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WO1997014288A3 - Spray drying method and apparatus and cleaning method for such an apparatus - Google Patents

Spray drying method and apparatus and cleaning method for such an apparatus Download PDF

Info

Publication number
WO1997014288A3
WO1997014288A3 PCT/DK1997/000078 DK9700078W WO9714288A3 WO 1997014288 A3 WO1997014288 A3 WO 1997014288A3 DK 9700078 W DK9700078 W DK 9700078W WO 9714288 A3 WO9714288 A3 WO 9714288A3
Authority
WO
WIPO (PCT)
Prior art keywords
filter elements
drying
filter
spray drying
chamber
Prior art date
Application number
PCT/DK1997/000078
Other languages
French (fr)
Other versions
WO1997014288A2 (en
Inventor
Poul Bach
Keith Masters
Original Assignee
Niro Atomizer As
Poul Bach
Keith Masters
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Niro Atomizer As, Poul Bach, Keith Masters filed Critical Niro Atomizer As
Priority to AU18712/97A priority Critical patent/AU1871297A/en
Priority to EP97904997A priority patent/EP0961646B1/en
Priority to AT97904997T priority patent/ATE216621T1/en
Priority to DE69712226T priority patent/DE69712226T2/en
Priority to US08/793,993 priority patent/US6058624A/en
Priority to PCT/DK1997/000078 priority patent/WO1997014288A2/en
Priority to DK97904997T priority patent/DK0961646T3/en
Publication of WO1997014288A2 publication Critical patent/WO1997014288A2/en
Publication of WO1997014288A3 publication Critical patent/WO1997014288A3/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Drying Of Solid Materials (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Cleaning By Liquid Or Steam (AREA)

Abstract

In fluidized spray drying of a feedstock to produce an agglomerate product by means of at least one spraying device (7) arranged in the upper part (2) of a vertically disposed drying chamber (1), in a lower part of which a fluid-bed is accommodated, a drying gas introduced into a processing zone (16) of the chamber (1) is exhausted through an integrated arrangement of filter elements (11) in the upper chamber part (2) to retain and allow agglomerationof the particles carried by the flow of drying gas on the filter elements (11). By intermittent supply of reverse flow gas pulses to the filter elements (11) the retained particles are released and returned to agglomeration zones (16, 17). The drying gas is introduced at a rate producing at the filter walls (13) a flow rate amounting to at least 150 cubic meters per hour per square meter of filter wall surface. In the non-operative condition of the spray drying apparatus the filter elements (11) may be cleaned-in-place by supplying a cleaning liquid to the interior of the elements.
PCT/DK1997/000078 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus WO1997014288A2 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
AU18712/97A AU1871297A (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus
EP97904997A EP0961646B1 (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus
AT97904997T ATE216621T1 (en) 1997-02-20 1997-02-20 METHOD AND DEVICE FOR SPRAY DRYING AND CLEANING METHOD FOR SUCH DEVICE
DE69712226T DE69712226T2 (en) 1997-02-20 1997-02-20 METHOD AND DEVICE FOR SPRAY DRYING AND CLEANING METHOD FOR SUCH A DEVICE
US08/793,993 US6058624A (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus
PCT/DK1997/000078 WO1997014288A2 (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus
DK97904997T DK0961646T3 (en) 1997-02-20 1997-02-20 Method and apparatus for spray drying and method for cleaning such apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/DK1997/000078 WO1997014288A2 (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus

Publications (2)

Publication Number Publication Date
WO1997014288A2 WO1997014288A2 (en) 1997-04-24
WO1997014288A3 true WO1997014288A3 (en) 1997-12-18

Family

ID=8155978

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DK1997/000078 WO1997014288A2 (en) 1997-02-20 1997-02-20 Spray drying method and apparatus and cleaning method for such an apparatus

Country Status (7)

Country Link
US (1) US6058624A (en)
EP (1) EP0961646B1 (en)
AT (1) ATE216621T1 (en)
AU (1) AU1871297A (en)
DE (1) DE69712226T2 (en)
DK (1) DK0961646T3 (en)
WO (1) WO1997014288A2 (en)

