SG11201900068PA - Single crystal silicon plate-shaped body and production method therefor - Google Patents
Single crystal silicon plate-shaped body and production method thereforInfo
- Publication number
- SG11201900068PA SG11201900068PA SG11201900068PA SG11201900068PA SG11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA
- Authority
- SG
- Singapore
- Prior art keywords
- single crystal
- crystal silicon
- shaped body
- silicon plate
- ppma
- Prior art date
Links
- 229910021421 monocrystalline silicon Inorganic materials 0.000 title abstract 7
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 5
- 229910052760 oxygen Inorganic materials 0.000 abstract 5
- 239000001301 oxygen Substances 0.000 abstract 5
- 239000002244 precipitate Substances 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 230000005540 biological transmission Effects 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/20—Controlling or regulating
- C30B15/206—Controlling or regulating the thermal history of growing the ingot
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/06—Silicon
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
- C30B29/64—Flat crystals, e.g. plates, strips or discs
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L31/00—Semiconductor devices sensitive to infrared radiation, light, electromagnetic radiation of shorter wavelength or corpuscular radiation and specially adapted either for the conversion of the energy of such radiation into electrical energy or for the control of electrical energy by such radiation; Processes or apparatus specially adapted for the manufacture or treatment thereof or of parts thereof; Details thereof
- H01L31/18—Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof
- H01L31/1804—Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof comprising only elements of Group IV of the Periodic Table
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
SINGLE CRYSTAL SILICON PLATE-SHAPED BODY AND PRODUCTION METHOD THEREFOR An object of the invention is to develop a single crystal silicon that becomes such a high-performance device as a solar cell or a power device in which decrease in lifetime is suppressed even if heating treatment from 800°C to 1100°C performed in a device production process is applied in a single crystal silicon plate-shaped body having a high oxygen concentration. Provided is a single crystal silicon plate-shaped body as cut out from an upper portion of a straight body portion of a CZ method single crystal silicon ingot in which an interstitial oxygen concentration in a crystal is 25 ppma to 45 ppma and a substitutional carbon concentration is 0.5 ppma or less in a radial center, wherein in the radial center, oxygen precipitates are not observed in a bulk in an image of 200,000 times by means of a transmission electron microscope, and after heating the single crystal silicon plate-shaped body at 950°C for 60 minutes, oxygen precipitates are observed in an image of the 200,000 times, and a shape of the oxygen precipitates is observed in a polyhedral structure in an image of 2,000,000 times. (Fig.1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016134375 | 2016-07-06 | ||
PCT/JP2017/024235 WO2018008561A1 (en) | 2016-07-06 | 2017-06-30 | Single crystal silicon plate-shaped body and production method therefor |
Publications (1)
Publication Number | Publication Date |
---|---|
SG11201900068PA true SG11201900068PA (en) | 2019-02-27 |
Family
ID=60912812
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SG11201900068PA SG11201900068PA (en) | 2016-07-06 | 2017-06-30 | Single crystal silicon plate-shaped body and production method therefor |
Country Status (8)
Country | Link |
---|---|
US (1) | US10975496B2 (en) |
JP (1) | JP6484762B2 (en) |
KR (1) | KR102032535B1 (en) |
CN (1) | CN109477240B (en) |
DE (1) | DE112017003436T5 (en) |
SG (1) | SG11201900068PA (en) |
TW (1) | TWI732898B (en) |
WO (1) | WO2018008561A1 (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6645545B1 (en) * | 2018-09-03 | 2020-02-14 | 株式会社Sumco | Method for evaluating carbon concentration of silicon sample, method for evaluating silicon wafer manufacturing process, method for manufacturing silicon wafer, and method for manufacturing silicon single crystal ingot |
JP6979007B2 (en) * | 2018-12-17 | 2021-12-08 | グローバルウェーハズ・ジャパン株式会社 | Ultra-low oxygen concentration measurement method for silicon wafers |
US11885036B2 (en) | 2019-08-09 | 2024-01-30 | Leading Edge Equipment Technologies, Inc. | Producing a ribbon or wafer with regions of low oxygen concentration |
CN115148858B (en) * | 2022-08-01 | 2024-06-11 | 安徽华晟新能源科技有限公司 | Passivation method of silicon solar cell |
Family Cites Families (30)
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JPH03133121A (en) * | 1989-10-19 | 1991-06-06 | Showa Denko Kk | Silicon substrate for semiconductor device and manufacture thereof |
JPH0789789A (en) | 1993-09-20 | 1995-04-04 | Fujitsu Ltd | Si crystal, method for growing crystal and device therefor |
US5593494A (en) * | 1995-03-14 | 1997-01-14 | Memc Electronic Materials, Inc. | Precision controlled precipitation of oxygen in silicon |
JP3006669B2 (en) | 1995-06-20 | 2000-02-07 | 信越半導体株式会社 | Method and apparatus for producing silicon single crystal having uniform crystal defects |
JPH09190954A (en) | 1996-01-10 | 1997-07-22 | Sumitomo Sitix Corp | Semiconductor substrate and its manufacture |
US6277501B1 (en) * | 1996-07-29 | 2001-08-21 | Sumitomo Metal Industries, Ltd. | Silicon epitaxial wafer and method for manufacturing the same |
US6503594B2 (en) | 1997-02-13 | 2003-01-07 | Samsung Electronics Co., Ltd. | Silicon wafers having controlled distribution of defects and slip |
JPH1143393A (en) * | 1997-07-23 | 1999-02-16 | Nippon Steel Corp | Silicon single crystal wafer and its production |
JP4112654B2 (en) * | 1997-09-19 | 2008-07-02 | シルトロニック・ジャパン株式会社 | Method for manufacturing silicon wafer |
CN1326518A (en) | 1998-06-26 | 2001-12-12 | Memc电子材料有限公司 | Process for growth of defect free silicon crystals of arbitrarily large diameters |
TW505710B (en) * | 1998-11-20 | 2002-10-11 | Komatsu Denshi Kinzoku Kk | Production method for silicon single crystal and production device for single crystal ingot, and heat treating method for silicon single crystal wafer |
JP3750526B2 (en) * | 1999-03-16 | 2006-03-01 | 信越半導体株式会社 | Silicon wafer manufacturing method and silicon wafer |
JP2002043318A (en) * | 2000-07-28 | 2002-02-08 | Shin Etsu Handotai Co Ltd | Method for manufacturing silicon single crystal wafer |
JP2002184779A (en) * | 2000-12-13 | 2002-06-28 | Shin Etsu Handotai Co Ltd | Annealed wafer and method of manufacturing the same |
DE60213759T2 (en) * | 2001-01-26 | 2006-11-30 | Memc Electronic Materials, Inc. | SILICON WITH LOW DEFECT DENSITY AND EMPTY-DOMINANTED CORE THAT IS ESSENTIALLY FREE FROM OXIDATION-INDUCED STACKING ERRORS |
US7201800B2 (en) * | 2001-12-21 | 2007-04-10 | Memc Electronic Materials, Inc. | Process for making silicon wafers with stabilized oxygen precipitate nucleation centers |
TWI276161B (en) | 2001-12-21 | 2007-03-11 | Memc Electronic Materials | Ideal oxygen precipitating silicon wafers with nitrogen/carbon stabilized oxygen precipitate nucleation centers and process for making the same |
WO2003088346A1 (en) * | 2002-04-10 | 2003-10-23 | Memc Electronic Materials, Inc. | Process for controlling denuded zone depth in an ideal oxygen precipitating silicon wafer |
KR100573473B1 (en) | 2004-05-10 | 2006-04-24 | 주식회사 실트론 | Silicon wafer and method of fabricating the same |
EP1780781B1 (en) * | 2004-06-30 | 2019-08-07 | SUMCO Corporation | Process for producing silicon wafer |
CN1269186C (en) * | 2004-11-22 | 2006-08-09 | 浙江大学 | Carbon doped silicon sheet with internal impurity absorbing function and production thereof |
JPWO2007013189A1 (en) * | 2005-07-27 | 2009-02-05 | 株式会社Sumco | Silicon wafer and manufacturing method thereof |
JP2007194232A (en) * | 2006-01-17 | 2007-08-02 | Shin Etsu Handotai Co Ltd | Process for producing silicon single crystal wafer |
JP5151777B2 (en) * | 2008-07-30 | 2013-02-27 | 株式会社Sumco | Method for manufacturing silicon epitaxial wafer and silicon epitaxial wafer |
KR20100036155A (en) * | 2008-09-29 | 2010-04-07 | 매그나칩 반도체 유한회사 | Silicon wafer and fabrication method thereof |
JP5088338B2 (en) * | 2009-03-10 | 2012-12-05 | 信越半導体株式会社 | Method of pulling silicon single crystal |
JP2011228459A (en) | 2010-04-19 | 2011-11-10 | Sumco Corp | Silicon wafer and method of manufacturing the same |
JP5984448B2 (en) * | 2012-03-26 | 2016-09-06 | グローバルウェーハズ・ジャパン株式会社 | Silicon wafer |
JP5885305B2 (en) * | 2013-08-07 | 2016-03-15 | グローバルウェーハズ・ジャパン株式会社 | Silicon wafer and manufacturing method thereof |
CN104726931A (en) * | 2015-03-30 | 2015-06-24 | 江苏盎华光伏工程技术研究中心有限公司 | Single crystal furnace with annealing device and control method for single crystal furnace |
-
2017
- 2017-06-30 SG SG11201900068PA patent/SG11201900068PA/en unknown
- 2017-06-30 CN CN201780041617.XA patent/CN109477240B/en not_active Expired - Fee Related
- 2017-06-30 DE DE112017003436.1T patent/DE112017003436T5/en not_active Withdrawn
- 2017-06-30 KR KR1020187037710A patent/KR102032535B1/en active IP Right Grant
- 2017-06-30 US US16/315,216 patent/US10975496B2/en active Active
- 2017-06-30 WO PCT/JP2017/024235 patent/WO2018008561A1/en active Application Filing
- 2017-06-30 JP JP2018526343A patent/JP6484762B2/en active Active
- 2017-07-04 TW TW106122354A patent/TWI732898B/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO2018008561A1 (en) | 2018-01-11 |
DE112017003436T5 (en) | 2019-03-21 |
CN109477240B (en) | 2019-12-27 |
TWI732898B (en) | 2021-07-11 |
JPWO2018008561A1 (en) | 2018-11-29 |
KR102032535B1 (en) | 2019-10-15 |
US20190161888A1 (en) | 2019-05-30 |
CN109477240A (en) | 2019-03-15 |
JP6484762B2 (en) | 2019-03-13 |
KR20190007502A (en) | 2019-01-22 |
TW201816201A (en) | 2018-05-01 |
US10975496B2 (en) | 2021-04-13 |
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