KR960010686A - 저분자량 셀룰로즈 에테르의 제조방법 - Google Patents
저분자량 셀룰로즈 에테르의 제조방법 Download PDFInfo
- Publication number
- KR960010686A KR960010686A KR1019950031777A KR19950031777A KR960010686A KR 960010686 A KR960010686 A KR 960010686A KR 1019950031777 A KR1019950031777 A KR 1019950031777A KR 19950031777 A KR19950031777 A KR 19950031777A KR 960010686 A KR960010686 A KR 960010686A
- Authority
- KR
- South Korea
- Prior art keywords
- molecular weight
- ethers
- ether
- cellulose
- cellulose ether
- Prior art date
Links
- 229920003086 cellulose ether Polymers 0.000 title claims abstract 12
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 claims abstract 5
- 239000000654 additive Substances 0.000 claims abstract 2
- 239000001913 cellulose Substances 0.000 claims abstract 2
- 239000000919 ceramic Substances 0.000 claims abstract 2
- 239000011248 coating agent Substances 0.000 claims abstract 2
- 238000000576 coating method Methods 0.000 claims abstract 2
- 239000002537 cosmetic Substances 0.000 claims abstract 2
- 239000000463 material Substances 0.000 claims abstract 2
- 238000006116 polymerization reaction Methods 0.000 claims abstract 2
- 238000002360 preparation method Methods 0.000 claims abstract 2
- 239000007787 solid Substances 0.000 claims abstract 2
- 238000005303 weighing Methods 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims 13
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 238000010894 electron beam technology Methods 0.000 claims 2
- 150000002170 ethers Chemical class 0.000 claims 2
- 229920013821 hydroxy alkyl cellulose Polymers 0.000 claims 2
- 239000004902 Softening Agent Substances 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 230000003139 buffering effect Effects 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- 229910017053 inorganic salt Inorganic materials 0.000 claims 1
- 230000001678 irradiating effect Effects 0.000 claims 1
- 229920000609 methyl cellulose Polymers 0.000 claims 1
- YLGXILFCIXHCMC-JHGZEJCSSA-N methyl cellulose Chemical compound COC1C(OC)C(OC)C(COC)O[C@H]1O[C@H]1C(OC)C(OC)C(OC)OC1COC YLGXILFCIXHCMC-JHGZEJCSSA-N 0.000 claims 1
- 239000001923 methylcellulose Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 229920003124 powdered cellulose Polymers 0.000 claims 1
- 235000019814 powdered cellulose Nutrition 0.000 claims 1
- -1 powdered cellulose ethers Chemical class 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/28—Dragees; Coated pills or tablets, e.g. with film or compression coating
- A61K9/2806—Coating materials
- A61K9/2833—Organic macromolecular compounds
- A61K9/286—Polysaccharides, e.g. gums; Cyclodextrin
- A61K9/2866—Cellulose; Cellulose derivatives, e.g. hydroxypropyl methylcellulose
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/20—Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Wood Science & Technology (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dermatology (AREA)
- Polymers & Plastics (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Pharmacology & Pharmacy (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Medicinal Preparation (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Cosmetics (AREA)
Abstract
고체 칭량 단위용 피복재 및 세라믹 조성물 또는 화장품 제제에서의 첨가제 또는 중합반응 보조제로서 적합한 저분자량 셀룰로즈 에테로즈 고분자량 셀룰로즈 에테르와 염기의 혼합물을 전자 조사하여 수득한다.
Description
내용없음
Claims (13)
- 고분자량 셀룰로즈 에테르와 염기의 혼합물을 가속화된 전자로 조사하여 저분자량 셀룰로즈 에테르를 제조하는 방법.
- 제1항에 있어서, 고분자량 셀룰로즈 에테즈의 평균 분자량(Mη)이 50,000내지 500,000g/㏖인 방법.
- 제1항에 있어서, 메틸셀룰로즈 에테르 또는 비이온성 또는 이온성 메틸셀룰로즈 혼합 에테르가 사용되는방법.
- 제1항에 있어서, 하이드록시알킬셀룰로즈 에테르 또는 비이온성 또는 이온성 하이드록시알킬셀룰로즈 혼합 에테르가 사용되는 방법.
- 제1항에 있어서,완충작용을 하는 수용성 무기염이 염기로서 사용되는 방법.
- 제1항에 있어서, 염기의 함량이, 셀룰로즈 에테르를 기준으로 하여, 0.01내지 4중량 %인 방법.
