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WO2002000736A3 - Purification process of polymers of alkoxystyrene - Google Patents

Purification process of polymers of alkoxystyrene Download PDF

Info

Publication number
WO2002000736A3
WO2002000736A3 PCT/US2001/020227 US0120227W WO0200736A3 WO 2002000736 A3 WO2002000736 A3 WO 2002000736A3 US 0120227 W US0120227 W US 0120227W WO 0200736 A3 WO0200736 A3 WO 0200736A3
Authority
WO
WIPO (PCT)
Prior art keywords
alkoxystyrene
polymers
purification process
purifying4
polymerin
Prior art date
Application number
PCT/US2001/020227
Other languages
French (fr)
Other versions
WO2002000736A2 (en
Inventor
Michael Thomas Sheehan
Original Assignee
Triquest Lp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Triquest Lp filed Critical Triquest Lp
Priority to AU2001271444A priority Critical patent/AU2001271444A1/en
Priority to JP2002505858A priority patent/JP4129177B2/en
Priority to EP01950455A priority patent/EP1285007A2/en
Publication of WO2002000736A2 publication Critical patent/WO2002000736A2/en
Publication of WO2002000736A3 publication Critical patent/WO2002000736A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/04—Fractionation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/008—Treatment of solid polymer wetted by water or organic solvents, e.g. coagulum, filter cakes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F12/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F12/02—Monomers containing only one unsaturated aliphatic radical
    • C08F12/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F12/14—Monomers containing only one unsaturated aliphatic radical containing one ring substituted by hetero atoms or groups containing heteroatoms
    • C08F12/22—Oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F212/02—Monomers containing only one unsaturated aliphatic radical
    • C08F212/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F212/06—Hydrocarbons
    • C08F212/08—Styrene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F212/02—Monomers containing only one unsaturated aliphatic radical
    • C08F212/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F212/06—Hydrocarbons
    • C08F212/12—Monomers containing a branched unsaturated aliphatic radical or a ring substituted by an alkyl radical
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/02—Monomers containing chlorine
    • C08F214/04—Monomers containing two carbon atoms
    • C08F214/06—Vinyl chloride
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10—Esters
    • C08F220/12—Esters of monohydric alcohols or phenols
    • C08F220/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
    • C08F222/04—Anhydrides, e.g. cyclic anhydrides
    • C08F222/06—Maleic anhydride
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/26—Treatment of polymers prepared in bulk also solid polymers or polymer melts
    • C08F6/28—Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

The invention provides a novel process for purifying4-alkoxystyrene polymers by slurrying the crude polymerin methanol. After rigorous stirring, the purified polymer is removed by centrifugation, filtration or decantation. The process is repeated as long as necessary to remove by-products and low molecular weight materials.
PCT/US2001/020227 2000-06-27 2001-06-25 Purification process of polymers of alkoxystyrene WO2002000736A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AU2001271444A AU2001271444A1 (en) 2000-06-27 2001-06-25 Purification means
JP2002505858A JP4129177B2 (en) 2000-06-27 2001-06-25 Purification means
EP01950455A EP1285007A2 (en) 2000-06-27 2001-06-25 Purification process of polymers of alkoxystyrene

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US60414000A 2000-06-27 2000-06-27
US09/604,140 2000-06-27

Publications (2)

Publication Number Publication Date
WO2002000736A2 WO2002000736A2 (en) 2002-01-03
WO2002000736A3 true WO2002000736A3 (en) 2002-05-23

Family

ID=24418332

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2001/020227 WO2002000736A2 (en) 2000-06-27 2001-06-25 Purification process of polymers of alkoxystyrene

Country Status (6)

Country Link
EP (1) EP1285007A2 (en)
JP (1) JP4129177B2 (en)
KR (1) KR100574132B1 (en)
AU (1) AU2001271444A1 (en)
TW (1) TW538060B (en)
WO (1) WO2002000736A2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6787611B2 (en) * 2000-06-27 2004-09-07 Chemfirst Electronic Materials L.P. Purification means
JP4929552B2 (en) * 2000-10-30 2012-05-09 住友化学株式会社 Method for producing solid resin
US6864324B2 (en) * 2002-04-19 2005-03-08 Chem First Electronic Materials L.P. Anhydrous, liquid phase process for preparing hydroxyl containing polymers of enhanced purity
US7534837B2 (en) * 2005-09-26 2009-05-19 E.I. Du Pont De Nemours And Company Random copolymers of ethylene and 4-vinylphenyl esters and method for preparing the same

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0357178A2 (en) * 1988-08-08 1990-03-07 Hoechst Celanese Corporation Process for the preparation of poly (vinylphenol) from poly (acetoxystyrene) by acid catalyzed transesterification
US5612452A (en) * 1993-01-11 1997-03-18 Idemitsu Kosan Co., Ltd. Process for purification of styrenic polymer
US5625007A (en) * 1990-06-29 1997-04-29 Hoechst Celanese Corp. Process for making low optical polymers and copolymers for photoresists and optical applications

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0357178A2 (en) * 1988-08-08 1990-03-07 Hoechst Celanese Corporation Process for the preparation of poly (vinylphenol) from poly (acetoxystyrene) by acid catalyzed transesterification
US5625007A (en) * 1990-06-29 1997-04-29 Hoechst Celanese Corp. Process for making low optical polymers and copolymers for photoresists and optical applications
US5612452A (en) * 1993-01-11 1997-03-18 Idemitsu Kosan Co., Ltd. Process for purification of styrenic polymer

Also Published As

Publication number Publication date
JP4129177B2 (en) 2008-08-06
AU2001271444A1 (en) 2002-01-08
TW538060B (en) 2003-06-21
EP1285007A2 (en) 2003-02-26
KR20020037349A (en) 2002-05-18
JP2004501988A (en) 2004-01-22
KR100574132B1 (en) 2006-04-25
WO2002000736A2 (en) 2002-01-03

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