[go: up one dir, main page]
More Web Proxy on the site http://driver.im/

KR930700518A - 포스포러스트리스락탐류 및 그 제조방법 - Google Patents

포스포러스트리스락탐류 및 그 제조방법

Info

Publication number
KR930700518A
KR930700518A KR1019920703005A KR920703005A KR930700518A KR 930700518 A KR930700518 A KR 930700518A KR 1019920703005 A KR1019920703005 A KR 1019920703005A KR 920703005 A KR920703005 A KR 920703005A KR 930700518 A KR930700518 A KR 930700518A
Authority
KR
South Korea
Prior art keywords
lactam
phosphorus trihalide
reaction mixture
group
phosphorus
Prior art date
Application number
KR1019920703005A
Other languages
English (en)
Inventor
하퍼 글랜즈 제프리
크리슈나 아케페디 무랄리
Original Assignee
제라드 피. 루우니
알라이드-시그날 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 제라드 피. 루우니, 알라이드-시그날 인코포레이티드 filed Critical 제라드 피. 루우니
Publication of KR930700518A publication Critical patent/KR930700518A/ko

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/5399—Phosphorus bound to nitrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/5532—Seven-(or more) membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/576—Six-membered rings
    • C07F9/59—Hydrogenated pyridine rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/52—Phosphorus bound to oxygen only
    • C08K5/529—Esters containing heterocyclic rings not representing cyclic esters of phosphoric or phosphorous acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Compounds Of Unknown Constitution (AREA)

Abstract

내용 없음.

Description

포스포러스트리스락탐류 및 그 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (22)

  1. 다음 일반식에 의한 조성물.
  3. 또는
  5. 상기 일반식들에서, X는 4 -11의 CH2단위체 반복단위들의 쇄를 나타낸다.
  6. 제1항에 있어서, CH2단위체 반복 단위들의 수가 5이며 다음 일반식에 의하여 표현된 수 있는 조성물.
  8. 제1항에 있어서, CH2단위체 반복 단위들의 수가 11인 조성물.
  9. 불황성 용매내 염기의 존재하에서 락탐과 포스포러스 트리할라이드를 반응시키는 단계를 포함하는, 청구범위 1항에 의한 조성물을 제조하는 방법.
  10. 제4항에 있어서, 락탐이 2 -피페리돈, 카프로락탐 및 라우로락탐으로 구성된 군으로부터 선택된 것인 방법.
  11. 제4항에 있어서, 포스포러스 트리할라이드가 다음 일반식에 의하여 표현되는 물질인 것인 방법.
  13. 상기 일반식에서, Y는 불소, 브롬, 요드 및 염소로 구성된 군으로부터 선택된다.
  14. 제4항에 있어서, 락탐이 포스포러스 트리할라이드에 대하여 최소한 3배 이상의 비율로 혼합되는 것인 방법.
  15. 제4항에 있어서, 유기 염기 용액이 테트라히드로푸란, 또는 디옥산, 글림, 및 디글림을 포함한 비양성자성 용매들로 구성된 군으로부터 선택된 것인 방법.
  16. 제4항에 있어서, 불황성 용매내 염기의 존재하에서 락탐과 포스포러스 트리할라이드를 함유하는 반응 혼합물을 냉각시키는 단계를 더 포함하는 것인 방법.
  17. 제4항에 있어서, 락탐과 포스포러스 트리할라이드를 함유하는 반응 혼합물에 물을 첨가하는 단계를 더 포함하는 것인 방법.
  18. 제4항에 있어서, 락탐과 포스포러스 트리할라이드의 반응 산물을 물, K2CO3의 수용액, 테트라히드로푸란, 디에틸 에테르로 구성된 군으로부터 선택된 최소한 하나의 시약으로 세척하는 단계를 더 포함하는 것인 방법.
  19. 제4항에 있어서, 포스포러스 트리할라이드와 락탐의 반응의 건조 반응산물을 회수하는 단계를 더 포함하는 것인 방법.
  20. 제4항에 있어서, 반응혼합물의 온도를 25℃이하로 유지시키기에 충분한 속도로 반응 혼합물내 락탐에 포스포러스 트리할라이드를 첨가하는 단계를 포함하는 것인 방법.
  21. 제13항에 있어서, 공정 전체를 통하여 5 -25℃의 범위에서 온도가 유지되도록 반응혼합물을 선택적으로 냉각시키는 단계를 포함하는 것인 방법.
  22. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019920703005A 1990-06-25 1991-06-13 포스포러스트리스락탐류 및 그 제조방법 KR930700518A (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US54249890A 1990-06-25 1990-06-25
US542,498 1990-06-25
US07/688,773 US5118805A (en) 1990-06-25 1991-04-22 Phosphoroustrislactams and methods for their production
US688,773 1991-04-22
PCT/US1991/004224 WO1992000305A1 (en) 1990-06-25 1991-06-13 Phosphoroustrislactams and methods for their production

Publications (1)

Publication Number Publication Date
KR930700518A true KR930700518A (ko) 1993-03-15

Family

ID=27067050

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920703005A KR930700518A (ko) 1990-06-25 1991-06-13 포스포러스트리스락탐류 및 그 제조방법

Country Status (11)

