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SG11201804341XA - Catalysts containing brookite titanium - Google Patents

Catalysts containing brookite titanium

Info

Publication number
SG11201804341XA
SG11201804341XA SG11201804341XA SG11201804341XA SG11201804341XA SG 11201804341X A SG11201804341X A SG 11201804341XA SG 11201804341X A SG11201804341X A SG 11201804341XA SG 11201804341X A SG11201804341X A SG 11201804341XA SG 11201804341X A SG11201804341X A SG 11201804341XA
Authority
SG
Singapore
Prior art keywords
houston
suite
international
lyondellbasell
mckinney
Prior art date
Application number
SG11201804341XA
Inventor
Sandor Nagy
Barbara Kimmich
Xueyong Yang
Osment Jenny Oran
Debra Jackson
Original Assignee
Lyondell Chemical Technology L P
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lyondell Chemical Technology L P filed Critical Lyondell Chemical Technology L P
Publication of SG11201804341XA publication Critical patent/SG11201804341XA/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/19—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic hydroperoxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/617—500-1000 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/618—Surface area more than 1000 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/638—Pore volume more than 1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0207—Pretreatment of the support
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0209—Impregnation involving a reaction between the support and a fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0217—Pretreatment of the substrate before coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0238—Impregnation, coating or precipitation via the gaseous phase-sublimation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/12—After treatment, characterised by the effect to be obtained to alter the outside of the crystallites, e.g. selectivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/32—Reaction with silicon compounds, e.g. TEOS, siliconfluoride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/36—Steaming

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Peptides Or Proteins (AREA)

Abstract

International Patent Classification: BOM 37/02 (2006.01) BO1J 35/00 (2006.01) BO1J 21/06 (2006.01) BO1J 35/10 (2006.01) BO1J 21/08 (2006.01) CO7D 301/19 (2006.01) (21) International Application Number: PCT/US2016/062537 A RUTILE 5 MOSE 0 BROOKITE ' , , 9 \".\" \\ \° A 0 \' \ \ A r CATALYST NI (AFTER TESTING) CATALYST N3 rt ,,,. •ni.././e•—•,,.,_,..,: •- • ........_,,. \"'\"•• ;i'''' , . , ..k —41, —. .. .... „pr . 11.• ,,,,,••• 4, •••y y• d 1 % 1 I 1”.1..1. 19 i 01 • I CATALYSTNI (BEFORE TESTING) CATALYSTN2 CATALYSTCI (12) INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property Organization International Bureau 111111111M 11111111111111111111111111111111111111111111111111111111111111R111111111111111 (10) International Publication Number WO 2017/095639 Al WIPOI PCT (43) International Publication Date 8 June 2017 (08.06.2017) TX 77010 (US). ORAN OSMENT, Jenny, M.; c/o Ly- ondellBasell IP Legal Dept., 1221 Mckinney Street, Suite 700, Houston, TX 77010 (US). JACKSON, Debra, L.; c/o LyondellBasell IP Legal Dept., 1221 Mckinney Street, Suite 700, Houston, TX 77010 (US). (74) Agents: KILPATRICK-LEE, Diane, L. et al.; Lyondell- Basell Industries, 1221 Mckinney Street, Houston, TX 77010 (US). (81) Designated States (unless otherwise indicated, for every kind of national protection available): AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JP, KE, KG, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW. (84) Designated States (unless otherwise indicated, for every kind of regional protection available): ARIPO (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, (22) International Filing Date: 17 November 2016 (17.11.2016) (25) Filing Language: English (26) Publication Language: English (30) Priority Data: 62/262,089 2 December 2015 (02.12.2015) US (71) Applicant: LYONDELL CHEMICAL TECHNO- LOGY, L.P. [US/US]; LyondellBasell Tower, 1221 Mckinney, Suite 700, Houston, TX 77010 (US). (72) Inventors: NAGY, Sandor; c/o LyondellBasell IP Legal Dept., 1221 Mckinney Street, Suite 700, Houston, TX 77010 (US). KIMMICH, Barbara; c/o LyondellBasell IP Legal Dept., 1221 Mckinney Street, Suite 700, Houston, TX 77010 (US). YANG, Xueyong; c/o LyondellBasell IP Legal Dept., 1221 Mckinney Street, Suite 700, Houston, [Continued on next page] (54) Title: CATALYSTS CONTAINING BROOKITE TITANIUM (57) : A catalyst composition which comprises ti- tanium, wherein part of the titanium is present as a titanium dioxide phase and at least some of the titanium dioxide phase is in the brookite polymorphic foiin is provided. In some embodiments, the catalyst also comprises a silica sup- port which exhibits a high surface area and pore volume. Methods of preparing the catalyst and its use in an epoxida- tion reaction are also provided. XRD Phase Identification • Rutile, Anatase, and Brooldie 62500 40000 22500 10000 2500 W O 20 17 /095 639 Al 0 25 30 35 40 95 50 55 60 65 70 75 2Thett) WO 2017/095639 Al MIDEDIMOHNOMOIDEMOMMHIMIDIIMENVOIS TZ, UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, Published: TJ, TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, with international search report (Art. 21(3)) LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG).
SG11201804341XA 2015-12-02 2016-11-17 Catalysts containing brookite titanium SG11201804341XA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201562262089P 2015-12-02 2015-12-02
PCT/US2016/062537 WO2017095639A1 (en) 2015-12-02 2016-11-17 Catalysts containing brookite titanium

Publications (1)

Publication Number Publication Date
SG11201804341XA true SG11201804341XA (en) 2018-06-28

Family

ID=57590810

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201804341XA SG11201804341XA (en) 2015-12-02 2016-11-17 Catalysts containing brookite titanium

Country Status (8)

Country Link
US (1) US10017484B2 (en)
EP (1) EP3383533A1 (en)
JP (1) JP6646747B2 (en)
KR (1) KR101992075B1 (en)
CN (1) CN108290148B (en)
BR (1) BR112018011169B1 (en)
SG (1) SG11201804341XA (en)
WO (1) WO2017095639A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11590477B2 (en) 2019-11-04 2023-02-28 Lyondell Chemical Technology, L.P. Titanated catalysts, methods of preparing titanated catalysts, and methods of epoxidation
EP4054759A1 (en) 2019-11-04 2022-09-14 Lyondell Chemical Technology, L.P. Titanated catalysts, methods of preparing titanated catalysts, and methods of epoxidation

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100449421B1 (en) * 1996-07-01 2005-01-24 다우 글로벌 테크놀로지스 인크. Preparation method and catalyst composition of olefin oxide
US6011162A (en) * 1997-05-05 2000-01-04 Arco Chemical Technology, L.P. Epoxidation process using improved heterogeneous catalyst composition
AU756230B2 (en) * 1998-12-16 2003-01-09 Dow Global Technologies Inc. Process for the direct oxidation of olefins to olefin oxides
US6114552A (en) 1999-09-28 2000-09-05 Arco Chemical Technology, L.P. Heterogeneous epoxidation catalyst
EP1138386A1 (en) * 2000-03-29 2001-10-04 Degussa AG Process for the preparation of titanium silicalite shaped body
US8222302B2 (en) * 2005-11-29 2012-07-17 The Hong Kong University Of Science And Technology Titania-silica aerogel monolith with ordered mesoporosity and preparation thereof
BRPI0710696A2 (en) * 2006-05-02 2011-08-23 Shell Internacionale Res Mij B V process for the preparation of a titanium catalyst, catalyst, and, process for the preparation of alkylene oxide
WO2011161412A1 (en) 2010-06-24 2011-12-29 Pq Corporation Catalyst supports, catalysts and their manufacture and use
US8664412B2 (en) 2010-07-19 2014-03-04 Shell Oil Company Epoxidation process
CN102441430B (en) * 2010-10-11 2013-06-12 中国石油化工股份有限公司 Catalyst, preparation method thereof and alkene epoxidation method
WO2013042357A1 (en) * 2011-09-22 2013-03-28 Canon Kabushiki Kaisha White organic el element and illuminating apparatus and display apparatus using the same

Also Published As

Publication number Publication date
BR112018011169B1 (en) 2022-03-29
US20170158655A1 (en) 2017-06-08
KR20180088838A (en) 2018-08-07
JP6646747B2 (en) 2020-02-14
EP3383533A1 (en) 2018-10-10
CN108290148A (en) 2018-07-17
BR112018011169A2 (en) 2018-11-21
KR101992075B1 (en) 2019-06-21
JP2018537280A (en) 2018-12-20
US10017484B2 (en) 2018-07-10
WO2017095639A1 (en) 2017-06-08
CN108290148B (en) 2021-12-24

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