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KR970704859A - Vi 선택성 촉매를 사용하여 윤활유를 제조하는 방법 - Google Patents

Vi 선택성 촉매를 사용하여 윤활유를 제조하는 방법 Download PDF

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KR970704859A
KR970704859A KR1019970700639A KR19970700639A KR970704859A KR 970704859 A KR970704859 A KR 970704859A KR 1019970700639 A KR1019970700639 A KR 1019970700639A KR 19970700639 A KR19970700639 A KR 19970700639A KR 970704859 A KR970704859 A KR 970704859A
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pore diameter
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제임스 엔. 짐머
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터너 더블유. 케이쓰
세브런 유.에스.에이. 인코퍼레이티드
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C10G47/18—Crystalline alumino-silicate carriers the catalyst containing platinum group metals or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/301—Boiling range
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/10—Lubricating oil

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Catalysts (AREA)
  • Lubricants (AREA)

Abstract

높은 점도 지수 선택성 및 낮은 오염률을 가진 촉매로 양질의 윤활유를 제조하는 방법을 제공한다. 촉매는 소량의 제올라이트를 함유하며 큰 기공이 상당량있는 것으로 특징되는 기공 크기 분포를 갖는다.

Description

VI 선택성 촉매를 사용하여 윤활유를 제조하는 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (23)

  1. 수소화분해 조건하에서 제올라이트, 수소화 성분 및 무기 산화물 매트릭스 물질을 포함하고, 기공부피가 약 0.25 내지 약 0.60cm3/g이고 평균기공직경이 약 40Å 내지 약 1OOÅ이며 기공부피의 약 5%이상은 기공직경이 200Å이상인 촉매를 함탄화수소 공급원료와 접촉시키는 것을 특징으로 하는 윤활유 기제 공급원료의 제조방법.
  2. 제 1 항에 있어서, 평균기공직경이 약 40 내지 80Å인 제조방법.
  3. 제 1 항에 있어서,기공부피의 약 10%이상은 기공직경이 200Å이상인 제조방법.
  4. 제 1 항에 있어서, 기공부피의 약 15%이상은 기공직경이 200Å이상인 제조방법.
  5. 제 4 항에 있어서, 기공부피의 약 1%이상은 기공직경이 1OOOÅ이상인 제조방법.
  6. 제 1 항에 있어서, 제올라이트가 제올라이트 Y, 탈알루미나화된 제올라이트 Y 및 초안정(ultrastable) 제올라이트 Y인 제조방법.
  7. 제 1 항에 있어서, 촉매가 제올라이트를 약 1 내지 약 20 중량% 포함하는 제조방법.
  8. 제 1 항에 있어서, 촉매가 제올라이트를 약 1 내지 약 10중량% 포함하는 제조방법.
  9. 제 1 항에 있어서, 제올라이트는 Si02/A1203의 몰비가 약 5 내지 약 100인 제조방법.
  10. 제 1 항에 있어서, 제올라이트는 Si02/A1203의 몰비가 약 5 내지 약 60인 제조방법.
  11. 제 1 항에 있어서, 촉매가 수소화 성분을 약 0.01 내지 약 45중량% 함유하는 제조방법.
  12. 제 11 항에 있어서, 수소화성분이 금속 삼산화물로서 텅스텐, 몰리브덴, 및 이의 결합물로부터 선택된 하나이상의 VIB족 금속의 약 5 내지 약 30중량%를 함유하는 제조방법.
  13. 제 12 항에 있어서, 수소화성분이 금속 일산화물로서 니켈, 코발트 및 이의 결합물로부터 선택된 하나이상의 VⅢ족 염기 금속의 약 1 내지 약 15중량%를 함유하는 제조방법.
  14. 제 1 항에 있어서, 촉매가 무기 산화물 매트릭스 물질을 약 30 내지 90중량%를 함유하는 제조방법.
  15. 제 1 항에 있어서, 무기산화물 매트릭스 물질이 알루미나, 실리카 알루미나 및 이의 결합물로부터 선택되는 제조방법.
  16. 제 1 항에 있어서, 함탄화수소 공급원료가 정상 비점범위가 약 350 내지 590℃인 진공가스오일인 제조방법.
  17. 제 1 항에 있어서, 함탄화수소 공급원료가 정상 비점 범위가 약 480 내지 650℃인 탈아스팔트화된 잔유인 제조방법.
  18. 제 1 항에 있어서, 수소화분해 조건이 400℉(204℃) 내지 950℉(510℃)의 온도, 500 내지 3500psig(3550 내지 24200 KPa abs)압력, O.1 내지 20.0의 액체 시간당 공간속도, 및 함탄화수소 공급원료 1 밸럴당 200 내지 20,000 SCF 수소(43-4300 std H2/kg 원료)의 총 수소공급을 포함하는 제조방법.
  19. 제 1 항에 있어서, 약 10 내지 약 80 중량% 전화가 제공되는 제조방법.
  20. 제 1 항에 있어서, 윤활유 기제 공급원료중 650℉(343℃)이상 분획이 탈납, 수소화마무리, 또는 이를 결합하여 수행되는 제조방법.
  21. 제 20 항에 있어서, 탈납이 촉매 탈납 또는 용매탈납 조건에서 수행되는 제조방법.
  22. 수소화분해 조건하에서 a) 파우자사이트 구조를 갖는 제올라이트가 약 1 내지 10 중량%이고; b) 금속일산화물로서 니켈, 코발트 및 이의 결합물로부터 선택된 하나 이상의 VⅢ족 금속이 약 1 내지 15 중량% 이고 금속 삼산화물로서 텅스텐, 몰리브덴 및 이의 결합물로 선택된 하나이상의 ⅥB 족 금속이 약 5 내지 30중량%이고; c) 무형의 실리카-알루미나 매트릭스 물질이 약 45 내지 75중량%이고; d) 100중량%를 만들기 위하여 충분한 알루미나 지지체 물질을 포함하며, 기공부피가 약 0.25 내지 약 0.45cm3/g이고 평균기공직경이 약 40Å 내지 약 1OOÅ이며 기공부피의 약 5%이상은 기공직경이 200Å이상안 촉매를 정상비점 범위가 약 350 내지 590℃의 진공 가스오일인 함탄화수소 공급원료와 접촉시키는 것을 특징으로 하는 윤활유 기제 공급원료의 제조방법.
  23. a) 수소화전화 조건하에서 함탄화수소 공급원료를 수소화전화 촉매와 접촉시켜 lOOppm이하의 질소함량을 갖는 수소화처리된 생성물을 제조하고; b) 수소화분해 조건하에서 수소화처리된 생성물을 파우자사이트 구조, 수소화성분, 및 실리카-알루미나 매트릭스 물질를 포함하고, 기공부피가 약 0.25 내지 약 0.60cm3/g이고 평균기공직경이 약 40Å 내지 약 1OOÅ이며 기공부피의 약 5%이상은 기공직경이 200Å이상인 촉매와 접촉시키는 것을 특징으르 하는 윤활유 기제 공급원료의 제조방법.
KR1019970700639A 1994-08-01 1995-06-20 Vi 선택성 촉매를 사용하여 윤활유를 제조하는 방법 KR970704859A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US08/284,933 1994-08-01
US08/284,933 US5543035A (en) 1994-08-01 1994-08-01 Process for producing a high quality lubricating oil using a VI selective catalyst
PCT/US1995/008018 WO1996004354A1 (en) 1994-08-01 1995-06-20 Lubricating oil production with vi-selective catalyst

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KR970704859A true KR970704859A (ko) 1997-09-06

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KR1019970700639A KR970704859A (ko) 1994-08-01 1995-06-20 Vi 선택성 촉매를 사용하여 윤활유를 제조하는 방법

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Country Link
US (1) US5543035A (ko)
EP (1) EP0775184B2 (ko)
JP (1) JPH10503542A (ko)
KR (1) KR970704859A (ko)
CN (1) CN1046544C (ko)
AT (1) ATE281504T1 (ko)
AU (1) AU692574B2 (ko)
BR (1) BR9508454A (ko)
CA (1) CA2194975A1 (ko)
CZ (1) CZ4397A3 (ko)
DE (1) DE69533716T3 (ko)
FI (1) FI970395A (ko)
HU (1) HU218039B (ko)
PL (1) PL179172B1 (ko)
RU (1) RU2140966C1 (ko)
SK (1) SK10697A3 (ko)
WO (1) WO1996004354A1 (ko)

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CA2194975A1 (en) 1996-02-15
JPH10503542A (ja) 1998-03-31
FI970395A0 (fi) 1997-01-30
US5543035A (en) 1996-08-06
SK10697A3 (en) 1997-06-04
EP0775184B2 (en) 2012-05-02
EP0775184A4 (en) 1998-11-04
AU2909695A (en) 1996-03-04
CN1154130A (zh) 1997-07-09
PL318267A1 (en) 1997-05-26
CZ4397A3 (en) 1997-06-11
CN1046544C (zh) 1999-11-17
FI970395A (fi) 1997-01-30
RU2140966C1 (ru) 1999-11-10
WO1996004354A1 (en) 1996-02-15
EP0775184B1 (en) 2004-11-03
HUT77419A (hu) 1998-04-28
AU692574B2 (en) 1998-06-11
EP0775184A1 (en) 1997-05-28
DE69533716D1 (de) 2004-12-09
DE69533716T3 (de) 2012-09-20
HU218039B (hu) 2000-05-28
ATE281504T1 (de) 2004-11-15
BR9508454A (pt) 1998-07-14
DE69533716T2 (de) 2006-02-02
PL179172B1 (pl) 2000-07-31

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