KR20230006157A - Composition for controlling eco-friendly ticks using vegetable oil - Google Patents
Composition for controlling eco-friendly ticks using vegetable oil Download PDFInfo
- Publication number
- KR20230006157A KR20230006157A KR1020210087000A KR20210087000A KR20230006157A KR 20230006157 A KR20230006157 A KR 20230006157A KR 1020210087000 A KR1020210087000 A KR 1020210087000A KR 20210087000 A KR20210087000 A KR 20210087000A KR 20230006157 A KR20230006157 A KR 20230006157A
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- KR
- South Korea
- Prior art keywords
- oil
- weight
- friendly
- vegetable oil
- eco
- Prior art date
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Images
Classifications
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
Description
본 발명은 식물성 오일을 이용한 친환경 진드기 방제용 조성물에 관한 것으로, 더욱 상세하게는 식물성 오일을 주성분으로 하여 친환경적이며 우수한 보존성을 나타내고, 닭 진드기에 대해 우수한 방제효과를 나타낼 뿐만 아니라, 물에 희석하여 사용하더라도 방제효과가 유지되어 산업상 이용가능성이 매우 높은 식물성 오일을 이용한 친환경 진드기 방제용 조성물에 관한 것이다.The present invention relates to a composition for controlling eco-friendly ticks using vegetable oil, and more particularly, to a composition for controlling eco-friendly mites using vegetable oil as a main component, which is environmentally friendly and exhibits excellent preservative properties, exhibits excellent control effects against chicken mites, and is used after diluting with water Even if the control effect is maintained, it relates to a composition for controlling eco-friendly mites using vegetable oil, which has a very high industrial applicability.
닭진드기(Dermanyssus galinae, Poultry red mite)는 가시진드기목, 새진드기과에 속하는 아열대성 외부 기생충으로 닭의 체표면에 붙어 기생하고 흡혈한다.Chicken mite (Dermanyssus galinae, Poultry red mite) is a subtropical ectoparasite that belongs to the order Prickly mite and Bird mite, attaching to the body surface of chickens and sucking blood.
양계농가에서 가장 빈번히 발생하는 닭진드기로는 큰닭진드기(닭붉은옴, 와구모; fowl red mite, Dermanyssus gallinae)와 북방새진드기(northern fowl mite, Ornithonyssus sylviarum)가 있는데, 오래 전부터 국내뿐 만 아니라 전 세계적으로 분포되어 있으며 특히, 유럽과 아시아를 중심으로 양계 농가에 큰 피해를 주고 있다. 과거에는 북방새진드기가 진드기 피해의 주요 원인이었으나, 10년전부터는 큰닭진드기(닭붉은옴, 와구모)의 피해가 주요 원인이 되었다.Chicken mites that occur most frequently in poultry farms include fowl red mite (Dermanyssus gallinae) and northern fowl mite (Ornithonyssus sylviarum). It is distributed all over the world, especially in Europe and Asia, causing great damage to poultry farms. In the past, northern bird ticks were the main cause of mite damage, but since 10 years ago, large chicken ticks (chicken mange, wagumo) have become the main cause.
최근 기후 변화로 인하여 사육환경이 고온다습해져 감에 따라 계절에 관계없이 그 피해는 날로 증가하고 있으며, 닭에 기생하여 흡혈함으로써 닭에게 가려움증과 빈혈 등을 일으키고, 낮에는 주로 사료를 비롯해 계분벨트, 계사의 갈라진 틈새, 사료통, 닭털과 분변 등에 숨어서 서식하다가 어두워지면 닭 몸에 붙어 흡혈을 하는 특성을 보이기 때문에 초기에 발견하기 어렵고 이미 발견했을 때에는 엄청난 집단이 서식하여 방제가 매우 어렵다는 문제점이 있었다.As the breeding environment has become hot and humid due to recent climate change, the damage is increasing day by day regardless of the season. It hides in the cracks of cages, feed bins, chicken hair and feces, and when it gets dark, it attaches to the chicken body and shows blood-sucking characteristics.
또한, 닭 진드기는 양계농가에 산란계 닭의 산란율 감소 및 오염란 생산, 빈혈, 발육지연, 수면장애, 영양결핍 및 영양흡수 장애 등의 피해를 주며 가금티푸스, 가금콜레라와 같은 닭과 관련된 다양한 전염병을 일으키는 바이러스 등의 매개자 역할을 하여 산란계 닭의 집단 폐사를 일으키기도 한다.In addition, chicken mites cause damage to poultry farms by reducing egg production and production of contaminated eggs, anemia, growth retardation, sleep disorders, malnutrition and malabsorption, and causing various chicken-related infectious diseases such as fowl typhus and fowl cholera. It acts as a mediator of viruses, etc., causing mass death of laying hens.
국내에서는 수년전부터 닭진드기의 방제에 사용되는 화학농약 약제로서 피레트로이드(pyrethroid)계, 카바메이트(carbamate)계, 유기인(organophosphorus)계가 대표적이며, 최근 페닐피라조에(phenylpyrazoe)계의 피프로닐(fipronil) 및 비펜트린(Bifenthrin)도 사용되고 있다. 그러나, 최근 이러한 농약들은 독성이 매우 강하여 환경문제를 더욱 심각하게 만들고 있을 뿐만 아니라, 생산물의 잔류농약으로 인하여 이를 직접 섭취하는 인체에도 치명적인 위해 요인으로 작용하는 심각한 문제를 야기하고 있어 농약 사용이 줄어드는 추세이다.In Korea, pyrethroid, carbamate, and organophosphorus are representative chemical pesticides used to control chicken mites for several years. Recently, phenylpyrazoe fipronil (fipronil) and Bifenthrin are also used. However, in recent years, these pesticides are very toxic, which not only makes environmental problems more serious, but also causes serious problems that act as fatal hazards to the human body directly ingesting them due to pesticide residues in the products, so the use of pesticides is decreasing. to be.