- 제1항에 있어서, 셀룰로즈 에테르와 염기의 혼합물이, 먼저 셀룰로즈 에테르와 염기를 서로 개별적으로 미세하게 연마하고, 이어서 이들을 혼합장치에서 혼합시킴으로써 제조되는 방법.
- 제1항에 있어서, 셀룰로즈 에테르가 염기의 수용액과 함께 분무된 다음, 습윤성 셀룰로즈 에테르가 연마건조되는 방법.
- 제1항에 있어서,조사되는 셀룰로즈 에테르의 벌크 밀도가 0.2내지 0.7g/㎤인 방법.
- 제1항에 있어서, 조사가 연속적인 전자 빔 가솟화제를 사용하여 수행되는 방법.
- 제1항에 있어서, 전자 빔의 에너지 조사량이 5내지 500kGy인 방법.
- 제1항에 있어서, 청구한 방법으로 제조한 저분자량 셀룰로즈 에테르의 고체 칭량 단위용 피복재로서의 용도.
- 제1항에 있어서, 청구한 방법으로 제조한 제분자량 셀룰로즈 에테르의 세라믹 조성물 또는 화장품 제제에서의 첨가제 또는 중합반응 보조제로서의 용도.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEP4434280.2 | 1994-09-26 | ||
DE4434280A DE4434280C2 (de) | 1994-09-26 | 1994-09-26 | Verfahren zur Herstellung von niedermolekularen Celluloseethern und ihre Verwendung als Überzugsmaterial für feste Dosiereinheiten |
Publications (1)
Publication Number | Publication Date |
---|---|
KR960010686A true KR960010686A (ko) | 1996-04-20 |
Family
ID=6529177
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019950031777A KR960010686A (ko) | 1994-09-26 | 1995-09-26 | 저분자량 셀룰로즈 에테르의 제조방법 |
Country Status (6)
Country | Link |
---|---|
US (2) | US5719274A (ko) |
EP (1) | EP0708113B1 (ko) |
JP (1) | JPH08176201A (ko) |
KR (1) | KR960010686A (ko) |
CA (1) | CA2159045A1 (ko) |
DE (2) | DE4434280C2 (ko) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5807580A (en) * | 1996-10-30 | 1998-09-15 | Mcneil-Ppc, Inc. | Film coated tablet compositions having enhanced disintegration characteristics |
JP3114016B2 (ja) * | 1998-05-15 | 2000-12-04 | 株式会社ホギメディカル | 細胞接着促進効果を有する創傷止血材 |
JP3578627B2 (ja) | 1998-05-15 | 2004-10-20 | 株式会社ホギメディカル | 創傷患部の治癒を促進する組織シーラント |
DE19913533A1 (de) | 1999-03-25 | 2000-09-28 | Bayer Ag | Hochverzweigte Polykondensate |
KR100661918B1 (ko) * | 1999-04-01 | 2006-12-28 | 다우 글로벌 테크놀로지스 인크. | 겔 강도가 증가된 메틸셀룰로스, 이의 제조방법 및 이를 포함하는 식품 조성물 |
US6294008B1 (en) * | 1999-04-21 | 2001-09-25 | The Dow Chemical Company | Haze-free cellulose ether capsules and process for making |
DE19941893A1 (de) * | 1999-09-03 | 2001-03-08 | Clariant Gmbh | Niederviskose, heisswasser-flockbare Celluloseether, Verfahren zu deren Herstellung durch Depolymerisation sowie deren Verwendung |
US6383344B1 (en) * | 2000-07-19 | 2002-05-07 | Genzyme Corporation | Molecular weight reduction of polymer using irradiation treatment |
ES2386772T3 (es) * | 2001-03-15 | 2012-08-30 | Sappi Limited | Tratamiento y procedimiento de pasta papelera |
US6506712B2 (en) * | 2001-05-21 | 2003-01-14 | React, Llc | Method of manufacturing a multifunctional additive and using the same |
ITVA20030025A1 (it) * | 2003-07-17 | 2005-01-18 | Lamberti Spa | Depolimerizzazione enzimatica di carbossimetilcellulosa e relativi prodotti. |
US8324377B2 (en) * | 2004-11-02 | 2012-12-04 | Shin-Etsu Chemical Co., Ltd. | Method of separating water-soluble cellulose ether |
US20080221482A1 (en) * | 2007-03-06 | 2008-09-11 | Labor Saving Devices, Inc. | Steerable tip for flexible rods |
US9174879B2 (en) * | 2007-11-30 | 2015-11-03 | Corning Incorporated | Ceramic precursor batch composition and method of increasing ceramic precursor batch extrusion rate |
NZ626808A (en) | 2008-10-28 | 2015-08-28 | Xyleco Inc | Processing hydrocarbon-containing materials by irradiation |
