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KR960705608A - 무수, 자유 유동 당 계면 활성제 분말의 제조 방법(process for producing anhydrous pourable sugar tenside powders) - Google Patents

무수, 자유 유동 당 계면 활성제 분말의 제조 방법(process for producing anhydrous pourable sugar tenside powders)

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Publication number
KR960705608A
KR960705608A KR1019960702663A KR19960702663A KR960705608A KR 960705608 A KR960705608 A KR 960705608A KR 1019960702663 A KR1019960702663 A KR 1019960702663A KR 19960702663 A KR19960702663 A KR 19960702663A KR 960705608 A KR960705608 A KR 960705608A
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South Korea
Prior art keywords
alkyl
process according
carbon atoms
radical containing
alkaline earth
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KR1019960702663A
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English (en)
Inventor
레제 빌프리트
파프 카틀렌
브라이츠케 빌리
자이펄 베르너
테스만 홀거
하인쯔 슈미트 칼
파브리 베른트
Original Assignee
게오르그 챠이트ㆍ요한 글라슬
헨켈 코만디트게젤샤프트 아우프 아크티엔
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Priority claimed from DE4340015A external-priority patent/DE4340015C2/de
Application filed by 게오르그 챠이트ㆍ요한 글라슬, 헨켈 코만디트게젤샤프트 아우프 아크티엔 filed Critical 게오르그 챠이트ㆍ요한 글라슬
Publication of KR960705608A publication Critical patent/KR960705608A/ko

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42—Amides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/16—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms
    • C07C233/17—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/18—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a hydrogen atom or to a carbon atom of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/16—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms
    • C07C233/17—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/20—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a carbon atom of an acyclic unsaturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/017—Mixtures of compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
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    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
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    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters

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Abstract

무수, 자유 유동 당 계면 활성 분말을 100~225℃의 온도에서 과열 증기로써(a1) 알킬 및/또는 알케닐 올리고글리코시드 및/또는 (a2) 지방산-N- 알킬폴리히드록시알킬아미드를 함유한 수성 제조물을 처리하고 건조된 생성물을 제거하여 수득한다. 상기 수득된 생성물을 우수한 향 및 맛 특성을 가지며 치약 및 합성비누와 같은 계면 활성제의 생성물에 사용할 수 있다.

Description

무수, 자유 유동 당 계면 활성제 분말의 제조방법(PROCESS FOR PRODUCING ANHYDROUS POURABLE SUGAR TENSIDE POWDERS)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (17)

  1. (a1) 알킬 및/또는 알케닐 올리고글리코시드 및/또는 (a2) 지방산-N-알킬 폴리히드록시알킬아미드를 함유한 수성 제조물을 100~225℃의 온도에서 과열증기로써 처리하고 건조된 물질을 제거하는 무수, 자유 유동당 계면 활성제의 제조 방법.
  2. 제1항에 있어서, 하기 일반식(Ⅰ)에 상응하는 알킬 및/또는 알케닐 올리고글리코시드를 성분(a1)으로서 사용하는 것을 특징으로 하는 방법.;
    R1O-[G]p(Ⅰ)
    (식 중, R1은 6~22개의 탄소 원자를 함유하는 알킬 및/또는 알케닐 라디칼이며, G는 5 또는 6개의 탄소 원자를 함유하는 당 단위이며, p는 1~10의 숫자이다)
  3. 제1항 또는 제2항에 있어서, 하기 일반식(II)에 상응하는 지방산-N-알킬 폴리히드록시알킬아미드를 성분(a2)로서 사용하는 것을 특징으로 하는 방법;
    (식 중, R2CO는 6~22개의 탄소원자를 함유하는 지방족 아실 라디칼이며, R3는 수소, 1~4개의 탄소원자를 함유하는 알킬 또는 히드록시알킬 라디칼 및 [Z]는 3~12개의 탄소원자 및 3~10개의 히드록실기를 함유하는 직쇄 또는 분지된 폴리히드록시알킬 라디칼이다).
  4. 제1항 내지 제3항 중 어느 한 항에 있어서, 첨가적으로 음이온 계면 활성제를 함유한 수성 제조물을 특징으로 하는 방법.
  5. 제1항 내지 제4항 중 어느 한 항에 있어서, 하기 일반식(Ⅳ)에 상응하는 알킬 및/또는 알케닐 술폰산을 음이온 계면 활성제(성분 b)로서 사용하는 것을 특징으로 하는 방법;
    R4O-SO3X (Ⅳ)
    (식 중, R4는 직쇄 또는 분지쇄 8~22개의 탄소원자를 함유하는 알킬 및/또는 알케닐 라디칼이며, X는 알킬리 금속 및/또는 알칼리 토 금속, 암모늄, 알킬 암모늄, 알카놀암모늄 또는 글루카모늄이다).
  6. 제5항에 있어서, 일반식(IV)에 상응하는 알킬 황산을 사용하는 것을 특징으로 하는 방법(식 중, R4는 16~18개의 탄소원자를 함유하는 알킬 라디칼이고 X는 나트륨이다).
  7. 제5항에 있어서, 한편으로는 16~18개의 탄소원자 및 다른 한편으로는 12~14개의 탄소원자를 함유하는 알킬 라디칼의 비가 50 : 50~90 : 10 중량부의 범위인 일반식(Ⅳ)를 사용하는 것을 특징으로 하는 방법(식 중, R4는 C12-18알킬 라디칼이고 X는 나트륨이다).
  8. 제1항 내지 제7항 중 어느 한 항에 있어서, 성분(a) 및 (b)를 40 : 60~99 : 1의 중량비로 사용하는 것을 특징으로 하는 방법.
  9. 제1항 내지 제8항 중 어느 한 항에 있어서, 5~70중량%의 고체 함량을 가진 수성 제조물을 사용하는 것을 특징으로 하는 방법.
  10. 제1항 내지 제9항 중 어느 한 항에 있어서, 건조를 지지체로서 알칼리 금속 및/또는 알칼리 토 금속 실리케이트의 존재에서 수행하는 것을 특징으로 하는 방법.
  11. 제1항 내지 제10항 중 어느 한 항에 있어서, 또 다른 지지체로서 알칼리 금속 및/또는 알칼리 토 금속 산화물, 황산염, 탄산염, 탄산수소, 인산염, 피로인산염 및 할로겐화물로 구성된 군으로부터 선택된 무기염을 사용하는 것을 특징으로 하는 방법.
  12. 제1항 내지 제11항 중 어느 한 항에 있어서, 또 다른 지지체로서 잘 분산되는 실리카를 사용하는 것을 특징으로 하는 방법.
  13. 제1항 내지 제12항 중 어느 한 항에 있어서, 또 다른 지지체로서 알칼리 금속 및/또는 알칼리 토 금속석험의 무기염을 사용하는 것을 특징으로 하는 방법.
  14. 제1항 내지 제13항 중 어느 한 항에 있어서, 지지체를 생성 분말내에 고체 함량을 기준으로 0.1~50중량%의 양으로 사용하는 것을 특징으로 하는 방법.
  15. 제1항 내지 제14항 중 어느 한 항에 있어서, 수성 제조물을 120~280℃의 온도에서 과열 증기로써 폐쇄계내로 분무하고, 응축물을 거기에 용해된 불순물과 함께 제거한 다음, 건조시켜 정제된 유용한 물질을 순환계로부터 제거하는 것을 특징으로 하는 방법.
  16. 제1항 내지 제15항 중 어느 한 항에 있어서, 건조된 유용한 물질을 분말화 하는 것을 특징으로 하는 방법.
  17. 계면-활성 배합물의 제조에 관한 제1항 내지 제16항 중 어느 한 항에 따른 방법에 의해 제조된 무수, 자유 유동 당 계면 활성제 분말의 용도.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019960702663A 1993-11-24 1994-11-22 무수, 자유 유동 당 계면 활성제 분말의 제조 방법(process for producing anhydrous pourable sugar tenside powders) KR960705608A (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
DE4340015A DE4340015C2 (de) 1993-11-24 1993-11-24 Verfahren zur Herstellung wasserfreier, rieselfähiger Zuckertensidpulver und deren Verwendung
DEP4340015.9 1993-11-24
DEP4431157.5 1994-09-01
DE4431157 1994-09-01
PCT/EP1994/003855 WO1995014519A1 (de) 1993-11-24 1994-11-22 Verfahren zur herstellung wasserfreier, rieselfähiger zuckertensidpulver

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Publication Number Publication Date
KR960705608A true KR960705608A (ko) 1996-11-08

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KR1019960702663A KR960705608A (ko) 1993-11-24 1994-11-22 무수, 자유 유동 당 계면 활성제 분말의 제조 방법(process for producing anhydrous pourable sugar tenside powders)

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Country Link
EP (1) EP0730484A1 (ko)
JP (1) JPH09505621A (ko)
KR (1) KR960705608A (ko)
CN (1) CN1135724A (ko)
WO (1) WO1995014519A1 (ko)

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DE19524464C2 (de) * 1995-07-10 2000-08-24 Cognis Deutschland Gmbh Verfahren zur Herstellung von Zuckertensidgranulaten
DE19533539A1 (de) * 1995-09-11 1997-03-13 Henkel Kgaa O/W-Emulgatoren
DE19534371C1 (de) * 1995-09-15 1997-02-20 Henkel Kgaa Verfahren zur Herstellung wasser- und staubfreier Zuckertensidgranulate
DE19548068C1 (de) * 1995-12-21 1997-06-19 Henkel Kgaa Verfahren zur Herstellung hellfarbiger, niedrigviskoser Tensidkonzentrate
DE19710153C1 (de) 1997-03-12 1998-02-12 Henkel Kgaa Verfahren zur Herstellung neutraler Zuckertensidgranulate
DE19961333B4 (de) * 1999-12-17 2006-12-14 Henkel Kgaa Verfahren zur Herstellung von Zuckertensidgranulaten
DE10018812A1 (de) 2000-04-15 2001-10-25 Cognis Deutschland Gmbh Verfahren zur Herstellung von nichtionischen Tensidgranulaten

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DE4030688A1 (de) * 1990-09-28 1992-04-02 Henkel Kgaa Verfahren zur spruehtrocknung von wertstoffen und wertstoffgemischen unter verwendung von ueberhitztem wasserdampf
US5519948A (en) * 1992-02-12 1996-05-28 Henkel Corporation Process for the production of granules suitable as wetting agents, detergents and/or cleaning products
DE4234376A1 (de) * 1992-10-12 1994-04-14 Henkel Kgaa Wertstoffe und Wertstoffgemische für Netz-, Wasch- und/oder Reinigungsmittel in neuer Zubereitungsform

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WO1995014519A1 (de) 1995-06-01
JPH09505621A (ja) 1997-06-03
EP0730484A1 (de) 1996-09-11
CN1135724A (zh) 1996-11-13

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