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PT89776A - Processo para a preparacao de solucoes aquosas de acido 2-hidroxi-4-metiltio-bitirico - Google Patents

Processo para a preparacao de solucoes aquosas de acido 2-hidroxi-4-metiltio-bitirico

Info

Publication number
PT89776A
PT89776A PT89776A PT8977689A PT89776A PT 89776 A PT89776 A PT 89776A PT 89776 A PT89776 A PT 89776A PT 8977689 A PT8977689 A PT 8977689A PT 89776 A PT89776 A PT 89776A
Authority
PT
Portugal
Prior art keywords
hydroxy
acid
organic phase
bythric
methylthyl
Prior art date
Application number
PT89776A
Other languages
English (en)
Other versions
PT89776B (pt
Inventor
Javier Azagra Hernandez
Luis Ruiz Moreno
Original Assignee
Desarrollo Tecnico Ind
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Desarrollo Tecnico Ind filed Critical Desarrollo Tecnico Ind
Publication of PT89776A publication Critical patent/PT89776A/pt
Publication of PT89776B publication Critical patent/PT89776B/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
PT89776A 1988-02-22 1989-02-21 Processo para a preparacao de solucoes aquosas de acido 2-hidroxi-4-metiltio-bitirico PT89776B (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES8800496A ES2005784A6 (es) 1988-02-22 1988-02-22 Un procedimiento para preparar soluciones acuosas de acido 2-hidroxi-4-metil-tiobutirico.

Publications (2)

Publication Number Publication Date
PT89776A true PT89776A (pt) 1989-10-04
PT89776B PT89776B (pt) 1994-03-31

Family

ID=8254970

Family Applications (1)

Application Number Title Priority Date Filing Date
PT89776A PT89776B (pt) 1988-02-22 1989-02-21 Processo para a preparacao de solucoes aquosas de acido 2-hidroxi-4-metiltio-bitirico

Country Status (12)

Country Link
US (1) US4912257A (pt)
EP (1) EP0330527B1 (pt)
AT (1) ATE80871T1 (pt)
CA (1) CA1308419C (pt)
DE (1) DE68902934T2 (pt)
DK (1) DK175368B1 (pt)
ES (2) ES2005784A6 (pt)
GR (1) GR3005881T3 (pt)
HK (1) HK17793A (pt)
IE (1) IE63393B1 (pt)
PT (1) PT89776B (pt)
SG (1) SG125692G (pt)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY109603A (en) * 1992-05-21 1997-03-31 Daicel Chem Process for producing 2-hydroxy-4-methylthiobutanoic acid
US5498790A (en) * 1993-06-09 1996-03-12 Novus International, Inc. Regeneration of sulfuric acid from sulfate by-products of 2-hydroxy-4-(methylthio)butyric acid manufacture
KR100389971B1 (ko) * 1994-07-11 2004-05-17 데구사 아게 2-하이드록시-4-메틸티오부티르산(mha)의회수방법및mha를포함하는동물사료첨가제용혼합물
DE4428608C1 (de) * 1994-08-12 1996-02-29 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
FR2733231B1 (fr) * 1995-04-24 1997-07-04 Rhone Poulenc Nutrition Animal Procede de condensation de l'acide cyanhydrique avec un aldehyde
US5583243A (en) * 1995-05-19 1996-12-10 Zinpro Corporation Salts of alpha-hydroxy aliphatic carboxylic acids and uses thereof
DE69615183T2 (de) 1995-06-07 2002-05-29 Novus International, Inc. Kontinuerliches hydrolyse-verfahren zur herstellung von 2-hydroxy-4-methylthiobutansäure oder salze davon
US5856567A (en) * 1995-06-07 1999-01-05 Novus International, Inc. Continuous hydrolysis process for preparing 2-hydroxy-4-methylthiobutanioc acid or salts thereof
DE19548538C2 (de) * 1995-12-23 1997-12-18 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
JP3804210B2 (ja) * 1997-03-04 2006-08-02 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法
DE19754562A1 (de) * 1997-12-09 1999-06-10 Degussa Verfahren zur Rückgewinnung von Schwefelsäure aus schwefelhaltigen Nebenprodukten eines Prozesses zur Herstellung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
FR2780969B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de separation de l'acide hydroxymethylthiobutyrique
FR2780968B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de preparation de l'acide hydroxymethylthiobutyrique
RU2213729C2 (ru) * 1999-02-03 2003-10-10 Сумитомо Кемикал Компани, Лимитед Способ получения 2-гидрокси-4-метилтиобутановой кислоты
US6342651B1 (en) 1999-08-05 2002-01-29 Novus International, Inc. Reductive combustion of ammonium salts of sulfuric acid
US6649794B2 (en) * 2000-02-18 2003-11-18 Sumitomo Chemical Company, Limited Method for producing 2-Hydroxy-4-Methylthiobutanoic Acid
MXPA06009797A (es) * 2004-02-26 2007-08-14 Tasker Products Ip Holdings Co Composicion anti-microbiana para tratamiento pre-cosecha y post-cosecha de plantas y animales.
JP4696496B2 (ja) * 2004-08-18 2011-06-08 住友化学株式会社 2−ヒドロキシ−4−メチルチオ酪酸の製造方法
DE102004041250A1 (de) * 2004-08-26 2006-03-02 Degussa Ag Herstellung von 2-Hydroxy-4-Methylthiobuttersäure
JP4896548B2 (ja) * 2006-03-10 2012-03-14 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法および製造装置
JP4948002B2 (ja) * 2006-03-10 2012-06-06 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法および製造装置
KR101907230B1 (ko) * 2011-02-23 2018-10-11 에보니크 데구사 게엠베하 저장 안정성 2-히드록시-4-(메틸티오)부티르산 니트릴
MX341595B (es) 2011-02-23 2016-08-26 Evonik Degussa Gmbh Metodo para producir 2-hidroxi-4-(metiltio)butironitrilo a partir de 3-(metiltio)propanal y cianuro de hidrogeno.
CN103420883A (zh) * 2013-08-28 2013-12-04 重庆紫光化工股份有限公司 利用粗氢氰酸气体制备2-羟基-4-甲硫基丁腈的方法
CN103641754B (zh) * 2013-11-19 2016-08-24 宁夏紫光天化蛋氨酸有限责任公司 药用d,l-2-羟基-4-甲硫基丁酸金属螯合物的制备方法
CN104262216A (zh) * 2014-10-15 2015-01-07 重庆紫光化工股份有限公司 一种2-羟基-4-甲硫基丁酸的制备方法
CN105130861A (zh) * 2015-07-28 2015-12-09 重庆紫光国际化工有限责任公司 氰醇水解法合成蛋氨酸羟基类似物的分离纯化方法
FR3064006B1 (fr) 2017-03-16 2019-03-29 Adisseo France S.A.S. Procede de fabrication de l'acide-2-hydroxy-4-methylthio-butyrique
CN111116437B (zh) 2018-11-01 2021-02-05 山东新和成氨基酸有限公司 制备2-羟基-4-甲硫基丁酸及其中间体的方法和装置
CN109232336A (zh) * 2018-11-09 2019-01-18 禄丰天宝磷化工有限公司 一种清洁环保的蛋氨酸羟基类似物生产方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA694650A (en) * 1964-09-22 Mark Victor Preparation of 4-(alkylthio)-2-hydroxybutyric acids
CA694610A (en) * 1964-09-22 J. Wineman Robert Preparation of salts of 2-hydroxy-4-alkylthiobutyric acid
GB722024A (en) * 1950-10-31 1955-01-19 Monsanto Chemicals Production of alpha-hydroxy-gamma-mercapto-carboxylic acids and salts thereof and compositions containing the same
US2745745A (en) * 1952-10-30 1956-05-15 Monsanto Chemicals Poultry feed
US2938053A (en) * 1955-12-29 1960-05-24 Monsanto Chemicals Amino acid analogues
CH385823A (de) * 1959-09-01 1964-12-31 Inventa Ag Verfahren zur Herstellung des Calciumsalzes der a-Oxy-y-methylthio-buttersäure
BE611435A (fr) * 1960-12-14 1962-06-12 Stamicarbon Procédé de préparation de sels métalliques d'acide alpha-hydroxy- gamma -méthylmercaptobutyrique
GB1353832A (en) * 1971-08-03 1974-05-22 Degussa Sulphonium compounds of alpha-hydroxy-gamma-alkyl-mercapto butyric acid
US3773927A (en) * 1971-12-20 1973-11-20 Du Pont Preparation of an aqueous slurry of ammonium chloride and methylmercapto-hydroxybutyric acid
US4353924A (en) * 1979-09-04 1982-10-12 Monsanto Company Animal feed supplement having reduced corrosion characteristics
US4524077A (en) * 1983-11-14 1985-06-18 Monsanto Company Liquid 2-hydroxy-4-methylthiobutyric acid and process for the preparation thereof
EP0143100B1 (en) * 1983-11-14 1987-08-05 Monsanto Company Process for the preparation of liquid 2-hydroxy-methylthiobutyric acid

Also Published As

Publication number Publication date
ES2045478T3 (es) 1994-01-16
SG125692G (en) 1993-02-19
IE890547L (en) 1989-08-22
DE68902934D1 (de) 1992-10-29
EP0330527B1 (fr) 1992-09-23
HK17793A (en) 1993-03-12
DK78889A (da) 1989-08-22
IE63393B1 (en) 1995-04-19
EP0330527A1 (fr) 1989-08-30
DK78889D0 (da) 1989-02-21
DE68902934T2 (de) 1993-04-08
ES2005784A6 (es) 1989-03-16
ATE80871T1 (de) 1992-10-15
US4912257A (en) 1990-03-27
DK175368B1 (da) 2004-09-13
PT89776B (pt) 1994-03-31
CA1308419C (fr) 1992-10-06
GR3005881T3 (pt) 1993-06-07

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Legal Events

Date Code Title Description
FG3A Patent granted, date of granting

Effective date: 19930913

PC3A Transfer or assignment

Free format text: 940825 RHONE-POULENC NUTRITION ANIMALE FR

PC3A Transfer or assignment

Owner name: ADISSEO IRELAND LIMITED, IE

Effective date: 20041129

PD3A Change of proprietorship

Owner name: AVENTIS ANIMAL NUTRITION SA, FR

Effective date: 20041129

Owner name: RHONE-POULENC ANINAL NUTRITION S.A., FR

Effective date: 20041129

TE3A Change of address (patent)

Owner name: AVENTIS ANIMAL NUTRITION S. A., FR

Effective date: 20041129

Owner name: RHONE-POULENC NUTRITION ANIMALE, SA., FR

Effective date: 20041129

MM4A Annulment/lapse due to non-payment of fees, searched and examined patent

Free format text: LAPSE DUE TO NON-PAYMENT OF FEES

Effective date: 20080313

MM4A Annulment/lapse due to non-payment of fees, searched and examined patent

Free format text: MAXIMUM VALIDITY LIMIT REACHED

Effective date: 20090221