JP5827232B2 (ja) * | 2009-10-14 | 2015-12-02 | キシレコ インコーポレイテッド | 紙製品のマーキング法 |
IT1400340B1 (it) | 2010-05-25 | 2013-05-24 | Lamberti Spa | Metodo per sigillare i baccelli. |
ITVA20110028A1 (it) | 2011-10-03 | 2013-04-04 | Lamberti Spa | Depolimerizzazione di polisaccaridi e prodotti correlati |
US9464227B2 (en) | 2014-03-24 | 2016-10-11 | Lamberti Spa | Moisturizing agents |
JP2015183095A (ja) * | 2014-03-24 | 2015-10-22 | 凸版印刷株式会社 | 機能性セルロース及びその製造方法、並びに、機能性セルロース分散体、成形体 |
DE17784205T1 (de) | 2016-09-28 | 2019-11-28 | Cp Kelco Oy | Waschmittelzusammensetzungen mit polysacchariden mit extrem niedrigem molekulargewicht |
IT201900012597A1 (it) | 2019-07-22 | 2021-01-22 | Lamberti Spa | Composizioni di gesso |
IT202000021232A1 (it) | 2020-09-08 | 2022-03-08 | Lamberti Spa | Metodo per migliorare le prestazioni di sostanze attive sistemiche e di inoculanti microbici |
WO2022064272A1 (en) * | 2020-09-22 | 2022-03-31 | Rensselaer Polytechnic Institute | Polysaccharide-including liquid material and its manufacturing method |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2895891A (en) | 1957-05-15 | 1959-07-21 | Gen Electric | Cellulosic materials |
US3108890A (en) * | 1960-05-23 | 1963-10-29 | Dow Chemical Co | Aqueous cellulosic compositions and method of making same |
DE1928045A1 (de) * | 1968-06-18 | 1970-01-02 | Dow Chemical Co | Verfahren zur Herstellung von wasserloeslichen Zelluloseprodukten mit niedriger Viskositaet durch Elektronenbestrahlung |
DE2917104A1 (de) * | 1979-04-27 | 1980-11-06 | Hoechst Ag | Verfahren zur viskositaetserniedrigung von celluloseethern durch ozon und seine verwendung |
US4420611A (en) * | 1982-03-18 | 1983-12-13 | Hercules Incorporated | Stabilization of irradiated carboxymethyl cellulose |
DE3530857A1 (de) * | 1985-08-29 | 1987-03-05 | Hoechst Ag | Verfahren zur herstellung von niedrigviskosen celluloseethern |
-
1994
- 1994-09-26 DE DE4434280A patent/DE4434280C2/de not_active Revoked
-
1995
- 1995-09-20 DE DE59505079T patent/DE59505079D1/de not_active Expired - Lifetime
- 1995-09-20 EP EP95114763A patent/EP0708113B1/de not_active Expired - Lifetime
- 1995-09-22 US US08/532,414 patent/US5719274A/en not_active Expired - Lifetime
- 1995-09-25 JP JP7246435A patent/JPH08176201A/ja not_active Withdrawn
- 1995-09-25 CA CA002159045A patent/CA2159045A1/en not_active Abandoned
- 1995-09-26 KR KR1019950031777A patent/KR960010686A/ko not_active Application Discontinuation
-
1997
- 1997-11-14 US US08/971,094 patent/US5928709A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE59505079D1 (de) | 1999-03-25 |
EP0708113B1 (de) | 1999-02-10 |
US5928709A (en) | 1999-07-27 |
CA2159045A1 (en) | 1996-03-27 |
JPH08176201A (ja) | 1996-07-09 |
DE4434280A1 (de) | 1996-03-28 |
EP0708113A1 (de) | 1996-04-24 |
US5719274A (en) | 1998-02-17 |
DE4434280C2 (de) | 1998-09-10 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19950926 |
|
PG1501 | Laying open of application | ||
PC1203 | Withdrawal of no request for examination | ||
WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |