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RU2012124187A - METHOD FOR PRODUCING NON-TEXTURED ELECTROTECHNICAL STEEL WITH HIGH MAGNETIC INDUCTION - Google Patents

METHOD FOR PRODUCING NON-TEXTURED ELECTROTECHNICAL STEEL WITH HIGH MAGNETIC INDUCTION Download PDF

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RU2012124187A
RU2012124187A RU2012124187/02A RU2012124187A RU2012124187A RU 2012124187 A RU2012124187 A RU 2012124187A RU 2012124187/02 A RU2012124187/02 A RU 2012124187/02A RU 2012124187 A RU2012124187 A RU 2012124187A RU 2012124187 A RU2012124187 A RU 2012124187A
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temperature
steel
strip
rolled
cold
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RU2527827C2 (en
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Цзытао ВАН
Бо ВАН
Шишу СЕ
Бинчжун ЦЗИНЬ
Айхуа МА
Лиан ЦЗОУ
Юйхуа ЧЖУ
Чжаньюань ХУ
Сяо ЧЭНЬ
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Баошан Айрон Энд Стил Ко., Лтд.
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D11/00Continuous casting of metals, i.e. casting in indefinite lengths
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/008Heat treatment of ferrous alloys containing Si
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/001Ferrous alloys, e.g. steel alloys containing N
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/002Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/004Very low carbon steels, i.e. having a carbon content of less than 0,01%
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/12Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/14Ferrous alloys, e.g. steel alloys containing titanium or zirconium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/12Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
    • H01F1/14Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
    • H01F1/16Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of sheets

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Dispersion Chemistry (AREA)
  • Power Engineering (AREA)
  • Manufacturing Of Steel Electrode Plates (AREA)
  • Soft Magnetic Materials (AREA)

Abstract

1. Способ производства нетекстурированной электротехнической стали с высокой магнитной индукцией, состоящий из следующих процедур:1) Выплавка и отливкаХимический состав нетекстурированной электротехнический стали в процентах по весу таков: Si 0,1~1%, Al 0,005~1,0%, С≤0,004%, Mn 0,10~1,50%, P≤0,2%, S≤0,005%, N≤0,002, Nb+V+Ti≤0,006%, a остальное составляет Fe и неустранимые включения; нетекстурированную электротехническую сталь подвергают выплавке и вторичному рафинированию в конвертере или электрической печи, а затем отливают в виде стального прутка;2) Горячая прокаткаСтальной пруток нагревают до температуры в диапазоне 1150~1200°C и вымачивают при этой температуре в течение определенного времени, после чего при помощи горячей прокатки при температуре отделочной прокатки 830~900°C получают стальную полосу; при охлаждении до температуры ≥570°C полоса закручивается в рулон;3) ПравкаГорячекатаную полосу подвергают холодной прокатке с коэффициентом обжатия 2~5%;4) НормализацияПосле холодной прокатки горячекатаную полосу подвергают непрерывной нормализации при температуре не ниже 950°C, и выдерживают при этой температуре в течение 30~180 сек;5) Травление и холодная прокаткаНормализованную полосу подвергают травлению, а затем несколько раз проводят холодную прокатку с суммарным коэффициентом обжатия 70~80% до получения листа холоднокатаной стали с толщиной итогового изделия;6) ОтжигХолоднокатаный лист быстро нагревают и отжигают, при этом темп роста температуры составляет не менее 100°C/сек, нагрев выполняют до температуры в диапазоне 800~100°C, и выдерживают сталь при этой температуре в течение 5~60 сек, после чего медленно охлаждают до температуры 600~750°C при ско�1. Method for the production of non-oriented electrical steel with high magnetic induction, consisting of the following procedures: 1) Smelting and casting The chemical composition of non-oriented electrical steel in percentage by weight is as follows: Si 0.1 ~ 1%, Al 0.005 ~ 1.0%, C≤ 0.004%, Mn 0.10 ~ 1.50%, P≤0.2%, S≤0.005%, N≤0.002, Nb + V + Ti≤0.006%, and the rest is Fe and fatal inclusions; non-oriented electrical steel is smelted and re-refined in a converter or electric furnace, and then cast into a steel bar; 2) Hot rolling The steel bar is heated to a temperature in the range of 1150 ~ 1200 ° C and soaked at this temperature for a certain time, and then at a steel strip is obtained by hot rolling at a finishing rolling temperature of 830 ~ 900 ° C; when cooled to a temperature of ≥570 ° C, the strip is rolled into a coil; 3) Straightening Hot-rolled strip is subjected to cold rolling with a reduction ratio of 2 ~ 5%; 4) Normalization After cold rolling, the hot-rolled strip is subjected to continuous normalization at a temperature not lower than 950 ° C, and kept at this temperature for 30 ~ 180 sec; 5) Pickling and cold rolling The normalized strip is pickled and then cold rolled several times with a total reduction ratio of 70 ~ 80% to obtain a cold rolled steel sheet with the thickness of the final product; 6) Annealing The cold rolled sheet is rapidly heated and annealed, while the rate of temperature rise is not less than 100 ° C / sec, heating is performed to a temperature in the range of 800 ~ 100 ° C, and the steel is kept at this temperature for 5 ~ 60 sec, after which it is slowly cooled to a temperature of 600 ~ 750 ° C at speed

Claims (2)

1. Способ производства нетекстурированной электротехнической стали с высокой магнитной индукцией, состоящий из следующих процедур:1. Method for the production of non-textured electrical steel with high magnetic induction, consisting of the following procedures: 1) Выплавка и отливка1) Smelting and casting Химический состав нетекстурированной электротехнический стали в процентах по весу таков: Si 0,1~1%, Al 0,005~1,0%, С≤0,004%, Mn 0,10~1,50%, P≤0,2%, S≤0,005%, N≤0,002, Nb+V+Ti≤0,006%, a остальное составляет Fe и неустранимые включения; нетекстурированную электротехническую сталь подвергают выплавке и вторичному рафинированию в конвертере или электрической печи, а затем отливают в виде стального прутка;The chemical composition of non-textured electrical steel in percent by weight is as follows: Si 0.1 ~ 1%, Al 0.005 ~ 1.0%, C≤0.004%, Mn 0.10 ~ 1.50%, P≤0.2%, S ≤0.005%, N≤0.002, Nb + V + Ti≤0.006%, and the rest is Fe and fatal inclusions; non-textured electrical steel is subjected to smelting and secondary refining in a converter or an electric furnace, and then cast in the form of a steel bar; 2) Горячая прокатка2) Hot rolling Стальной пруток нагревают до температуры в диапазоне 1150~1200°C и вымачивают при этой температуре в течение определенного времени, после чего при помощи горячей прокатки при температуре отделочной прокатки 830~900°C получают стальную полосу; при охлаждении до температуры ≥570°C полоса закручивается в рулон;The steel bar is heated to a temperature in the range of 1150 ~ 1200 ° C and soaked at this temperature for a certain time, after which, using hot rolling at a finishing rolling temperature of 830 ~ 900 ° C, a steel strip is obtained; when cooled to a temperature of ≥570 ° C, the strip is twisted into a roll; 3) Правка3) Edit Горячекатаную полосу подвергают холодной прокатке с коэффициентом обжатия 2~5%;The hot rolled strip is cold rolled with a reduction ratio of 2 ~ 5%; 4) Нормализация4) Normalization После холодной прокатки горячекатаную полосу подвергают непрерывной нормализации при температуре не ниже 950°C, и выдерживают при этой температуре в течение 30~180 сек;After cold rolling, the hot-rolled strip is subjected to continuous normalization at a temperature not lower than 950 ° C, and maintained at this temperature for 30 ~ 180 sec; 5) Травление и холодная прокатка5) Pickling and cold rolling Нормализованную полосу подвергают травлению, а затем несколько раз проводят холодную прокатку с суммарным коэффициентом обжатия 70~80% до получения листа холоднокатаной стали с толщиной итогового изделия;The normalized strip is etched and then cold rolled several times with a total reduction ratio of 70 ~ 80% to obtain a sheet of cold rolled steel with a thickness of the final product; 6) Отжиг6) Annealing Холоднокатаный лист быстро нагревают и отжигают, при этом темп роста температуры составляет не менее 100°C/сек, нагрев выполняют до температуры в диапазоне 800~100°C, и выдерживают сталь при этой температуре в течение 5~60 сек, после чего медленно охлаждают до температуры 600~750°C при скорости охлаждения 3~15°C/сек.The cold-rolled sheet is quickly heated and annealed, while the temperature growth rate is at least 100 ° C / s, heating is performed to a temperature in the range of 800 ~ 100 ° C, and the steel is held at this temperature for 5 ~ 60 seconds, after which it is slowly cooled to a temperature of 600 ~ 750 ° C at a cooling rate of 3 ~ 15 ° C / s. 2. Способ по п.1, отличающийся тем, что атмосфера отжига в процентах по объему содержит Н2 в количестве 30%~70%+N2 в количестве 70%~30%, точка росы ≤ -25°C. 2. The method according to claim 1, characterized in that the annealing atmosphere as a percentage by volume contains H 2 in an amount of 30% ~ 70% + N 2 in an amount of 70% ~ 30%, dew point ≤ -25 ° C.
RU2012124187/02A 2010-10-25 2011-04-14 Production of random-orientation electric steel with high magnetic induction RU2527827C2 (en)

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CN201010517872.7 2010-10-25
CN2010105178727A CN102453837B (en) 2010-10-25 2010-10-25 Method for preparing non-oriented silicon steel with high magnetic induction
PCT/CN2011/072775 WO2012055215A1 (en) 2010-10-25 2011-04-14 Method for manufacturing non-oriented silicon steel with high-magnetic induction

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JP (1) JP2013513724A (en)
KR (1) KR101404101B1 (en)
CN (1) CN102453837B (en)
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