이에 따라 화학 농약을 대체하기 위하여 천연물 및 천적 미생물 등을 이용한 닭진드기 방제의 연구가 활발하게 진행되어 새로운 친환경 제품들이 출시되고 있으나, 대부분의 천연물 및 천적 미생물들을 이용한 약제에 대한 닭진드기의 저항성(내성)이 빠르게 진행되어 방제효과가 미약하거나, 살충율 및 살충효과가 미미하여 농민들로부터 큰 호응을 얻지 못하고 있어 화학 농약의 대체 약제로서 성공하지 못하고 있다.Accordingly, in order to replace chemical pesticides, research on chicken mite control using natural products and natural enemy microorganisms is being actively conducted and new eco-friendly products are being released. ) is rapidly progressing, and the control effect is weak, or the insecticidal rate and insecticidal effect are insignificant, so it is not successful as a substitute for chemical pesticides because it is not well received by farmers.
살충제의 내성문제에 관하여는 닭진드기 뿐만아니라 모든 병해충에는 현용되는 살충제에 대해 내성이 생기고 있다. 따라서, 새로운 살충제, 특히 새로운 작용 모드를 갖는 살충제가 필요하다. 내성을 방지하거나 제한하는 가능한 다른 방법은 그 작용 모드가 상이한 살충제의 혼합물을 사용하는 것이다. 이러한 살충제 혼합물들은 실용적이고 효과적이도록 화학적으로 안정해야 한다.Regarding the problem of resistance to insecticides, not only chicken mites but also all pests are developing resistance to currently used insecticides. Therefore, there is a need for new pesticides, especially pesticides with new modes of action. Another possible way to prevent or limit resistance is to use mixtures of pesticides with different modes of action. These pesticide mixtures must be chemically stable to be practical and effective.
본 발명의 목적은 식물성 오일을 주성분으로 하여 친환경적이며 우수한 보존성을 나타내고, 닭 진드기에 대해 우수한 방제효과를 나타낼 뿐만 아니라, 물에 희석하여 사용하더라도 방제효과가 유지되어 산업상 이용가능성이 매우 높은 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제공하는 것이다.An object of the present invention is to use vegetable oil as a main component, which is eco-friendly and exhibits excellent preservative properties, exhibits excellent control effects against chicken mites, and maintains control effects even when diluted in water and used, vegetable oil with very high industrial applicability To provide an eco-friendly mite control composition using.
본 발명의 목적은 식물성오일 혼합물, 글리세린, 계면활성제 및 지방산으로 이루어지며, 상기 식물성오일 혼합물은 타임오일, 시다오일, 올리브오일 및 세사미오일로 이루어진 그룹에서 선택된 둘 이상으로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제공함에 의해 달성된다.An object of the present invention is a vegetable oil mixture consisting of a vegetable oil mixture, glycerin, a surfactant and a fatty acid, wherein the vegetable oil mixture consists of two or more selected from the group consisting of thyme oil, cedar oil, olive oil and sesame oil. It is achieved by providing an eco-friendly mite control composition using.
본 발명의 바람직한 특징에 따르면, 상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 식물성오일 혼합물 50 내지 70 중량%, 글리세린 15 내지 20 중량%, 계면활성제 5 내지 10 중량% 및 지방산 10 내지 20 중량%로 이루어지는 것으로 한다.According to a preferred feature of the present invention, the eco-friendly mite control composition using the vegetable oil is 50 to 70% by weight of a vegetable oil mixture, 15 to 20% by weight of glycerin, 5 to 10% by weight of a surfactant and 10 to 20% by weight of fatty acids to be made
본 발명의 더 바람직한 특징에 따르면, 상기 식물성오일 혼합물은 타임오일 100 중량부, 시다오일 45 내지 55 중량부, 올리브오일 60 내지 70 중량부 및 세사미오일 10 내지 20 중량부로 이루어지는 것으로 한다.According to a more preferred feature of the present invention, the vegetable oil mixture is composed of 100 parts by weight of thyme oil, 45 to 55 parts by weight of cedar oil, 60 to 70 parts by weight of olive oil, and 10 to 20 parts by weight of Sesame oil.
본 발명의 더욱 바람직한 특징에 따르면, 상기 식물성오일 혼합물은 타임오일 100 중량부, 올리브오일 80 내지 85 중량부 및 세사미 오밀 8 내지 12 중량부로 이루어지는 것으로 한다.According to a more preferred feature of the present invention, the vegetable oil mixture is composed of 100 parts by weight of thyme oil, 80 to 85 parts by weight of olive oil, and 8 to 12 parts by weight of sesame oil.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 지방산은 올레산으로 이루어지는 것으로 한다.According to a further preferred feature of the present invention, the fatty acid is made of oleic acid.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물에는 상기 방제용 조성물 100 중량부 대비 채종유, 피마자유, 옥수수유, 해바라기유 및 대두유로 이루어진 그룹에서 선택된 하나 이상으로 이루어진 오일첨가제 10 내지 30 중량부가 더 함유되는 것으로 한다.According to a more preferred feature of the present invention, the eco-friendly mite control composition using the vegetable oil is composed of at least one selected from the group consisting of rapeseed oil, castor oil, corn oil, sunflower oil and soybean oil, based on 100 parts by weight of the control composition. 10 to 30 parts by weight of oil additives are further contained.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 정제수에 500 내지 750배로 희석되어 사용되는 것으로 한다.According to a more preferred feature of the present invention, the eco-friendly mite control composition using the vegetable oil is to be used diluted 500 to 750 times in purified water.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 오일 스프레이, 습윤성 분말, 유동물 과립, 에어로졸, 훈연제 및 훈증제로 이루어진 그룹에서 선택된 하나의 제형에 적용되는 것으로 한다.According to a more preferred feature of the present invention, the eco-friendly mite control composition using the vegetable oil is applied to one formulation selected from the group consisting of oil spray, wettable powder, flow granule, aerosol, smoker and fumigator.
본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 식물성 오일을 주성분으로 하여 친환경적이며 우수한 보존성을 나타내고, 닭 진드기에 대해 우수한 방제효과를 나타낼 뿐만 아니라, 물에 희석하여 사용하더라도 방제효과가 유지되어 산업상 이용가능성이 매우 높은 진드기 방제용 조성물을 제공하는 탁월한 효과를 나타낸다.The composition for controlling eco-friendly mites using vegetable oil according to the present invention is eco-friendly and exhibits excellent preservative properties using vegetable oil as a main component, and exhibits excellent control effects against chicken mites. Even when diluted in water, the control effect is maintained It shows an excellent effect of providing a composition for controlling ticks with very high industrial applicability.
도 1은 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 살포하는 과정을 촬영하여 나타낸 사진이다.
도 2는 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 살포 전과 후에 닭장의 모습을 촬영하여 나타낸 사진이다.1 is a photograph showing a process of spraying an eco-friendly mite control composition using vegetable oil according to the present invention.
Figure 2 is a photograph showing the appearance of the chicken coop before and after spraying the eco-friendly mite control composition using vegetable oil according to the present invention.
이하에는, 본 발명의 바람직한 실시예와 각 성분의 물성을 상세하게 설명하되, 이는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 발명을 용이하게 실시할 수 있을 정도로 상세하게 설명하기 위한 것이지, 이로 인해 본 발명의 기술적인 사상 및 범주가 한정되는 것을 의미하지는 않는다.Hereinafter, a preferred embodiment of the present invention and the physical properties of each component will be described in detail, but this is to be explained in detail so that a person having ordinary knowledge in the art to which the present invention belongs can easily practice the invention, This is not meant to limit the technical spirit and scope of the present invention.
본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 식물성오일 혼합물, 글리세린, 계면활성제 및 지방산으로 이루어지며, 식물성오일 혼합물 50 내지 70 중량%, 글리세린 15 내지 20 중량%, 계면활성제 5 내지 10 중량% 및 지방산 10 내지 20 중량%로 이루어지는 것이 바람직하다.Eco-friendly mite control composition using vegetable oil according to the present invention is composed of a vegetable oil mixture, glycerin, a surfactant and a fatty acid, 50 to 70% by weight of the vegetable oil mixture, 15 to 20% by weight of glycerin, 5 to 10% by weight of a surfactant % and 10 to 20% by weight of fatty acids.
상기 식물성오일 혼합물은 타임오일, 시다오일, 올리브오일 및 세사미오일로 이루어진 그룹에서 선택된 둘 이상으로 이루어진다.The vegetable oil mixture consists of two or more selected from the group consisting of thyme oil, cedar oil, olive oil and sesame oil.
상기 타임오일(Thyme Oil)은 타임의 꽃, 꽃대, 잎에서 추출한 에센셜 오일로 몸과 마음을 자극하고 살균효과가 강하며 면역계 강화를 돕는 오일이다. 꿀풀과 식물인 타임의 꽃, 꽃대, 잎을 증기 증류법(수증기로 식물의 방향성 유효성분을 추출하고 냉각수로 식혀 응축하는 방법)으로 추출한 에센셜 오일로, 엷은 노란색과 약간의 점도가 있는 액체로 신선하면서 강한 허브 향이 난다.The thyme oil is an essential oil extracted from flowers, stems, and leaves of thyme, which stimulates the body and mind, has a strong sterilization effect, and helps strengthen the immune system. It is an essential oil extracted from the flowers, stems, and leaves of thyme, a plant of the Lamiaceae family, by steam distillation (a method of extracting the plant's aromatic active ingredients with steam and cooling them with cooling water to condense them). It has a strong herbal scent.
또한, 상기 타임오일은 고대로부터 널리 사용되어 왔으며 강한 살균작용이 있어 각종 세균성 질병에 광범위한 개선 효과를 나타내는데, 상기와 같이 증기증류법으로 추출한 에센셜오일을 사용할 수도 있으나, 타임오일의 추출방법은 이에 한정되지 않는다.In addition, the thyme oil has been widely used since ancient times and has a strong bactericidal action, showing a wide range of ameliorating effects on various bacterial diseases. Although essential oils extracted by steam distillation as described above can be used, the extraction method of thyme oil is not limited thereto. don't
또한, 상기 시다오일(Ceder Oil)은 향나무속 삼목(杉木)의 목질부로부터 추출된 기름인데, 무색이거나 황갈색의 점성이 있는 액체로서, 발삼 같은 향기가 있다. 성분은 세드렌(cedren) 약 80%, 세드롤(cedrol) 3∼14%, 세드레놀(cedrenol) 등이다. 화장품이나 향수에 향기를 가미시킬 때나, 살균효과가 뛰어나 목재의 코팅에도 사용된다.In addition, the Ceder Oil is an oil extracted from the woody part of the juniper cedar, and is a colorless or yellowish brown viscous liquid with a balsam-like fragrance. The ingredients are about 80% of cedren, 3-14% of cedrol, and cedrenol. It is used to add fragrance to cosmetics or perfume, or to coat wood due to its excellent sterilization effect.
