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SU852811A1 - Black enamel - Google Patents

Black enamel Download PDF

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Publication number
SU852811A1
SU852811A1 SU792854951A SU2854951A SU852811A1 SU 852811 A1 SU852811 A1 SU 852811A1 SU 792854951 A SU792854951 A SU 792854951A SU 2854951 A SU2854951 A SU 2854951A SU 852811 A1 SU852811 A1 SU 852811A1
Authority
SU
USSR - Soviet Union
Prior art keywords
glaze
firing temperature
black
cao
feo
Prior art date
Application number
SU792854951A
Other languages
Russian (ru)
Inventor
Гурам Григорьевич Гаприндашвили
Роин Иосифович Девидзе
Манана Корнеловна Кекелидзе
Original Assignee
Грузинский Ордена Ленина И Орденатрудового Красного Знамени Политехническийинститут Им. B.И.Ленина
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Application filed by Грузинский Ордена Ленина И Орденатрудового Красного Знамени Политехническийинститут Им. B.И.Ленина filed Critical Грузинский Ордена Ленина И Орденатрудового Красного Знамени Политехническийинститут Им. B.И.Ленина
Priority to SU792854951A priority Critical patent/SU852811A1/en
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Publication of SU852811A1 publication Critical patent/SU852811A1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02—Frit compositions, i.e. in a powdered or comminuted form

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Description

Изобретение относится к керамической промышленности и может быть использовано для покрытия фарфоровых, полуфарфоровых, каменных и других керамических изделий при низкой температуре.The invention relates to the ceramic industry and can be used for coating porcelain, semi-porcelain, stone and other ceramic products at low temperature.

Известна черная глазурь, включающая следующие компоненты, вес.%:Known black glaze, comprising the following components, wt.%:

S i oz S io z 40,1-45,2 40.1-45.2 1 и 1 and А Мз A mz 14,5-16 14.5-16 6,6-8,2 6.6-8.2 Т i 02 T i 0 2 0,8-1,1 0.8-1.1 Мп 02 Mp 0 2 2,6-3 2.6-3 15 fifteen с ао with ao 4,3-5,5 4.3-5.5 Мд 0 Md 0 3,1-3,8 3.1-3.8 N а 2 0N a 2 0 2-2,9 2-2.9 кгоto r about 0,9-1,2 0.9-1.2 С о 2 0 к C about 2 0 to 3,8-5,5 3.8-5.5 20 20 13,6-16,2 13.6-16.2 UJ. UJ. Наиболее близкой Closest по составу in composition / являет· / is ся черная глазурь, black icing содержащая containing следую- following- щие компоненты, вес total components, weight % : %: S i 0 2 А F е 2 0 т;ог-S i 0 2 A F e 2 0 t; о g - 52-60 23-26,3 4,2-5,8 0,3-0,4 52-60 23-26.3 4.2-5.8 0.3-0.4 25 25 Мп 0 Mp 0 0,4-0, 5 0.4-0.5 С а 0 C a 0 5,8-4,1 5.8-4.1 30 thirty И <] 0 And <] 0 2,1-2.9 2.1-2.9

К2С 3,2-5,6K 2 C 3.2-5.6

Со?03 3-5 [2].So ? 0 3 3-5 [2].

Недостатком известных глазурей является высокая температура обжига и короткий интервал плавления 12601280е С.A disadvantage of the known glazes is the high firing temperature and a short melting range of 12601280 e C.

Целью изобретения является снижение температуры обжига и расширениеThe aim of the invention is to reduce the firing temperature and expansion

его интервала. Она достигается тем, its interval. It is achieved by что глазурь, what is the icing включающая Si02 , АЕ^Оа,including Si0 2 , AE ^ Oa, F&2. 0j , Fe 0 , Т F & 2. 0j, Fe 0, T i 02 ,i 0 2 , MnO, СаО, MgO.Na^O , MnO, CaO, MgO.Na ^ O, К 20 , С о 20-¾ ,K 2 0, C o 20-¾, содержит указанные ком- contains the specified com поненты в следующем соотношении вес. % ponents in the following weight ratio. % S i 02 S i 0 2 55,60-60,10 55.60-60.10 A h 0э A h 0 e 13,72-15,82 13.72-15.82 F е 2 СЩ F e 2 2,80-2,95 2.80-2.95 FeO FeO 0,53-0,62 0.53-0.62 Т ί 0 2 T ί 0 2 0,32-0,41 0.32-0.41 ИпО IPO 0,05-0,07 0.05-0.07 СаО CaO 12,8-13,66 12.8-13.66 М g 0 M g 0 1,60-1,80 1.60-1.80 N а 2 0 N a 2 0 2,80-3,61 2.80-3.61 κλοκ λ ο 1,88-2,64 1.88-2.64 С οι. 0-j With οι. 0-j 3,20-4,30. 3.20-4.30. Согласно изобретению приготовлены According to the invention prepared составы глазурей, glaze formulations, содержащие,вес.%: containing, wt.%: ί ί 1 1 III 1 1 III S i 0 2. S i 0 2. 5 5,60 5 5.60 60,10 57,82 60.10 57.82 А £20-5 A £ 20-5 15,82 15.82 13,72 14,03 13.72 14.03

