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RU2013395C1 - Glass - Google Patents

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Publication number
RU2013395C1
RU2013395C1 SU4921764A RU2013395C1 RU 2013395 C1 RU2013395 C1 RU 2013395C1 SU 4921764 A SU4921764 A SU 4921764A RU 2013395 C1 RU2013395 C1 RU 2013395C1
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RU
Russia
Prior art keywords
oxide
glass
teo
cdo
pbo
Prior art date
Application number
Other languages
Russian (ru)
Inventor
Юлия Алексеевна Щепочкина
Original Assignee
Юлия Алексеевна Щепочкина
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Юлия Алексеевна Щепочкина filed Critical Юлия Алексеевна Щепочкина
Priority to SU4921764 priority Critical patent/RU2013395C1/en
Application granted granted Critical
Publication of RU2013395C1 publication Critical patent/RU2013395C1/en

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    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/16—Silica-free oxide glass compositions containing phosphorus
    • C03C3/21—Silica-free oxide glass compositions containing phosphorus containing titanium, zirconium, vanadium, tungsten or molybdenum
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/24—Fusion seal compositions being frit compositions having non-frit additions, i.e. for use as seals between dissimilar materials, e.g. glass and metal; Glass solders

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Abstract

FIELD: electronic engineering. SUBSTANCE: the glass comprises (wt % ): 47-56 vanadium; 5-7 molybdenum oxide; 2-4 phosphorus oxide; 1-4 tellurium oxide; 11-18 lead oxide; 10-15 tin oxide; 3-6 cadmium oxide; and 9-12 aluminium oxide. The soldering temperature 480 C. EFFECT: improved properties of the glass. 1 tbl

Description

Изобретение относится к технологии силикатов, в частности стекла, предназначенного преимущественно для использования в электронной технике. The invention relates to the technology of silicates, in particular glass, intended primarily for use in electronic technology.

Известно легкоплавкое стекло, включающее V2O5, ZnO, B2O3, P2O5, ВаО.Fusible glass is known, including V 2 O 5 , ZnO, B 2 O 3 , P 2 O 5 , BaO.

Наиболее близким к предложенному стеклу по химическому составу является стекло, включающее следующие компоненты, мас. % : P2O5 17-23; V2O5 50-58; MoO3 7-9; TeO2 1-8; PbO 11-18. Такое стекло используется, например, для спаивания планшайб. Процесс спаивания производят при температуре 490-500оС.Closest to the proposed glass in chemical composition is glass, comprising the following components, wt. %: P 2 O 5 17-23; V 2 O 5 50-58; MoO 3 7-9; TeO 2 1-8; PbO 11-18. Such glass is used, for example, for soldering faceplates. The soldering process is carried out at a temperature of 490-500 about C.

Известные составы стекла обладают сравнительно высокой температурой спаивания (485-500оС).Known glass compositions have a relatively high soldering temperature (485-500 about C).

Целью изобретения является снижение температуры спаивания. The aim of the invention is to reduce the temperature of soldering.

Для этого в состав стекла дополнительно вводят SnO2, CdO, Al2O3, при этом содержание компонентов должно быть следующим, мас. % : V2O5 47-56; MoO3 5-7; P2O5 2-4; TeO2 1-4; PbO 11-18; SnO2 10-15; CdO 3-6; Al2O3 9-12.For this, SnO 2 , CdO, Al 2 O 3 are additionally introduced into the glass composition, while the content of the components should be as follows, wt. %: V 2 O 5 47-56; MoO 3 5-7; P 2 O 5 2-4; TeO 2 1-4; PbO 11-18; SnO 2 10-15; CdO 3-6; Al 2 O 3 9-12.

В таблице приведены конкретные составы стекла. The table shows the specific compositions of glass.

Температура спаивания описываемого стекла с металлами 480оС.The soldering temperature of the described glass with metals 480 about C.

Взвешенные в указанных количествах компоненты засыпают в корундовые тигли и загружают в силитовую электропечь. Варят стекло при температуре 950-1000оС в течение 0,5-1 ч. В остальном технология получения предложенного стекла не изменяется в сравнении с известной.Weighted in the indicated amounts, the components are poured into corundum crucibles and loaded into a silicon electric furnace. Cook glass at a temperature of 950-1000 ° C for 0.5-1 hours. The rest of the proposed technology for producing glass is not changed in comparison with the known.

Claims (1)

СТЕКЛО, включающее V2O5, MoO3, P2O5, TeO2, PbO, отличающееся тем, что, с целью снижения температуры спаивания, оно дополнительно содержит SnO2, CdO, Al2O3 при следующем соотношении компонентов, мас. % :
V2O5 47 - 56
MoO3 5 - 7
P2O5 2 - 4
TeO2 1 - 4
PbO 11 - 18
SnO2 10 - 15
CdO 3 - 6
Al2 O3 9 - 12GLASS, including V 2 O 5 , MoO 3 , P 2 O 5 , TeO 2 , PbO, characterized in that, in order to reduce the soldering temperature, it additionally contains SnO 2 , CdO, Al 2 O 3 in the following ratio of components, wt . %:
V 2 O 5 47 - 56
MoO 3 5 - 7
P 2 O 5 2 - 4
TeO 2 1 - 4
PbO 11 - 18
SnO 2 10 - 15
CdO 3 - 6
Al 2 O 3 9 - 12
SU4921764 1991-03-25 1991-03-25 Glass RU2013395C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU4921764 RU2013395C1 (en) 1991-03-25 1991-03-25 Glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU4921764 RU2013395C1 (en) 1991-03-25 1991-03-25 Glass

Publications (1)

Publication Number Publication Date
RU2013395C1 true RU2013395C1 (en) 1994-05-30

Family

ID=21566513

Family Applications (1)

Application Number Title Priority Date Filing Date
SU4921764 RU2013395C1 (en) 1991-03-25 1991-03-25 Glass

Country Status (1)

Country Link
RU (1) RU2013395C1 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108298822A (en) * 2018-04-08 2018-07-20 武汉理工大学 A kind of low-melting-point glass powder for vacuum glass sealing and its anode linkage enhance packaging method
RU2782750C1 (en) * 2019-01-30 2022-11-02 ЭлДжи ЭЛЕКТРОНИКС ИНК. Lead-free glass frit fired at low temperatures, paste, and vacuum glass assembly applying said frit

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108298822A (en) * 2018-04-08 2018-07-20 武汉理工大学 A kind of low-melting-point glass powder for vacuum glass sealing and its anode linkage enhance packaging method
RU2782750C1 (en) * 2019-01-30 2022-11-02 ЭлДжи ЭЛЕКТРОНИКС ИНК. Lead-free glass frit fired at low temperatures, paste, and vacuum glass assembly applying said frit

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