또한, 상기 올리브오일(Olive Oil)은 올리브나무(감람나무)의 열매에 함유된 30 내지 70%의 기름을 압착법이나 추출법으로 채유하여 제조되는데, 항산화 작용, 면역 기능 증강, 항균 작용 등의 효과를 나타내어 유해세균이나 바이러스를 살균하고 면역력을 향상시키는 역할을 한다.In addition, the olive oil (Olive Oil) is prepared by extracting oil from 30 to 70% of the oil contained in the fruit of the olive tree (olive tree) by pressing or extracting, and has effects such as antioxidant action, immune function enhancement, and antibacterial action. It plays a role in sterilizing harmful bacteria or viruses and improving immunity.
본 발명에서 사용하는 올리브오일(Olive Oil)은 압착법으로 얻어지는 올리브 오일을 사용하나, 이에 제한 되지는 않는다. Olive oil used in the present invention uses olive oil obtained by pressing, but is not limited thereto.
또한, 상기 세사미오일(Sesame Oil)은 참깨 씨앗에서 추출되는데, 다양한 요리에 사용되고 있으며 항산화제인 비타민 E 외에도 리놀레인산, 스테아르산, 팔미트산이 풍부하여 보습력이 탁월하다. 본 발명에서 사용하는 세사미오일(Sesame Oil)은 널리 판매되고 있는 참깨오일(참기름)을 사용할 수 있다.In addition, the Sesame Oil is extracted from sesame seeds, and is used in various dishes, and is rich in linoleic acid, stearic acid, and palmitic acid in addition to vitamin E, which is an antioxidant, and has excellent moisturizing power. As the Sesame Oil used in the present invention, widely sold sesame oil (sesame oil) can be used.
상기의 성분으로 이루어지는 식물성오일 혼합물은 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 진드기 살충효과를 고려했을 때, 타임오일 100 중량부, 시다오일 45 내지 55 중량부, 올리브오일 60 내지 70 중량부 및 세사미오일 10 내지 20 중량부로 이루어지거나, 타임오일 100 중량부, 올리브오일 80 내지 85 중량부 및 세사미 오밀 8 내지 12 중량부로 이루어지는 것이 가장 바람직하다.The vegetable oil mixture composed of the above components is 100 parts by weight of thyme oil, 45 to 55 parts by weight of cedar oil, 60 to 70 parts by weight of olive oil, considering the mite insecticidal effect of the eco-friendly mite control composition using vegetable oil according to the present invention It is most preferably composed of 10 to 20 parts by weight and sesame oil, or 100 parts by weight of thyme oil, 80 to 85 parts by weight of olive oil, and 8 to 12 parts by weight of sesame oil.
상기 식물성오일 혼합물의 함량이 50 중량% 미만이면 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 진드기 살충효과가 저하되며, 상기 식물성오일 혼합물의 함량이 70중량%를 초과하게 되면 진드기 살충효과는 크게 향상되지 않으면서 제제시에 제형이 한정되는 문제점이 있다.When the content of the vegetable oil mixture is less than 50% by weight, the mite-killing effect of the eco-friendly composition for controlling mites using vegetable oil according to the present invention is reduced, and when the content of the vegetable oil mixture exceeds 70% by weight, the mite-killing effect There is a problem that the formulation is limited at the time of formulation without greatly improving.
상기 글리세린은 15 내지 20 중량%가 함유되는데, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 진드기 방제효과를 지속시키는 역할을 하며, 전착성을 형상시키는 역할을 한다.The glycerin is contained in 15 to 20% by weight, serves to maintain the mite control effect of the eco-friendly mite control composition using vegetable oil according to the present invention, and serves to shape the spreadability.
상기 글리세린의 함량이 15 중량% 미만이면 상기의 효과가 미미하며, 상기 글리세린의 함량이 20 중량%를 초과하게 되면 상기의 효과는 크게 향상되지 않으면서 상대적으로 식물성오일 혼합물의 함량이 줄어들기 때문에, 진드기 방제효과가 저하될 수 있다.If the content of glycerin is less than 15% by weight, the effect is insignificant, and if the content of glycerin exceeds 20% by weight, the effect is not greatly improved and the content of the vegetable oil mixture is relatively reduced. The effectiveness of tick control may be reduced.
상기 계면활성제는 5 내지 10 중량%가 함유되며, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 구성하는 각 성분이 고르게 혼합될 수 있도록 하여 균질한 물성을 나타내는 진드기 방제용 조성물을 제공하는 역할을 한다.The surfactant contains 5 to 10% by weight, and each component constituting the eco-friendly mite control composition using vegetable oil according to the present invention is evenly mixed to provide a mite control composition exhibiting homogeneous physical properties play a role
상기 계면활성제의 함량이 5 중량% 미만이면 상기의 효과가 미미하며, 상기 계면활성제의 함량이 20 중량%를 초과하게 되면 상기의 효과는 크게 향상되지 않으면서 상대적으로 식물성오일 혼합물의 함량이 줄어들기 때문에, 진드기 방제효과가 저하될 수 있다.If the content of the surfactant is less than 5% by weight, the effect is insignificant, and if the content of the surfactant exceeds 20% by weight, the effect is not greatly improved and the content of the vegetable oil mixture is relatively reduced. Therefore, the mite control effect may be reduced.
이때, 상기 계면활성제의 성분은 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 구성하는 각 성분이 고르게 혼합시킬 수 있는 성분이면 특별히 한정되지 않고 어떠한 것이든 사용가능하나, 트윈80(Tween80, Polysorbate 80tween80)을 사용하는 것이 바람직하다.At this time, the component of the surfactant is not particularly limited and any component can be used as long as each component constituting the eco-friendly mite control composition using vegetable oil according to the present invention can be mixed evenly, but Tween 80 (Tween80, Polysorbate 80tween80) is preferably used.
상기 지방산은 10 내지 20 중량%가 함유되며, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 진드기 방제효과를 더욱 향상시키는 역할을 하는데, 올레산(Oleic acid)으로 이루어지는 것이 바람직하다.The fatty acid contains 10 to 20% by weight, and serves to further improve the mite control effect of the eco-friendly mite control composition using vegetable oil according to the present invention, and is preferably composed of oleic acid.
상기 지방산의 함량이 10 중량% 미만이면 상기의 효과가 미미하며, 상기 지방산의 함량이 20 중량%를 초과하게 되면 진드기 살충효과는 크게 향상되지 않으면서 제제시에 제형이 한정되는 문제점이 있다.When the content of the fatty acid is less than 10% by weight, the effect is insignificant, and when the content of the fatty acid exceeds 20% by weight, the mite insecticidal effect is not greatly improved, and the formulation is limited at the time of formulation.
또한, 상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물에는 상기 방제용 조성물 100 중량부 대비 채종유, 피마자유, 옥수수유, 해바라기유 및 대두유로 이루어진 그룹에서 선택된 하나 이상으로 이루어진 오일첨가제 10 내지 30 중량부가 더 함유될 수도 있는데, 상기의 성분으로 이루어지는 오일첨가제가 더 함유되면 진드기 방제효과가 더욱 향상된 방제용 조성물이 제공될 수 있다.In addition, in the eco-friendly mite control composition using the vegetable oil, 10 to 30 parts by weight of an oil additive consisting of at least one selected from the group consisting of rapeseed oil, castor oil, corn oil, sunflower oil, and soybean oil is further added to 100 parts by weight of the control composition. It may be contained, and when an oil additive composed of the above components is further contained, a control composition for controlling mites with a further improved effect can be provided.
상기 오일첨가제의 함량이 10 중량부 미만이면 상기의 효과가 미미하며, 상기 오일첨가제의 함량이 30 중량부를 초과하게 되면, 제제시에 제형이 한정되는 문제점이 있다.If the content of the oil additive is less than 10 parts by weight, the effect is insignificant, and if the content of the oil additive exceeds 30 parts by weight, there is a problem in that the formulation is limited during formulation.
상기의 성분으로 이루어지는 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 정제수에 희석해서 사용해도 우수한 진드기 방제효과가 유지되어 산업상 이용가능성이 매우 높은데, 희석은 500 내지 750배로 이루어지는 것이 바람직하다.Eco-friendly mite control composition using vegetable oil consisting of the above components maintains excellent mite control effect even when diluted in purified water and has very high industrial applicability, dilution is preferably made 500 to 750 times.
상기 희석이 500배 미만이면 상기의 효과가 미미하며, 상기 희석이 750배를 초과하게 되면 진드기 방제효과가 저하될 수 있다.If the dilution is less than 500 times, the effect is insignificant, and if the dilution exceeds 750 times, the mite control effect may be reduced.
또한, 상기의 성분으로 이루어지는 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 오일 스프레이, 습윤성 분말, 유동물 과립, 에어로졸, 훈연제 및 훈증제로 이루어진 그룹에서 선택된 하나의 제형으로 적용될 수 있는데, 이에 한정되지는 않는다.In addition, the eco-friendly mite control composition using vegetable oil consisting of the above components may be applied as one formulation selected from the group consisting of oil spray, wettable powder, flow granule, aerosol, smoker, and fumigant, but is not limited thereto. .
또한, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 통상적으로 고체 담체, 액체 담체, 기체 담체 또는 유인물과 혼합하거나, 염기성물질, 예컨대 다공질 세라믹 플레이트 또는 부직포에 흡수시킨 후, 계면활성제 및 필요에 따라 기타 보조제들을 첨가하여, 각종 다양한 제형으로 제조될 수 있다.In addition, the eco-friendly mite control composition using vegetable oil according to the present invention is usually mixed with a solid carrier, liquid carrier, gas carrier or attractant, or absorbed into a basic material such as a porous ceramic plate or nonwoven fabric, and then a surfactant and necessary According to the addition of other adjuvants, it can be prepared in a variety of formulations.
상기 고체 담체로는 점토, 규조토, 산화규소, 벤토나이트 등의 점토 물질의 미세분말 또는 과립, 탈크, 세라믹 및 기타 무기 물질, 이를 테면 견운모, 석영, 황, 활성탄, 탄산칼슘 및 수화된 실리카 및 황산암모늄, 인산암모늄, 질산암모늄, 수산화칼륨, 우레아 및 염화암모늄과 같은 화학적 비료가 포함될 수 있다.The solid carrier includes fine powders or granules of clay materials such as clay, diatomaceous earth, silicon oxide, bentonite, talc, ceramics and other inorganic materials such as sericite, quartz, sulfur, activated carbon, calcium carbonate and hydrated silica and ammonium sulfate. , chemical fertilizers such as ammonium phosphate, ammonium nitrate, potassium hydroxide, urea and ammonium chloride.
상기 액체 담체로는 물, 에탄올, 에탄올아민, 아세톤, 에틸아세테이트, 대두유, 면실유가 포함될 수 있다.The liquid carrier may include water, ethanol, ethanolamine, acetone, ethyl acetate, soybean oil, and cottonseed oil.
또한, 본 발명의 방제제 조성물에 사용될 수 있는 기체 담체 또는 추진체로는(propellant) 프레온 가스, 부탄 가스, 액화석유가스(LPG) 및 이산화탄소가 포함될 수 있다.In addition, the gas carrier or propellant that can be used in the pesticide composition of the present invention may include Freon gas, butane gas, liquefied petroleum gas (LPG) and carbon dioxide.
또한, 본 발명의 방제제 조성물에 첨가될 수 있는 계면활성제로는 알킬 설페이트, 리니어알킬 설페이트, 알킬 아릴 설포네이트, 알킬 아릴 에테르 및 그것의 폴리옥시 에틸렌 유도체, 폴리에틸렌 글리콜 에테르, 다가 알콜 에스테르 및 당 알콜 유도체가 포함될 수 있다.In addition, surfactants that can be added to the pesticide composition of the present invention include alkyl sulfates, linear alkyl sulfates, alkyl aryl sulfonates, alkyl aryl ethers and polyoxyethylene derivatives thereof, polyethylene glycol ethers, polyhydric alcohol esters and sugar alcohols Derivatives may be included.
또한, 본 발명의 방제제 조성물에 첨가될 수 있는 전착제 또는 분산제와 같은 보조제로는 잔탄검, 카제인, 젤라틴, 전분, 아라비아검, 셀롤로스 유도체, 알긴산, 리그닌 유도체, 벤토나이트, 폴리비닐 알콜, 폴리비닐 피롤리돈 및 폴리아크릴 산이 포함될 수 있다.In addition, adjuvants such as spreaders or dispersants that can be added to the control agent composition of the present invention include xanthan gum, casein, gelatin, starch, gum arabic, cellulose derivatives, alginic acid, lignin derivatives, bentonite, polyvinyl alcohol, polyvinyl Pyrrolidone and polyacrylic acid may be included.
또한, 본 발명의 방제제 조성물은 다른 살곤충제, 살선충제, 살진드기제, 살세균제, 살진균제, 제초제, 식물 성장 조절제, 시너지스트, 비료, 토양 컨디셔너와 함께, 또는 그것들과 별도로 투여하거나 동시에 사용될 수도 있다.In addition, the control agent composition of the present invention is administered together with or separately from other insecticides, nematicides, acaricides, bactericides, fungicides, herbicides, plant growth regulators, synergists, fertilizers, and soil conditioners. or may be used simultaneously.
또한, 본 발명의 방제제 조성물은 닭진드기를 포함한 그의 알, 유충에 대한 방제 효력도 나타낸다. 또한 종래의 유기인계, 유기염소계 농약이나 천연물 유래 살충제에 대한 저항성을 갖는 닭진드기에 대해서도 방제 효과를 나타낸다.In addition, the control agent composition of the present invention also exhibits a control effect on eggs and larvae thereof, including chicken mites. In addition, it exhibits a control effect on chicken mites having resistance to conventional organophosphorus, organochlorine pesticides or insecticides derived from natural products.
이하에서는, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물의 제조방법 및 그 제조방법으로 제조된 방제용 조성물의 물성을 실시예를 들어 설명하기로 한다.Hereinafter, the manufacturing method of the eco-friendly mite control composition using vegetable oil according to the present invention and the physical properties of the control composition prepared by the manufacturing method will be described with examples.
<실시예 1><Example 1>
타임오일 30중량%, 시다오일 15중량%, 올리브오일20중량%, 세사미오일 5중량%, 글리세린 15중량%, 트윈80 5중량% 및 올레산 10중량%를 혼합하여 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제조하였다.30% by weight of thyme oil, 15% by weight of cedar oil, 20% by weight of olive oil, 5% by weight of Sesame oil, 15% by weight of glycerin, 5% by weight of Tween 80, and 10% by weight of oleic acid are mixed for eco-friendly mite control using vegetable oil A composition was prepared.
<실시예 2><Example 2>
타임오일 30중량%, 올리브오일 25중량%, 세사미오일 3중량%, 글리세린 15중량%, 트윈80 7중량% 및 올레산 20중량%를 혼합하여 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제조하였다.An eco-friendly mite control composition using vegetable oil was prepared by mixing 30% by weight of thyme oil, 25% by weight of olive oil, 3% by weight of sesame oil, 15% by weight of glycerin, 7% by weight of Tween 80, and 20% by weight of oleic acid.
<실시예 3><Example 3>
타임오일 40중량%, 시다오일 20중량%, 세사미오일 3중량%, 글리세린 15중량%, 트윈80 7중량% 및 올레산 15중량%를 혼합하여 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제조하였다.An eco-friendly composition for controlling ticks using vegetable oil was prepared by mixing 40% by weight of thyme oil, 20% by weight of cedar oil, 3% by weight of sesame oil, 15% by weight of glycerin, 7% by weight of Tween 80, and 15% by weight of oleic acid.
<실시예 4><Example 4>
시다오일 20중량%, 올리브오일 40중량%, 글리세린 20중량%, 트윈80 5중량% 및 올레산 15중량%를 혼합하여 식물성 오일을 이용한 친환경 진드기 방제용 조성물을 제조하였다.An eco-friendly mite control composition using vegetable oil was prepared by mixing 20% by weight of cedar oil, 40% by weight of olive oil, 20% by weight of glycerin, 5% by weight of Tween 80, and 15% by weight of oleic acid.
상기 실시예 1 내지 4를 통해 제조된 친환경 진드기 방제용 조성물의 닭진드기에 대한 방제효과를 측정하여 아래 표 1에 나타내었다.The control effect of the eco-friendly mite control composition prepared in Examples 1 to 4 on chicken mites was measured and shown in Table 1 below.
{단, 닭진드기에 대한 방제효과는 산란계 농장에서 닭진드기를 대량 채집하여, 실험 전까지 30℃의 온도와 상대습도 65% 및 어두운 조건에서 개체수를 유지시켰킨 후에 지름이 13cm인 배양 플레이트(plant culture plate)에 멸균된 종이여과지를 깔고 진드기가 호흡할 수 있도록 플레이트 뚜껑에 천공하고 미세메쉬로 마감하여 배양 플레이트를 준비하였다. 준비한 플레이트에 상기 개체수를 유지시킨 닭진드기를 각각 100 마리씩 분리하였다. 분리 후, 상기 실시예 1 내지 4를 통해 제조된 방제용 조성물을 각각 2000ppm의 농도로 희석하고 분무기를 이용하여 각각의 플레이트에 2 ㎖씩 균일하게 살포하였다. 살포 12 시간 후, 100배의 현미경으로 관찰하며 핀셋으로 건드려 움직임이 없는 개체를 죽은 진드기로 간주하였다. 음성 대조군으로는 물(멸균수)을 살포하였고, 양성 대조군으로는 시중에 판매되고 있는 친환경 닭진드기 구제 제품을 구입하여 권장 사용 농도로 살포 하였으며, 시험테스트는 3회 반복 수행하여 평균 살충율을 나타내는 방법을 이용하였다.{However, the control effect against chicken mites was obtained by collecting chicken mites in large quantities from laying hen farms, maintaining the population at a temperature of 30℃, 65% relative humidity, and dark conditions before the experiment, and then using a plant culture plate with a diameter of 13 cm. A culture plate was prepared by laying a sterilized paper filter paper on the plate), perforating the plate lid so that the mite could breathe, and closing it with a fine mesh. On the prepared plate, 100 chicken ticks each maintaining the above population were separated. After separation, each of the control compositions prepared in Examples 1 to 4 was diluted to a concentration of 2000 ppm and sprayed uniformly by 2 ml on each plate using a sprayer. After 12 hours of spraying, the mite was observed under a 100-fold magnification microscope, and an object that did not move by touching with tweezers was regarded as a dead mite. As a negative control, water (sterilized water) was sprayed, and as a positive control, an eco-friendly chicken mite control product sold on the market was purchased and sprayed at the recommended concentration. The test test was repeated three times to show the average insecticidal rate. method was used.
<표 1><Table 1>
상기 표 1에 나타낸 것처럼, 본 발명의 실시예 1 내지 4를 통해 제조된 진드기 방제용 조성물은 닭진드기에 대해 우수한 방제효과를 나타내는 것을 알 수 있으며, 특히 실시예 2를 통해 제조된 방제용 조성물의 방제효과가 가장 우수한 것을 알 수 있다.As shown in Table 1, it can be seen that the composition for controlling ticks prepared in Examples 1 to 4 of the present invention exhibits an excellent control effect against chicken mites, and in particular, the composition for controlling ticks prepared in Example 2 It can be seen that the control effect is the best.
또한, 상기 1 내지 4를 통해 제조된 친환경 진드기 방제용 조성물 희석액의 닭진드기에 대한 방제효과를 측정하여 아래 표 2 내지 3에 나타내었다.In addition, the control effect on chicken mites of the dilution of the eco-friendly mite control composition prepared through 1 to 4 was measured and shown in Tables 2 to 3 below.
{단, 방제용 조성물 희석액의 닭진드기에 대한 방제효과는 닭진드기 오염이 심한 양계농장을 2곳을 선정하고, 방제제 조성물과 양성대조군을 각각 500ppm, 750ppm 과 1000ppm의 농도로 물(지하수)에 희석한 후에 각 양계농장의 닭장에 1주일 간격으로 총 3회 고압 살포기를 이용하여 살포한 후에 살충효과를 확인하는 방법을 이용하였다.{However, for the control effect of the dilution of the control composition on chicken mites, two poultry farms with severe chicken mite contamination were selected, and the control composition and the positive control were mixed in water (groundwater) at concentrations of 500 ppm, 750 ppm, and 1000 ppm, respectively. After dilution, a method of confirming the insecticidal effect was used after spraying the chicken coop of each poultry farm using a high-pressure sprayer three times at intervals of one week.
또한, 살충효과는 3주 후에 확인하였으며, 닭진드기 오염의 심각함이 전혀 없음이 A(살충율 90% 초과), 조금 있음이 B(살충율 80 내지 90%, 닭진드기 오염이 조금 심각함을 C(살충율 50 내지 79%), 살충효과가 미미함을 D(살충율 50% 미만)로 나타내었다.In addition, the insecticidal effect was confirmed after 3 weeks, A for no seriousness of chicken mite contamination (more than 90% insecticidal rate), B for a little bit (80 to 90% insecticidal rate, little serious chicken mite contamination C ( Insecticidal rate 50 to 79%), and the insecticidal effect was insignificant was indicated by D (less than 50% insecticidal rate).
<표 2> A 양계농장<Table 2> A poultry farm
<표 3> B 양계농장<Table 3> B poultry farm
상기 표 2 내지 3에 나타낸 것처럼, 본 발명의 실시예 1 내지 4를 통해 제조된 방제용 조성물은 닭진드기에 대해 우수한 방제효과를 나타내는 것을 알 수 있다.As shown in Tables 2 to 3, it can be seen that the control compositions prepared in Examples 1 to 4 of the present invention exhibit excellent control effects against chicken mites.
또한, 상기 실시예 2를 통해 제조된 방제용 조성물을 상온에서 90일 동안 보관후에 육악으로 관찰한 결과 각 성분의 상분리가 발생하지 않아 우수한 보존성을 나타내는 것을 알 수 있다.In addition, as a result of observing the control composition prepared in Example 2 with meat after storage at room temperature for 90 days, it can be seen that phase separation of each component does not occur, indicating excellent preservation.
또한, 상기 실시예 2를 통해 제조된 방제용 조성물을 정제수에 500배, 750배, 1000배의 비율로 희석한 후에 닭진드기에 대한 방제효과를 측정하여 아래 표 4에 나타내었다.In addition, after diluting the control composition prepared in Example 2 in purified water at a ratio of 500 times, 750 times, and 1000 times, the control effect on chicken mites was measured and shown in Table 4 below.
{단, 방제효과는 상기에 기재된 방법을 이용하였으며, 대조군으로는 시판되고 있는 친환경 닭진드기 구제제를 250배 희석하여 사용하였다.}{However, the method described above was used for the control effect, and a commercially available eco-friendly chicken mite exterminator was diluted 250 times and used as a control group.}
<표 4><Table 4>
상기 표 4에 나타낸 것처럼, 본 발명의 실시예 2를 통해 제조된 방제용 조성물은 정제수로 희석하더라도 닭진드기에 대해 우수한 방제효과를 나타내는 것을 알 수 있는데, 희석배수가 1000배인 경우 방제효과가 70%대로 저하되기 때문에, 희석배수는 500 내지 750배로 진행하는 것이 가장 바람직한 것을 알 수 있다.As shown in Table 4, it can be seen that the control composition prepared in Example 2 of the present invention exhibits an excellent control effect against chicken mites even when diluted with purified water. It can be seen that it is most preferable to proceed with a dilution factor of 500 to 750 times.
따라서, 본 발명에 따른 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 식물성 오일을 주성분으로 하여 친환경적이며 우수한 보존성을 나타내고, 닭 진드기에 대해 우수한 방제효과를 나타낼 뿐만 아니라, 물에 희석하여 사용하더라도 방제효과가 유지되어 산업상 이용가능성이 매우 높다.Therefore, the eco-friendly mite control composition using vegetable oil according to the present invention is eco-friendly and exhibits excellent preservative properties using vegetable oil as a main component, not only exhibits excellent control effect against chicken mites, but also has a control effect even when diluted in water It is maintained and the industrial applicability is very high.
Claims (8)
상기 식물성오일 혼합물은 타임오일, 시다오일, 올리브오일 및 세사미오일로 이루어진 그룹에서 선택된 둘 이상으로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
It consists of a mixture of vegetable oils, glycerin, surfactants and fatty acids,
The vegetable oil mixture is an eco-friendly mite control composition using vegetable oil, characterized in that consisting of two or more selected from the group consisting of thyme oil, cedar oil, olive oil and sesame oil.
상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 식물성오일 혼합물 50 내지 70 중량%, 글리세린 15 내지 20 중량%, 계면활성제 5 내지 10 중량% 및 지방산 10 내지 20 중량%로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
The method of claim 1,
Eco-friendly mite control composition using the vegetable oil is vegetable oil, characterized in that consisting of 50 to 70% by weight of vegetable oil mixture, 15 to 20% by weight of glycerin, 5 to 10% by weight of surfactant and 10 to 20% by weight of fatty acid Eco-friendly mite control composition using.
상기 식물성오일 혼합물은 타임오일 100 중량부, 시다오일 45 내지 55 중량부, 올리브오일 60 내지 70 중량부 및 세사미오일 10 내지 20 중량부로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
According to claim 1 or 2,
The vegetable oil mixture is an eco-friendly mite control composition using vegetable oil, characterized in that consisting of 100 parts by weight of thyme oil, 45 to 55 parts by weight of cedar oil, 60 to 70 parts by weight of olive oil and 10 to 20 parts by weight of Sesame oil.
상기 식물성오일 혼합물은 타임오일 100 중량부, 올리브오일 80 내지 85 중량부 및 세사미오밀 8 내지 12 중량부로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
According to claim 1 or 2,
The vegetable oil mixture is an eco-friendly mite control composition using vegetable oil, characterized in that consisting of 100 parts by weight of thyme oil, 80 to 85 parts by weight of olive oil and 8 to 12 parts by weight of sesamiomil.
상기 지방산은 올레산으로 이루어지는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
According to claim 1 or 2,
The fatty acid is an eco-friendly mite control composition using vegetable oil, characterized in that consisting of oleic acid.
상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물에는 상기 방제용 조성물 100 중량부 대비 채종유, 피마자유, 옥수수유, 해바라기유 및 대두유로 이루어진 그룹에서 선택된 하나 이상으로 이루어진 오일첨가제 10 내지 30 중량부가 더 함유되는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
According to claim 1 or 2,
The eco-friendly mite control composition using the vegetable oil contains 10 to 30 parts by weight of an oil additive consisting of at least one selected from the group consisting of rapeseed oil, castor oil, corn oil, sunflower oil and soybean oil, based on 100 parts by weight of the control composition. Eco-friendly mite control composition using vegetable oil, characterized in that.
상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 정제수에 500 내지 750배로 희석되어 사용되는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.
According to claim 1 or 2,
Eco-friendly mite control composition using vegetable oil, characterized in that the eco-friendly mite control composition using vegetable oil is used diluted 500 to 750 times in purified water.
상기 식물성 오일을 이용한 친환경 진드기 방제용 조성물은 오일 스프레이, 습윤성 분말, 유동물 과립, 에어로졸, 훈연제 및 훈증제로 이루어진 그룹에서 선택된 하나의 제형에 적용되는 것을 특징으로 하는 식물성 오일을 이용한 친환경 진드기 방제용 조성물.The method of claim 1,
The eco-friendly mite control composition using the vegetable oil is an eco-friendly mite control composition using vegetable oil, characterized in that it is applied to one formulation selected from the group consisting of oil spray, wettable powder, flow granule, aerosol, smoker and fumigator .
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| KR20200091174A (en) * | 2019-01-22 | 2020-07-30 | 유종철 | Composition for Controlling Red Mite and Feed Comprising the Same |
| KR20210083738A (en) * | 2019-12-27 | 2021-07-07 | 배재대학교 산학협력단 | Composition for acaricide containing cedarwood oil |
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| KR102542124B1 (en) | 2023-06-13 |
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