Families Citing this family (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69728995T2 (en) * 1996-12-11 2004-10-28 Asahi Denka Kogyo K.K. METHOD AND APPARATUS FOR PRODUCING CHLORINE RUBBER
US6149716A (en) * 1997-10-31 2000-11-21 Niro A/S Method of cleaning a filter unit, and a filter unit for filtering gas
EP1155294A1 (en) * 1999-02-23 2001-11-21 Teraprobe Limited Method and apparatus for terahertz imaging
US6730349B2 (en) * 1999-04-19 2004-05-04 Scimed Life Systems, Inc. Mechanical and acoustical suspension coating of medical implants
AU4133899A (en) * 1999-06-08 2000-12-28 Niro A/S A process and a plant for spray drying
WO2000075281A2 (en) 1999-06-09 2000-12-14 University Technology Corporation Supercritical fluid-assisted nebulization and bubble drying
AU4770099A (en) * 1999-07-13 2001-01-30 Niro A/S A process and an apparatus for spray drying a liquid to produce an agglomerated product
US6463675B1 (en) 1999-09-29 2002-10-15 Niro A/S Process and a plant for spray drying
DK1227732T3 (en) * 1999-11-09 2003-11-03 Niro Atomizer As Process for producing a spray-dried, agglomerated infant, whole milk or skimmed milk powder and such powder
MXPA03003968A (en) 2000-11-06 2004-05-24 Cabot Corp Modified oxygen reduced valve metal oxides.
US8095687B1 (en) * 2001-03-26 2012-01-10 Microsoft Corporation Systems and methods for managing state in a cluster of servers
NL1022186C2 (en) * 2002-12-17 2004-06-18 Carlisle Process Systems B V Spray drying device.
MY139184A (en) * 2004-12-06 2009-08-28 Novartis Ag Method of drying molds
NL1028884C2 (en) * 2005-04-27 2006-10-30 Tabagh A G Method and device for increasing the dry matter content of a biological fluid, and use of water vapor from a biological fluid to produce a water product.
UA91722C2 (en) * 2005-09-30 2010-08-25 Ниро А/С Apparatus and process for drying high carbohydrate content liquids to non-sticky powder
EP2158029B1 (en) * 2007-04-10 2019-05-29 Gea Process Engineering Inc. Process gas filter and process for cleaning the same
US9332776B1 (en) 2010-09-27 2016-05-10 ZoomEssence, Inc. Methods and apparatus for low heat spray drying
US8939388B1 (en) 2010-09-27 2015-01-27 ZoomEssence, Inc. Methods and apparatus for low heat spray drying
US8715402B2 (en) * 2011-03-22 2014-05-06 Mitsubishi Heavy Industries, Ltd. Air pollution control system and air pollution control method, spray drying device of dewatering filtration fluid from desulfurization discharged water, and method thereof
JP5943820B2 (en) 2012-11-30 2016-07-05 三菱重工業株式会社 Spray drying apparatus and exhaust gas treatment system for dehydrated filtrate
IN2013CH04500A (en) 2013-10-04 2015-04-10 Kennametal India Ltd
SG11201602959TA (en) 2013-10-18 2016-05-30 Gea Process Engineering As Method for cleaning a nozzle arrangement in a spray drying apparatus, and spray drying apparatus for carrying out the method
DE102016218085A1 (en) * 2016-09-21 2018-03-22 Robert Bosch Gmbh Fluidized bed system
US10486173B2 (en) 2017-08-04 2019-11-26 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
CA3071115C (en) 2017-08-04 2022-06-21 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US9861945B1 (en) 2017-08-04 2018-01-09 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US9993787B1 (en) 2017-08-04 2018-06-12 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US10155234B1 (en) 2017-08-04 2018-12-18 ZoomEssence, Inc. Ultrahigh efficiency spray drying apparatus and process
US10569244B2 (en) 2018-04-28 2020-02-25 ZoomEssence, Inc. Low temperature spray drying of carrier-free compositions
ES2952135B2 (en) * 2022-03-11 2024-03-11 Quim Tecnica Ecologica S L U PROCESS FOR THE TREATMENT OF WATERS AND AQUEOUS SUSPENSIONS WITH HIGH CONTENT OF SALTS, AMMONIA, HYDROGEN SULFYRIC ACID AND ORGANIC MATTER AND THE REAGENTS USED
CN115265097B (en) * 2022-07-29 2023-05-16 重庆新申世纪新材料科技有限公司 Spray drying equipment for high specific area powder material

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4190622A (en) * 1978-05-04 1980-02-26 Standard Oil Company (Ohio) Process for prilling urea
GB2113112A (en) * 1982-01-09 1983-08-03 Sandoz Ltd Preparing dust-free granular material
EP0115285A1 (en) * 1983-01-21 1984-08-08 Henkel Kommanditgesellschaft auf Aktien Spray dryer and method of operating the dryer
DD281964A5 (en) * 1988-12-30 1990-08-29 Leipzig Energiekombinat METHOD AND DEVICE FOR THE ADVICE OF DAMAGING AND DUSTING
US5135611A (en) * 1990-05-25 1992-08-04 Cameron Gordon M Method and apparatus for combined spray drying and gas cleaning
EP0520953A1 (en) * 1991-06-28 1992-12-30 Glatt Air Techniques, Inc. Apparatus for moving and treating particles

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4953308A (en) * 1989-02-06 1990-09-04 Vector Corporation Filter system for a fluid bed granulator/dryer
US5446974A (en) * 1993-09-23 1995-09-05 Gubler; Scott A. Compact flexible filter assembly for a fluid bed granulator, coater and dryer
JPH09505516A (en) * 1993-11-17 1997-06-03 ニロ・ホールディング・アー／エス Spray drying method and apparatus for producing agglomerated powder

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4190622A (en) * 1978-05-04 1980-02-26 Standard Oil Company (Ohio) Process for prilling urea
GB2113112A (en) * 1982-01-09 1983-08-03 Sandoz Ltd Preparing dust-free granular material
EP0115285A1 (en) * 1983-01-21 1984-08-08 Henkel Kommanditgesellschaft auf Aktien Spray dryer and method of operating the dryer
DD281964A5 (en) * 1988-12-30 1990-08-29 Leipzig Energiekombinat METHOD AND DEVICE FOR THE ADVICE OF DAMAGING AND DUSTING
US5135611A (en) * 1990-05-25 1992-08-04 Cameron Gordon M Method and apparatus for combined spray drying and gas cleaning
EP0520953A1 (en) * 1991-06-28 1992-12-30 Glatt Air Techniques, Inc. Apparatus for moving and treating particles

Also Published As

Publication number Publication date
EP0961646B1 (en) 2002-04-24
WO1997014288A2 (en) 1997-04-24
AU1871297A (en) 1997-05-07
US6058624A (en) 2000-05-09
ATE216621T1 (en) 2002-05-15
DK0961646T3 (en) 2002-08-19
DE69712226T2 (en) 2002-10-17
EP0961646A2 (en) 1999-12-08
DE69712226D1 (en) 2002-05-29

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