Country Link
US (1) US5118805A (ko)
EP (1) EP0536252B1 (ko)
JP (1) JPH0751645B2 (ko)
KR (1) KR930700518A (ko)
AT (1) ATE105293T1 (ko)
BR (1) BR9106479A (ko)
CA (1) CA2085221C (ko)
DE (1) DE69101921T2 (ko)
DK (1) DK0536252T3 (ko)
ES (1) ES2055991T3 (ko)
WO (1) WO1992000305A1 (ko)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5357030A (en) * 1992-06-03 1994-10-18 Alliedsignal Inc. Process for producing and polyamide compositions comprising lactamyl phosphites as chain extending agents
US5281676A (en) * 1992-06-03 1994-01-25 Alliedsignal Inc. Process for producing and polyester compositions comprising lactamyl phosphites as chain extending agents
DE69307319T2 (de) * 1992-07-20 1997-04-24 Allied Signal Inc Verfahren zur herstellung von kettenverlängerte polymeren und pfropf- und blockcopolymeren
WO1994010242A1 (en) * 1992-10-26 1994-05-11 Allied-Signal Inc. Nucleating system for polyesters and articles formed therefrom
JPH08508530A (ja) * 1993-04-05 1996-09-10 アライドシグナル・インコーポレーテッド 高耐衝撃性ポリエステル組成物

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE755761A (fr) * 1969-09-04 1971-03-04 Upjohn Co Phosphonates de caprolactame
JPS6088065A (ja) * 1983-10-21 1985-05-17 Mitsubishi Gas Chem Co Inc ポリフエニレンエ−テル系樹脂組成物
WO1986001572A1 (en) * 1984-09-06 1986-03-13 Delta Ag Friction wheel torque converter
GB8520999D0 (en) * 1985-08-22 1985-09-25 Clinical Product Dev Ltd Wound closure device
US4927881A (en) * 1988-04-18 1990-05-22 General Electric Company Solvent-resistant, compatible polyphenylene ether-thermoplastic polyester blends containing large proportions of polycarbonate

Also Published As

Publication number Publication date
JPH0751645B2 (ja) 1995-06-05
DE69101921D1 (de) 1994-06-09
EP0536252A1 (en) 1993-04-14
EP0536252B1 (en) 1994-05-04
JPH05506867A (ja) 1993-10-07
CA2085221C (en) 1997-02-25
CA2085221A1 (en) 1991-12-26
BR9106479A (pt) 1993-06-22
DE69101921T2 (de) 1994-08-18
DK0536252T3 (da) 1994-06-06
WO1992000305A1 (en) 1992-01-09
ATE105293T1 (de) 1994-05-15
US5118805A (en) 1992-06-02
ES2055991T3 (es) 1994-09-01

Similar Documents

Publication Publication Date Title
KR900700489A (ko) 희토류 크립테이트, 제조방법, 합성중간물질 및 형광 트레이서로서의 용도
JPS63309527A (ja) 新規ポリシラザン及びその製造方法
KR930700518A (ko) 포스포러스트리스락탐류 및 그 제조방법
Campbell et al. Reactions of dioxetanes with sulfoxylates and sulfides. Preparation of novel tetraalkoxysulfuranes
Lockhart et al. 2, 3-Di-propyl-1, 4-dehydrobenzene
KR850003394A (ko) 신규의 벤젠설포닐-락탐을 활성물질로서 포함하는 약학적 조성물과 그 제조방법
RO91422B (ro) Procedeu pentru prepararea unor derivati de 1,3-oxazolidin-2-ona
Warren et al. Synthesis of. alpha.-cyanoglycine N-carboxyanhydride and. alpha.-cyanoglycine
KR870008619A (ko) 알칼리 금속 락타메이트로 된 촉매조성물 및 그 제조 방법
Inouye et al. Cyclopropanes. Xi. Solvent Effect in Partial Asymmetric SYNTHESIS1
US3375274A (en) Alkylene borazine polymers
Kuan et al. Facile syntheses of dibenzo-14-crown-41a and bis-butylbenzo-14-crown-41b
IE890858L (en) Process for the synthesis of arylsulphonylakylamide
KR890700587A (ko) 항궤양 작용의 화합물 제조방법
DK0454207T3 (da) Flydende reaktiv sammensætning med høj polymerisationshastighed indeholdende polyisocyanater og forb indelser med en eller flere epoxygrupper
US2941001A (en) Manufacture of aminophosphines
US4720562A (en) Novel titanium-containing reagents for methylenation and analogous reactions
KR850007253A (ko) d,1-트랜스-소브레롤의 데오필린-7-아세트산 에스테르의 제조방법
KR890005025A (ko) 3-(4'-브로모비페닐-4-일)테트랄린-i-온의 제조방법
RO86277B (ro) Procedeu de preparare a unor azolil-sililglicoeteri
US3923753A (en) 1,4-Dihydronaphthalene derivatives
US4420431A (en) Salts of 3-cyano-3-alkene-sulfinic acids and salts of 3-carbamoyl-3-alkene sulfonic acids and preparations thereof
US4754028A (en) 3,4,5-triselena-tricyclo-[5.2.1.0.2,6 ]decanes and derivatives thereof
KR830005272A (ko) 스티렌 중합체의 제조방법
JPS60185759A (ja) ４，４′−ジヒドロキシジフエニルジスルフイドの製造方法

Legal Events

Date Code Title Description
PA0109 Patent application

Patent event code: PA01091R01D

Comment text: Patent Application

Patent event date: 19921127

PG1501 Laying open of application
PC1203 Withdrawal of no request for examination
WITN Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid