,791 2007-02-14
USPCT/US07/07532 2007-03-27
PCT/US2007/007632 WO2007126855A1 (fr) 2006-03-28 2007-03-27 Compositions de polyester lesquelles comprennent du cyclobutanediol et certains agents stabilisants thermiques et/ou des produits de réaction de ceux-ci
PCT/US2007/007532 WO2007123631A1 (fr) 2006-03-28 2007-03-27 Compositions polyester comprenant du cyclobutanediol et au moins un compose phosphore
USPCT/US07/07632 2007-03-27
PCT/US2007/010551 WO2007139653A1 (fr) 2006-05-23 2007-05-02 Films de lcd ou feuilles comprenant des films comprenant des compositions polyester formées de 2,2,4,4,-tétraméthyl-1,3-cyclobutanediol et de 1,4-cyclohexanediméthanol
USPCT/US07/10551 2007-05-02
USPCT/US07/10590 2007-05-02
PCT/US2007/010590 WO2007139655A1 (fr) 2006-05-23 2007-05-02 Compositions de polyester comprenant un cyclobutanediol et un certain nombre de stabilisants thermiques et/ou des produits de réaction de ceux-ci
PCT/US2007/011150 WO2007139663A1 (fr) 2006-05-23 2007-05-09 Compositions de polyester comprenant du cyclobutanediol et certains stabilisants vis-à-vis de la chaleur et/ou des produits de réaction de ceux-ci
USPCT/US07/11150 2007-05-09
US91731607P 2007-05-10 2007-05-10
US60/917,316 2007-05-10
US11/773,275 US8586701B2 (en) 2005-10-28 2007-07-03 Process for the preparation of copolyesters based on 2,2,4,4-tetramethyl-1,3-cyclobutanediol and 1,4-cyclohexanedimethanol
US11/773,275 2007-07-03

Publications (2)

Publication Number Publication Date
WO2008054560A2 WO2008054560A2 (fr) 2008-05-08
WO2008054560A3 true WO2008054560A3 (fr) 2008-07-24

Family

ID=47831243

Family Applications (4)

Application Number Title Priority Date Filing Date
PCT/US2007/015713 WO2008054560A2 (fr) 2006-10-27 2007-07-10 Certaines compositions de polyester qui comprennent du cyclobutanediol, du cyclohexanediméthanol, et de l'acide trans-cyclohexanedicarboxylique supérieur
PCT/US2007/015702 WO2008054559A1 (fr) 2006-10-27 2007-07-10 Certaines compositions de polyester qui comprennent du tétraméthylcyclobutanediol, du cyclohexanediméthanol et un acide trans-cyclohexanedicarboxylique supérieur
PCT/US2007/015701 WO2008051320A1 (fr) 2006-10-27 2007-07-10 Compositions de polyester comprenant tétraméthylcyclobutanediol, cyclohexanediméthanol et éthylèneglycol, et méthodes de production desdites compositions
PCT/US2007/015704 WO2008051321A1 (fr) 2006-10-27 2007-07-10 Compositions de polyester de couleur améliorée comprenant cyclobutanediol, éthylèneglycol, titane et phosphore, et méthodes de production desdites compositions

Family Applications After (3)

Application Number Title Priority Date Filing Date
PCT/US2007/015702 WO2008054559A1 (fr) 2006-10-27 2007-07-10 Certaines compositions de polyester qui comprennent du tétraméthylcyclobutanediol, du cyclohexanediméthanol et un acide trans-cyclohexanedicarboxylique supérieur
PCT/US2007/015701 WO2008051320A1 (fr) 2006-10-27 2007-07-10 Compositions de polyester comprenant tétraméthylcyclobutanediol, cyclohexanediméthanol et éthylèneglycol, et méthodes de production desdites compositions
PCT/US2007/015704 WO2008051321A1 (fr) 2006-10-27 2007-07-10 Compositions de polyester de couleur améliorée comprenant cyclobutanediol, éthylèneglycol, titane et phosphore, et méthodes de production desdites compositions

Country Status (8)

Country Link
EP (2) EP2074158A1 (fr)
JP (2) JP2010507716A (fr)
KR (2) KR20090079211A (fr)
BR (2) BRPI0717761A2 (fr)
CA (2) CA2666571A1 (fr)
MX (2) MX2009003369A (fr)
TW (2) TW200819497A (fr)
WO (4) WO2008054560A2 (fr)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8163850B2 (en) * 2009-02-06 2012-04-24 Eastman Chemical Company Thermosetting polyester coating compositions containing tetramethyl cyclobutanediol
US9029460B2 (en) * 2009-02-06 2015-05-12 Stacey James Marsh Coating compositions containing acrylic and aliphatic polyester blends
US8168721B2 (en) * 2009-02-06 2012-05-01 Eastman Chemical Company Coating compositions containing tetramethyl cyclobutanediol
US7915374B2 (en) * 2009-04-27 2011-03-29 Eastman Chemical Company Copolyesters having improved thermal stability and methods for making them
US9156941B2 (en) * 2010-12-20 2015-10-13 Eastman Chemical Company Color in titanium catalyzed polyesters
US8309624B2 (en) * 2011-01-17 2012-11-13 Eastman Chemical Company Haze reduction for blends of aromatic-aliphatic polyesters and antimicrobial additives
US8580872B2 (en) * 2011-07-21 2013-11-12 Eastman Chemical Company Sulfopolyester polymer compositions with improved water dispersibility
JP5806326B2 (ja) * 2011-11-01 2015-11-10 ミドリ安全株式会社 樹脂組成物及び成形体
US8623483B1 (en) * 2012-10-23 2014-01-07 Eastman Chemical Company Copolyesters containing neopentyl glycol and 2,2,4,4-tetraalkyl 1,3-cyclobutanediol
WO2015125644A1 (fr) * 2014-02-24 2015-08-27 東レ株式会社 Film polyester
JPWO2015129500A1 (ja) * 2014-02-27 2017-03-30 東レ株式会社 積層フィルム
JP6323871B2 (ja) * 2014-07-31 2018-05-16 花王株式会社 電子写真用トナー
JP6323872B2 (ja) * 2014-07-31 2018-05-16 花王株式会社 電子写真用トナー
JP2015028177A (ja) * 2014-09-22 2015-02-12 イーストマン ケミカル カンパニー ポリエステルを製造するための改善された方法
CN109563247B (zh) 2016-08-18 2021-10-08 伊士曼化工公司 使用改进的催化剂体系的包含四甲基环丁二醇和乙二醇的聚酯组合物
EP3500616B1 (fr) 2016-08-18 2021-03-24 Eastman Chemical Company Compositions à base de polyester comprenant du tétraméthylcyclobutanediol et de l'éthylène glycol, avec système catalyseur amélioré
US11447601B2 (en) 2016-08-18 2022-09-20 Eastman Chemical Company Polyester compositions which comprise tetramethylcyclobutanediol and ethylene glycol for calendering
KR102589382B1 (ko) * 2018-08-08 2023-10-12 에스케이케미칼 주식회사 폴리에스테르 수지 및 이의 제조방법
WO2021025967A1 (fr) * 2019-08-02 2021-02-11 Eastman Chemical Company Feuille multicouche
US20220372216A1 (en) * 2019-10-08 2022-11-24 Eastman Chemical Company Catalyst systems for crystallizable reactor grade resins
US11788317B2 (en) * 2020-09-28 2023-10-17 Kathryn Corcoran Cell phone canopy
WO2024164223A1 (fr) * 2023-02-09 2024-08-15 Eastman Chemical (China) Co., Ltd. Articles en polyester moulé présentant une résistance chimique esthétique améliorée

Citations (2)

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US4525504A (en) * 1983-10-24 1985-06-25 Eastman Kodak Company Stabilized polyester compositions suitable for outdoor applications
US5498668A (en) * 1994-10-31 1996-03-12 Eastman Chemical Company Blends of certain polyesters with acrylics

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US6043322A (en) * 1996-12-28 2000-03-28 Eastman Chemical Company Clear polycarbonate and polyester blends
US6037424A (en) * 1996-12-28 2000-03-14 Eastman Chemical Company Clear blends of polycarbonates and polyesters
US5989663A (en) * 1996-12-30 1999-11-23 Eastman Chemical Company Blow-molding polyesters from terephthalic acid, 2, 2, 4, 4-tetramethyl-1,3-cyclobutanediol, and ethylene glycol
US6120889A (en) * 1999-06-03 2000-09-19 Eastman Chemical Company Low melt viscosity amorphous copolyesters with enhanced glass transition temperatures
US20050010017A1 (en) * 2003-07-11 2005-01-13 Blakely Dale Milton Addition of UV inhibitors to pet process for maximum yield
JP2007521378A (ja) * 2003-07-11 2007-08-02 イーストマン ケミカル カンパニー 最大歩留りのためのｐｅｔプロセスへのｕｖ吸収剤の添加
US20060094858A1 (en) * 2004-10-28 2006-05-04 Turner Sam R Novel copolyester compositions with improved impact strength at low temperatures
WO2007053549A1 (fr) * 2005-10-28 2007-05-10 Eastman Chemical Company Compositions de polyester contenant du cyclobutanediol qui presente une certaine combinaison d'indice logarithmique de viscosite et de temperature de transition vitreuse moderee et articles fabriques a partir de celles-ci
JP2009513799A (ja) * 2005-10-28 2009-04-02 イーストマン ケミカル カンパニー 最小量のシクロブタンジオールを含むポリエステル組成物

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4525504A (en) * 1983-10-24 1985-06-25 Eastman Kodak Company Stabilized polyester compositions suitable for outdoor applications
US5498668A (en) * 1994-10-31 1996-03-12 Eastman Chemical Company Blends of certain polyesters with acrylics

Also Published As

Publication number Publication date
WO2008051320A1 (fr) 2008-05-02
MX2009003369A (es) 2009-04-14
WO2008054560A2 (fr) 2008-05-08
MX2009003375A (es) 2009-04-14
BRPI0717761A2 (pt) 2013-03-12
EP2074158A1 (fr) 2009-07-01
CA2666571A1 (fr) 2008-05-02
TW200819497A (en) 2008-05-01
JP2010507717A (ja) 2010-03-11
TW200819496A (en) 2008-05-01
KR20090079212A (ko) 2009-07-21
BRPI0717755A2 (pt) 2013-03-12
JP2010507716A (ja) 2010-03-11
EP2074174A1 (fr) 2009-07-01
CA2666585A1 (fr) 2008-05-02
WO2008051321A1 (fr) 2008-05-02
KR20090079211A (ko) 2009-07-21
WO2008054559A1 (fr) 2008-05-08
WO2008051321A8 (fr) 2008-07-10

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