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KR840003268A - Process for preparing lodanphenylazo dye - Google Patents

Process for preparing lodanphenylazo dye Download PDF

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Publication number
KR840003268A
KR840003268A KR1019830000233A KR830000233A KR840003268A KR 840003268 A KR840003268 A KR 840003268A KR 1019830000233 A KR1019830000233 A KR 1019830000233A KR 830000233 A KR830000233 A KR 830000233A KR 840003268 A KR840003268 A KR 840003268A
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KR
South Korea
Prior art keywords
carbon atoms
alkoxy
alkyl
formula
hydrogen
Prior art date
Application number
KR1019830000233A
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Korean (ko)
Inventor
바우만 베르너
Original Assignee
진 크라머, 한스 루돌프 하우스
산도즈 리미티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 진 크라머, 한스 루돌프 하우스, 산도즈 리미티드 filed Critical 진 크라머, 한스 루돌프 하우스
Priority to KR1019830000233A priority Critical patent/KR840003268A/en
Publication of KR840003268A publication Critical patent/KR840003268A/en

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Plural Heterocyclic Compounds (AREA)

Abstract

내용 없음No content

Description

로단페닐아조 염료의 제조방법Process for preparing lodanphenylazo dye

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (6)

다음 일반식(Ⅳ)의 디아조화된 아민을 다음 일반식(Ⅴ)의 화합물과 커플링 시킴을 특징으로 하는, 다음 일반식(Ⅰ)의 화합물 제조방법.A method for preparing a compound of formula (I), characterized by coupling a diazotized amine of formula (IV) to a compound of formula (V): 상기식에서, k는 커플링 성분기이다.Wherein k is a coupling component group. 다음 일반식(Ⅵ)의 화합물을 티오시안산의 염과 반응시킴을 특징으로하는, 다음 일반식(Ⅰ)의 화합물의제조방법A process for preparing a compound of formula (I), characterized by reacting a compound of formula (VI) with a salt of thiocyanic acid 상기식에서, k는 커플링 성분기이며, x는 할로겐원자, 바람직하게 클로로 또는 브로모이다.Wherein k is a coupling component group and x is a halogen atom, preferably chloro or bromo. 제1 또는 2항에 있어서, k가 다음 일반식(Ⅱ)또는 일반식(Ⅲ)의 기인 K₁인 방법The method according to claim 1 or 2, wherein k is K 'which is a group of the following general formula (II) or (III). 상기식에서, R₁은 수소, 클로로, 브로모, 탄소수 3내지 4의 알킬, 탄소수 1내지 4의 알콕시, 탄소수 1내지 4의 알콕시에톡시 또는 벤질옥시이고, R₂는 수소, 클로로, 브로모, 탄소수 1내지 2의 알킬,탄소수 1내지 4의 알콕시, 페닐-탄소수 1내지 3의 알콕시,아실옥시 또는 아실아미노이며, R₃및 R₄는 독립적으로 수소; 탄소수 1내지 12의 알킬; 탄소수 3내지 4의 알케닐; 탄소수 3내지 4의 알키닐; 벤질 또는 OH, 탄소수 1내지 4의 알콕시, 아실옥시, 클로로, 브로모, 시아노, 페닐, 페녹시 또는 탄소수 1내지 3의 알콕시카보닐로부터 선택한 1 또는 2개의 치환기로 치환된 탄소수 2내지 6의 알킬로부터 선택하고,A는 탄소수 2내지 7의 알킬렌 또는 일반식-0-탄소수 2내지 4의 알킬렌-의 그룹인데, 단 일반식(Ⅲ)의 그룹의 N-원자는 산소원자에 부착되지 않는다.Wherein R 'is hydrogen, chloro, bromo, alkyl of 3 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, alkoxyethoxy or benzyloxy of 1 to 4 carbon atoms, R2 is hydrogen, chloro, bromo, 1 carbon Alkyl of 2 to 2, alkoxy of 1 to 4 carbon atoms, alkoxy of 1 to 3 carbon atoms, alkoxy, acyloxy or acylamino, and R 3 and R ′ are independently hydrogen; Alkyl of 1 to 12 carbon atoms; Alkenyl having 3 to 4 carbon atoms; Alkynyl having 3 to 4 carbon atoms; 2 to 6 carbon atoms substituted with 1 or 2 substituents selected from benzyl or OH, alkoxy having 1 to 4 carbon atoms, acyloxy, chloro, bromo, cyano, phenyl, phenoxy or alkoxycarbonyl having 1 to 3 carbon atoms And A is a group of alkylene having 2 to 7 carbon atoms or alkylene- having general formula 0-C2 to 4 carbon atoms, provided that the N-atom of the group of general formula (III) is not attached to an oxygen atom Do not. 제3항에 있어서, R₁이 수소, 메톡시 또는 에톡시인 방법.4. The process of claim 3 wherein R 'is hydrogen, methoxy or ethoxy. 제3 또는 4항에 있어서, R₂가 수소, 메틸, 탄소수 1내지 2의 알콕시, 탄소수 1내지 6의 알킬카보닐 아미노 또는 탄소수 1내지 2의 알콕시카보닐아미노인 방법.The process according to claim 3 or 4, wherein R2 is hydrogen, methyl, alkoxy having 1 to 2 carbon atoms, alkylcarbonyl amino having 1 to 6 carbon atoms or alkoxycarbonylamino having 1 to 2 carbon atoms. 제3 내지 5항중 어느 하나에 있어서, R₃및 R₄를 각각 독립적으로 수소; 탄소수 1내지 12의 알킬; 탄소수 3내지 4의 알케닐; 또는 OH, 탄소수1내지 2의 알킬카보닐옥시, 탄소수 1내지 2의 알콜시카보닐옥시, 시아노 또는 탄소수 1내지 3의 알콕시-카보닐로부터 선택한 1개의 치환기로 치환된 탄소수 2내지 6의 알킬로부터 선택하는 방법.6. A compound according to any one of claims 3 to 5, wherein R < 3 > and R 'are each independently hydrogen; Alkyl of 1 to 12 carbon atoms; Alkenyl having 3 to 4 carbon atoms; Or alkyl having 2 to 6 carbon atoms substituted with one substituent selected from OH, alkyl carbonyloxy having 1 to 2 carbon atoms, alcoholcarbonyloxy having 1 to 2 carbon atoms, cyano or alkoxy-carbonyl having 1 to 3 carbon atoms How to choose from. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019830000233A 1983-01-21 1983-01-21 Process for preparing lodanphenylazo dye KR840003268A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019830000233A KR840003268A (en) 1983-01-21 1983-01-21 Process for preparing lodanphenylazo dye

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019830000233A KR840003268A (en) 1983-01-21 1983-01-21 Process for preparing lodanphenylazo dye

Publications (1)

Publication Number Publication Date
KR840003268A true KR840003268A (en) 1984-08-20

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Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019830000233A KR840003268A (en) 1983-01-21 1983-01-21 Process for preparing lodanphenylazo dye

Country Status (1)

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KR (1) KR840003268A (en)

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