RU2013124654A - AMINOAMIDES IN THE SERIES OF BACTERIOCHLOROPHYL ALPHA WITH PHOTODYNAMIC ACTIVITY AND METHOD FOR PRODUCING THEM - Google Patents
AMINOAMIDES IN THE SERIES OF BACTERIOCHLOROPHYL ALPHA WITH PHOTODYNAMIC ACTIVITY AND METHOD FOR PRODUCING THEM Download PDFInfo
- Publication number
- RU2013124654A RU2013124654A RU2013124654/04A RU2013124654A RU2013124654A RU 2013124654 A RU2013124654 A RU 2013124654A RU 2013124654/04 A RU2013124654/04 A RU 2013124654/04A RU 2013124654 A RU2013124654 A RU 2013124654A RU 2013124654 A RU2013124654 A RU 2013124654A
- Authority
- RU
- Russia
- Prior art keywords
- aminoamides
- series
- producing
- bacteriochlorophyll
- bacteriochlorophyl
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical class NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000002028 Biomass Substances 0.000 claims abstract 2
- 241000191023 Rhodobacter capsulatus Species 0.000 claims abstract 2
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical class OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000005903 acid hydrolysis reaction Methods 0.000 claims abstract 2
- 230000000259 anti-tumor effect Effects 0.000 claims abstract 2
- 238000002955 isolation Methods 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims abstract 2
- 150000004702 methyl esters Chemical class 0.000 claims abstract 2
- 108010070075 Bacteriochlorophyll A Proteins 0.000 claims 3
- ZSERVQBSOBTXFV-DHHJBRQQSA-M bacteriochlorophyll a Chemical class C1([C@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC([C@@H](CC)[C@@H]3C)=[N+]4C3=CC3=C(C(C)=O)C(C)=C5N3[Mg]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ZSERVQBSOBTXFV-DHHJBRQQSA-M 0.000 claims 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- 108010003118 Bacteriochlorophylls Proteins 0.000 abstract 1
- DSJXIQQMORJERS-AGGZHOMASA-M bacteriochlorophyll a Chemical class C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC([C@H](CC)[C@H]3C)=[N+]4C3=CC3=C(C(C)=O)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 DSJXIQQMORJERS-AGGZHOMASA-M 0.000 abstract 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1. Аминоамиды в ряду бактериохлорофиллаобщей формулыгде n=2-10,обладающие фотоиндуцированной противоопухолевой активностью.2. Способ получения аминоамидов по п.1, включающий выделение бактериохлорофиллаиз биомассы бактерий Rhodobacter Capsulatus, двухстадийный кислотный гидролиз бактериохлорофилларастворами 15%-ной соляной и 80%-ной трифторуксусной кислот, обработку метилового эфира бактериофеофорбидадиаминоалканами в пиридине.1. Aminoamides in the series of bacteriochlorophyll of the general formula where n = 2-10, with photo-induced antitumor activity. 2. The method of producing aminoamides according to claim 1, including the isolation of bacteriochlorophyllium from the biomass of bacteria Rhodobacter Capsulatus, two-stage acid hydrolysis of bacteriochlorophyllum with solutions of 15% hydrochloric and 80% trifluoroacetic acids, treatment of methyl ester of bacteriofeoforbidadiaminoalkanes in pyridine.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2013124654/04A RU2548675C9 (en) | 2013-05-29 | 2013-05-29 | Amino amides in bacteriochlorophyll a series, having photodynamic activity and method for production thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2013124654/04A RU2548675C9 (en) | 2013-05-29 | 2013-05-29 | Amino amides in bacteriochlorophyll a series, having photodynamic activity and method for production thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| RU2013124654A true RU2013124654A (en) | 2014-12-10 |
| RU2548675C2 RU2548675C2 (en) | 2015-04-20 |
| RU2548675C9 RU2548675C9 (en) | 2015-11-10 |
Family
ID=53289665
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2013124654/04A RU2548675C9 (en) | 2013-05-29 | 2013-05-29 | Amino amides in bacteriochlorophyll a series, having photodynamic activity and method for production thereof |
Country Status (1)
| Country | Link |
|---|---|
| RU (1) | RU2548675C9 (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2680523C1 (en) * | 2017-12-01 | 2019-02-22 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Ивановский государственный химико-технологический университет" (ИГХТУ) | WATER-SOLUBLE DERIVATIVE OF CHLOROPHYLL α MODIFIED BY MYRISTIC ACID FRAGMENT |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PT1753457T (en) * | 2004-06-07 | 2016-11-10 | Yeda Res & Dev | Cationic bacteriochlorophyll derivatives and uses thereof |
| US20080138278A1 (en) * | 2006-08-23 | 2008-06-12 | Yeda Research & Development Co., Ltd. | Conjugates of rgd peptides and porphyrin or (bacterio) chlorohyll photosynthesizers and their uses |
| RU2416614C2 (en) * | 2007-12-05 | 2011-04-20 | Гелий Васильевич Пономарев | Photosensitiser and preparation method thereof |
| RU2479586C1 (en) * | 2012-03-13 | 2013-04-20 | Федеральное государственное унитарное предприятие "Государственный научный центр "Научно-исследовательский институт органических полупродуктов и красителей" (ФГУП "ГНЦ "НИОПИК") | Method of producing non-metal tetraazachlorins |
-
2013
- 2013-05-29 RU RU2013124654/04A patent/RU2548675C9/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| RU2548675C9 (en) | 2015-11-10 |
| RU2548675C2 (en) | 2015-04-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| TC4A | Altering the group of invention authors |
Effective date: 20151013 |
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| TH4A | Reissue of patent specification | ||
| TK4A | Correction to the publication in the bulletin (patent) |
Free format text: AMENDMENT TO CHAPTER -FG4A- IN JOURNAL: 11-2015 FOR TAG: (54) |
|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20180530 |