Fea03 Fe a 0 3 2,95 2.95 2,80 2.80 2,89 2.89 FeO FeO 0,53 0.53 0,62 0.62 0,56 0.56 Ti02 Ti0 2 0 ,32 0, 32 0,41 0.41 0 , 33 0, 33 MnO MnO 0,05 0.05 0,07 0,07 0,06 0.06 CaO Cao 13,38 13.38 12,80 12.80 13,06 13.06 MgO MgO 1,80 1.80 1 ,60 1, 60 1, 76 1, 76 N a ¢0 N a ¢ 0 3,61 3.61 2,80 2.80 3,21 3.21 K20K 2 0 2,64 2.64 1,88 1.88 1, 98 1, 98 Co£0 г Co £ 0 g 3,30 3.30 3 , 20 3, 20 4,30 4.30 Указанные Indicated составы compositions имеют have следующие the following

физико-химические свойства:physiochemical properties:

КТР Д1(Г71/градKTR D1 (G 7 1 / city 55 55 51 51 52 52 Термостойкость Heat resistance 9 9 10 10 10 10 Толщина глазурно- Glazed thickness го слоя, мм th layer, mm 0,2 0.2 0,22 0.22 0 ,25 0, 25 Плотность по Density by г g ареометру, град/см1,48 hydrometer, deg / cm1.48 1,48 1.48 1,46 1.46 Киелотостой- Kielotostoy- кость, % bone% 99,6 99.6 99,5 99.5 99,6 99.6 Микротвердость, Microhardness, кг/мм 2 kg / mm 2 620 620 58 0 58 0 610 610 Блеск, % Gloss,% 78 78 76 76 7 7 7 7

Температура плавления,°С Цвет покрытия Глазурь готовятMelting point, ° С Coating color Glaze is prepared

1190-12501190-1250

Черный следующим способом.Black in the following way.

доbefore

Составные-части глазури измельчают,^ прохождения через сито 10000отв/смThe constituent parts of the glaze are crushed, passing through a sieve of 10000 holes / cm

006) в шаровых мельницах мокрого помола и наносят на поверхность керамических изделий методом окунания или пульверизации.006) in wet ball mills and applied to the surface of ceramic products by dipping or spraying.

Применение глазури позволяет увеличить производительность и межремонтный период печей и уменьшить расход топлива.The use of glaze can increase the productivity and the overhaul period of furnaces and reduce fuel consumption.

Claims (2)

Изобретение откоситс  к ческой промьиилеипости и може использовано дл  покрыти  фа вых, полуфарфоровых, каменн гих керамических изделий при температуре. 40,1-45,2 14,5-16 6,6-8,2 О ,8-1, 1 2,6-3 4,8-5 , 5 3,1-3,8 2-2.9 0,9-1,2 3,8-5,5 13,6-16,2 Наиболее блиткой по соста с  черна  глазурь, содерхкаща щие компоненты, вес.%: SiO 52-60 дЕгО 23-26,3 ,2-5,8 о ,3-0,4 0,4-0,5 , 8 - 4 , 1 2,1-2,9 RjO3,2-5,6 Co.,0j3-5 2. Недостатком известных глазурей  ветс  высока  температура обжига и роткий интервал плав.пени  126080С . Целью изобретени   вл етс  снижее температуры обжига и расширение о интервала. Она достигаетс  тем, о глазурь, вкл.ючарэща  SiO, AEjOj, iOj, FeO, TiOj, MnO, CaO, MgO. , O , , содержит указанные комненты в следующем соотношении вес. % SiOs55,60-60,10 А 10з13,72-15,82 fejOg2,80-2,95 FeO0,53-0,62 Ti020,32-0,41 МпО0,05-0,07 СаО12,8-13,66 f-lgO1,60-1,80 ,80-3,61 К 2.01,88-2,64 CoiO-i3,20-4,30, Согласноизобретению приготовлены тавы глазурей, содержащие,вес.%: I { I III SiOi55,6060,10 57,82 АЕгО-з15,8213,72 14,03 РедО 2,95 F е О 0,53 О,32 МпО 0,05 СаО 13,38 МдО 1,80 МагО 3,61 2,64 3, 30 Указанные составы физико-химические ев КТР о(.1СГ1/град Термостойкость Толщина глазурного сло , мм Плотность по ареометру, град/с Киелотоетойкость , % Микротвердость, кг/мм Блеск, % Температура плавлени ,°С 1190-1250 Черный Цвет покрыти  следующим способом, Глазурь готов т глазури измельча от.25 Составнпз1е части до прохождени  через сито 10000отв/см (№ 006) в шаровых мельницах мокрого помола и нанос т на поверхность керамических изделий методом окунани  или пульверизации. чи ны то А M ю же ни з ш п № Применение глазури позвол ет увелить производительность и межремонтй период печей и уменьиаить расход плива. Формула изобретени  Черна  глазурь, включающа  S i 02 МпО, СаОТ 0ь feO. ОЭ, Fe; O, , , 5 о т л и ч а   тем, что. Д а   с с целью снини  температуры обжига и расшире  его интервала, она содержит уканные компоненты в следующем соотнонии ,вес.% : 55,60-60,10 13,72-15,82 2,80-2,95 0,53-0,62 0,32-0,41 0,05-0,07 12,8-13,66 1,60-1,80 2,80-3,61 1,88-2,64 3,20-4 ,30 Источники информации, ин тые во внимание при экспертизе 1.Авторское свидетельство СССР 380604, кл. С 03 С 9/00, 1973. The invention is agile and can be used to coat fusion, semi-porcelain, stone ceramics at a temperature. 40.1-45.2 14.5-16 6.6-8.2 O, 8-1, 1 2.6-3 4.8-5, 5 3.1-3.8 2-2.9 0, 9-1.2 3.8-5.5 13.6-16.2 The most glare of black glaze containing components, wt.%: SiO 52-60 DEGO 23-26.3, 2-5, 8 о, 3-0,4 0,4-0,5, 8 - 4, 1 2,1-2,9 RjO3,2-5,6 Co., 0j3-5 2. The disadvantage of the famous glaze of the vets is high firing temperature and a rotary interval of a floating penny 126080C. The aim of the invention is to reduce the firing temperature and the expansion of the interval. It is achieved by glazing, including SiO, AEjOj, iOj, FeO, TiOj, MnO, CaO, MgO. , O,, contains the specified comments in the following weight ratio. % SiOs55.60-60.10 A 10З13.72-15.82 fejOg2.80-2.95 FeO0.53-0.62 Ti020.32-0.41 MpO0.05-0.07 CaO12.8-13, 66 f-lgO1,60-1,80, 80-3,61 K 2.01,88-2,64 CoiO-i 3,20-4,30, According to the invention Tava glazes are prepared, containing, wt.%: I {I III SiOi55 , 6060.10 57.82 AEgO-h15.8213.72 14.03 RedO 2.95 F e O 0.53 O, 32 MpO 0.05 CaO 13.38 MgO 1.80 MagO 3.61 2.64 3 , 30 Specified compositions of physico-chemical EV KTR about (.1СГ1 / grad Thermal stability Thickness of glazing layer, mm Density by hydrometer, degree / s Kielototoyuykost,% Microhardness, kg / mm Gloss,% Melting point, ° С 1190-1250 Black Color of coating In the following way, the Glaze is prepared to grind a glaze of from .25 Composition As before passing through a 10000otv / cm sieve (No. 006) in wet milling ball mills, they are applied to the surface of ceramic products by dipping or spraying. This is done using glaze to increase productivity and overhaul furnaces and reduce the consumption of plyv. Claims of the invention Black glaze, including S i 02 MpO, CaUOT 0 feO. OE, Fe; O,,, 5 o tl and h and the fact that. In order to lower the firing temperature and expand its range, it contains the components in the following ratio, wt.%: 55.60-60.10 13.72-15.82 2.80-2.95 0.53- 0.62 0.32-0.41 0.05-0.07 12.8-13.66 1.60-1.80 2.80-3.61 1.88-2.64 3.20-4 , 30 Sources of information, which are taken into account in the examination 1. The author's certificate of the USSR 380604, cl. From 03 to 9/00, 1973. 2.Авторскоесвидетельство СССР 359241, кл. С 03 С 9/00, 1972.2. Authorship certificate USSR 359241, cl. From 03 to 9/00, 1972.
SU792854951A 1979-12-18 1979-12-18 Black enamel SU852811A1 (en)

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Cited By (12)

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WO2010126581A1 (en) * 2009-05-01 2010-11-04 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8500933B2 (en) 2007-12-14 2013-08-06 Guardian Industries Corp. Localized heating of edge seals for a vacuum insulating glass unit, and/or unitized oven for accomplishing the same
US8506738B2 (en) 2007-12-17 2013-08-13 Guardian Industries Corp. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US8733128B2 (en) 2011-02-22 2014-05-27 Guardian Industries Corp. Materials and/or method of making vacuum insulating glass units including the same
US8802203B2 (en) 2011-02-22 2014-08-12 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US9290408B2 (en) 2011-02-22 2016-03-22 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US9309146B2 (en) 2011-02-22 2016-04-12 Guardian Industries Corp. Vanadium-based frit materials, binders, and/or solvents and methods of making the same
US9359247B2 (en) 2011-02-22 2016-06-07 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9458052B2 (en) 2011-02-22 2016-10-04 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9593527B2 (en) 2014-02-04 2017-03-14 Guardian Industries Corp. Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same
US9822580B2 (en) 2011-02-22 2017-11-21 Guardian Glass, LLC Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same
US9988302B2 (en) 2014-02-04 2018-06-05 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods

Cited By (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8500933B2 (en) 2007-12-14 2013-08-06 Guardian Industries Corp. Localized heating of edge seals for a vacuum insulating glass unit, and/or unitized oven for accomplishing the same
US8506738B2 (en) 2007-12-17 2013-08-13 Guardian Industries Corp. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US10717668B2 (en) 2007-12-17 2020-07-21 Guardian Glass, Llc. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US10294140B2 (en) 2007-12-17 2019-05-21 Guardian Glass, LLC Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
WO2010126581A1 (en) * 2009-05-01 2010-11-04 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8227055B2 (en) 2009-05-01 2012-07-24 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8590343B2 (en) 2009-05-01 2013-11-26 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8763427B2 (en) 2009-05-01 2014-07-01 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US9822580B2 (en) 2011-02-22 2017-11-21 Guardian Glass, LLC Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same
US10196299B2 (en) 2011-02-22 2019-02-05 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US9359247B2 (en) 2011-02-22 2016-06-07 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9458052B2 (en) 2011-02-22 2016-10-04 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US11028009B2 (en) 2011-02-22 2021-06-08 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9776910B2 (en) 2011-02-22 2017-10-03 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US9290408B2 (en) 2011-02-22 2016-03-22 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US11014847B2 (en) 2011-02-22 2021-05-25 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US10087676B2 (en) 2011-02-22 2018-10-02 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US10107028B2 (en) 2011-02-22 2018-10-23 Guardian Glass, LLC Method of making vacuum insulated glass (VIG) window unit
US10125045B2 (en) 2011-02-22 2018-11-13 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9309146B2 (en) 2011-02-22 2016-04-12 Guardian Industries Corp. Vanadium-based frit materials, binders, and/or solvents and methods of making the same
US8802203B2 (en) 2011-02-22 2014-08-12 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US10329187B2 (en) 2011-02-22 2019-06-25 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US10858880B2 (en) 2011-02-22 2020-12-08 Guardian Glass, LLC Vanadium-based frit materials, binders, and/or solvents and/or methods of making the same
US10752535B2 (en) 2011-02-22 2020-08-25 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US8733128B2 (en) 2011-02-22 2014-05-27 Guardian Industries Corp. Materials and/or method of making vacuum insulating glass units including the same
US10465433B2 (en) 2014-02-04 2019-11-05 Guardian Glass, Llc. Vacuum insulating glass (VIG) unit with lead-free dual-frit seals and/or methods of making the same
US10421684B2 (en) 2014-02-04 2019-09-24 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods
US9988302B2 (en) 2014-02-04 2018-06-05 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods
US9593527B2 (en) 2014-02-04 2017-03-14 Guardian Industries Corp. Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same

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