KR20210002239A - Low irritating natural hairdye for pet - Google Patents
Low irritating natural hairdye for pet Download PDFInfo
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- KR20210002239A KR20210002239A KR1020190077635A KR20190077635A KR20210002239A KR 20210002239 A KR20210002239 A KR 20210002239A KR 1020190077635 A KR1020190077635 A KR 1020190077635A KR 20190077635 A KR20190077635 A KR 20190077635A KR 20210002239 A KR20210002239 A KR 20210002239A
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
- A61Q5/065—Preparations for temporary colouring the hair, e.g. direct dyes
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
Description
본 발명은 애완견 등을 포함하는 반려동물용 천연 염모제에 관한 것으로서, 일반적으로 사람 모발에 사용되는 염모제의 경우 피부자극성이 높아 반려동물에 사용하기에 부적합한 단점을 해소하기 위하여, 물(water);하이드록시에틸셀룰로오스(Hydroxy ethylcellulos); 카보머(Carbomer; 2% Solution); 천연염료; 양파외피추출물; 소목추출물; 밤꽃향료; 95% 에탄올(Ethanol, 95%); 벤질알코올(Benzyl Alcohol); 메틸피롤리돈(Methyl pyrrolidone); 글리콜산(Glycolic acid)을 포함함으로써 피부자극성이 낮고 반려동물들이 선호하는 방향성으로 인해, 소비자들의 사용만족도를 높일 수 있는 반려동물용 피부 저자극성 천연 염모제에 관한 것이다.The present invention relates to a natural hair dye for companion animals including pet dogs, and in general, in the case of hair dyes used for human hair, in order to solve the disadvantages that are not suitable for use in companion animals due to high skin irritation, water; Hydroxyethylcellulose (Hydroxy ethylcellulos); Carbomer (2% Solution); Natural dyes; Onion skin extract; Bovine extract; Chestnut fragrance; 95% ethanol (Ethanol, 95%); Benzyl Alcohol; Methyl pyrrolidone; The present invention relates to a hypoallergenic natural hair dye for companion animals that can increase consumer satisfaction due to low skin irritation and aroma favored by companion animals by including glycolic acid.
1인 가구수의 급증과 고령화에 따른 인구구조의 변화, 소득수준의 향상 등으로 인해 반려동물을 보유하고 있는 가구수는 점차 증가추세에 있다.The number of households with companion animals is on a gradual increase due to the rapid increase in the number of single-person households, changes in the demographic structure due to aging, and the improvement of income levels.
이와 같은 변화는 반려동물을 뜻하는 '펫(Pet)'과 가족을 의미하는 '패밀리(Family)'를 합친‘펫팸족(Pet+Family)’이라는 신조어를 탄생시키고, 반려동물 TV채널 서비스가 제공되고 있으며, 반려동물관리사, 반려동물행동교정사, 반려동물장례지도사 등을 유망직종으로 인지시키고 있다. 뿐만 아니라 반려동물을 위한 보험, 펫신탁 등 금융서비스도 출현하였다.This change has created a new term'Pet+Family', which combines'Pet' meaning companion animal and'Family' meaning family, and companion animal TV channel service is provided. Companion animal managers, companion animal behavior correctors, and companion animal funeral instructors are recognized as promising occupations. In addition, financial services such as insurance for companion animals and pet trust have also emerged.
이와 같은 시대 흐름에 맞춰 펫 숍(pet shop)과 애견미용사 등의 활동 또한 활발해지고 있으며, 애완동물의 건강과 미용을 제공해주는 헬스뷰티형 사업이 유망사업으로 떠오르고 있다.In line with this trend, activities such as pet shops and dog hairdressers are also becoming active, and health beauty-type businesses that provide health and beauty of pets are emerging as promising businesses.
본 발명은 이와 같은 현 흐름에 맞춰 반려동물 미용에 관련된 모발 염색에 사용되는 염모제를 제공하고자 한다. 시중에 판매되고 있는 제품의 대부분은 사람의 모발에 최적화된 것으로서 반려동물에 사용하기에는 피부자극성이 높아 사용 적합성이 떨어진다. 이와 같은 문제는 시중에 애완동물용이라고 사용되는 염색약에도 동일 적용된다.An object of the present invention is to provide a hair dye used for dyeing hair related to pet beauty in accordance with the current trend. Most of the products on the market are optimized for human hair, and they are highly irritating to the skin for use with companion animals, making them less suitable for use. The same problem applies to hair dyes that are commercially used for pets.
따라서 본 발명에서는 이와 같은 종래 기술의 문제점을 해소하고자, 피부자극성이 낮고 반려동물들이 좋아하는 향을 포함함으로써 반려동물의 털 염색에 최적화된 염모제를 제공하고자 한다.Therefore, in the present invention, in order to solve the problems of the prior art, it is intended to provide a hair dye optimized for dyeing the hair of companion animals by including a fragrance that has low skin irritation and likes companion animals.
본 발명과 관련하여, 대한민국 등록특허 10-1625470(등록일자 2016.05.24) '천연성분을 함유하는 산화염색용 염모제 조성물'; 대한민국 공개특허 10-2018-0080412(공개일자 2018.07.12) '천연허브파우더를 함유하는 태블릿 염모제 조성물'; 대한민국 등록특허 10-0540795(등록일자 2005.12.27) '천연 식물성 염모제 조성물 및 염모제와 그를 이용한 모발염색방법'; 대한민국 등록특허 10-1562615(등록일자 2015.10.16) '천연성분을 함유하는 1제형 산화형 염모제 조성물'; 대한민국 등록특허 10-1336966(등록일자 2013.11.28) '천연의 식물 추출물을 포함하며, 염색시간이 빠른 비산화형 염모제 조성물 및 그의 제조방법'; 및 대한민국 등록특허 10-0850928(등록일자 2008.08.01) '천연 추출물을 포함한 염모제용 조성물 및 제조방법';에 대한 기술이 개시된 바 있다.In connection with the present invention, Korean Patent Registration No. 10-1625470 (registration date 2016.05.24)'a hair dye composition for oxidation dyeing containing natural ingredients'; Republic of Korea Patent Publication 10-2018-0080412 (published date 2018.07.12)'Tablet hair dye composition containing natural herb powder'; Republic of Korea Patent Registration 10-0540795 (Registration date 2005.12.27)'Natural vegetable hair dye composition and hair dye and hair dyeing method using the same'; Republic of Korea Patent Registration 10-1562615 (registration date 2015.10.16)'one formulation oxidized hair dye composition containing natural ingredients'; Republic of Korea Patent Registration 10-1336966 (registration date 2013.11.28)'Non-oxidized hair dye composition comprising a natural plant extract, dyeing time is fast and its manufacturing method'; And Korean Patent Registration No. 10-0850928 (registration date 2008.08.01)'Composition and preparation method for hair dye including natural extract'; has been disclosed.
이와 같은 등록특허 및 공개특허에 개시된 염모제 또한 사람 모발에 최적화된 것으로서 본 발명에 따란 반려동물용 염모제로 사용하기에 적합하지 않다는 문제가 있다.The hair dye disclosed in such registered patents and published patents is also optimized for human hair and has a problem that it is not suitable for use as a hair dye for companion animals according to the present invention.
본 발명은 애완견 등을 포함하는 반려동물용 천연 염모제에 관한 것으로서, 일반적으로 사람 모발에 사용되는 염모제의 경우 피부자극성이 높아 반려동물에 사용하기에 부적합한 단점을 해소하기 위하여, 물(water);하이드록시에틸셀룰로오스(Hydroxy ethylcellulos); 카보머(Carbomer; 2% Solution); 천연염료; 양파외피추출물; 소목추출물; 밤꽃향료; 95% 에탄올(Ethanol, 95%); 벤질알코올(Benzyl Alcohol); 메틸피롤리돈(Methyl pyrrolidone); 글리콜산(Glycolic acid)을 포함함으로써 피부자극성이 낮고 반려동물들이 선호하는 방향성으로 인해, 소비자들의 사용만족도를 높일 수 있는 반려동물용 피부 저자극성 천연 염모제를 제공하고자 하는 것을 발명의 목적으로 한다.The present invention relates to a natural hair dye for companion animals including pet dogs, and in general, in the case of hair dyes used for human hair, in order to solve the disadvantages that are not suitable for use in companion animals due to high skin irritation, water; Hydroxyethylcellulose (Hydroxy ethylcellulos); Carbomer (2% Solution); Natural dyes; Onion skin extract; Bovine extract; Chestnut fragrance; 95% ethanol (Ethanol, 95%); Benzyl Alcohol; Methyl pyrrolidone; It is an object of the invention to provide a hypoallergenic natural hair dye for companion animals that can increase consumer satisfaction due to low skin irritation and aroma favored by companion animals by including glycolic acid.
상기 목적을 달성하기 위하여,To achieve the above object,
본 발명은,The present invention,
염모제의 전체 중량에 대해,With respect to the total weight of the hair dye,
천연염료 1.0 ~ 3.0 wt%,1.0 to 3.0 wt% of natural dye,
양파외피추출물 0.5 ~ 2.0 wt% 및Onion skin extract 0.5 ~ 2.0 wt% and
소목추출물 0.5 ~ 2.0 wt%Beefwood extract 0.5 ~ 2.0 wt%
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%를 포함하여 100.0 wt%를 구성하는 반려동물용 피부 저자극성 천연 염모제를 제공한다.Provides a skin hypoallergenic natural hair dye for companion animals comprising 100.0 wt%, including 0.1 to 0.5 wt% of fragrance selected from Vetiver fragrance, chestnut flower fragrance, or eucalyptus fragrance.
더욱 상세하게는,More specifically,
물(water) 40.0 ~ 55.0 wt%와, 40.0 to 55.0 wt% of water,
하이드록시에틸셀룰로오스(Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%와,Hydroxyethylcellulose (Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%,
카보머(Carbomer; 2% Solution) 10.0 ~ 15.0 wt%와,Carbomer (2% Solution) 10.0 ~ 15.0 wt% and,
천연염료 1.0 ~ 3.0 wt%와,1.0 to 3.0 wt% of natural dyes,
양파외피추출물 0.5 ~ 2.0 wt%와,0.5 to 2.0 wt% of onion skin extract,
소목추출물 0.5 ~ 2.0 wt%와,0.5 ~ 2.0 wt% of bovine extract and,
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%와,0.1 to 0.5 wt% of a fragrance selected from among vetiver fragrance, chestnut fragrance or eucalyptus fragrance,
95% 에탄올(Ethanol, 95%) 13.0 ~ 20.0 wt%와,95% ethanol (Ethanol, 95%) 13.0 to 20.0 wt%,
벤질알코올(Benzyl Alcohol) 5.0 ~ 12.0 wt%와,5.0 to 12.0 wt% of Benzyl Alcohol,
메틸피롤리돈(Methyl pyrrolidone) 5.0 ~ 10.0 wt%와,5.0 ~ 10.0 wt% of methyl pyrrolidone,
글리콜산(Glycolic acid) 2.0 ~ 6.0 wt%를 포함하는 반려동물용 피부 저자극성 천연 염모제를 제공한다.Provides a hypoallergenic natural hair dye for companion animals containing 2.0 to 6.0 wt% of glycolic acid.
본 발명에 따른 반려동물용 피부 저자극성 천연 염모제는 다음의 효과를 갖는다.The hypoallergenic natural hair dye for companion animals according to the present invention has the following effects.
첫째. 천연염료와 천연재료를 사용함으로써 가려움, 발진, 진물 등의 문제를 발생을 예방할 수 있으며, 피부에 대한 자극성이 낮기 때문에 애완견 등의 반려동물용으로 사용하기에 적합하다는 장점을 갖는다.first. The use of natural dyes and natural materials can prevent itchiness, rash, and sores, and has the advantage of being suitable for use as companion animals such as pet dogs because of low irritation to the skin.
둘째. 양파외피추출물 및 소목 추출물의 사용으로 피부자극성을 낮추면서 동시에 염색성을 향상시킬 수 있다는 장점을 갖는다.second. It has the advantage of improving dyeability while lowering skin irritation by using onion skin extract and botanical extract.
셋째. 애완견 등의 반려동물들이 좋아하는 흙냄새, 꽃냄새 및 풀냄새가 풍겨 염색작업에 대한 반려동물들의 거부감을 저감시켜 원활한 염색이 이루어질 수 있다.third. The smell of soil, flowers, and grass, which pets and other pets like, can reduce the resistance of pets to the dyeing process, so that seamless dyeing can be achieved.
이하, 본 발명에 따른 반려동물용 피부 저자극성 천연 염모제의 구체적인 기술 구성을 살펴보도록 한다.Hereinafter, a detailed technical configuration of the hypoallergenic natural hair dye for companion animals according to the present invention will be described.
상기한 바와 같이,As mentioned above,
본 발명에 따른 반려동물용 피부 저자극성 천연 염모제는The hypoallergenic natural hair dye for companion animals according to the present invention
염모제의 전체 중량에 대해,With respect to the total weight of the hair dye,
천연염료 1.0 ~ 3.0 wt%,1.0 to 3.0 wt% of natural dye,
양파외피추출물 0.5 ~ 2.0 wt% 및Onion skin extract 0.5 ~ 2.0 wt% and
소목추출물 0.5 ~ 2.0 wt%Beefwood extract 0.5 ~ 2.0 wt%
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%를 포함하여 100.0 wt%를 구성한다. It constitutes 100.0 wt%, including 0.1 to 0.5 wt% of a fragrance selected from among vetiver fragrances, chestnut fragrances, or eucalyptus fragrances.
더욱 상세하게는,More specifically,
물(water) 40.0 ~ 55.0 wt%와, 40.0 to 55.0 wt% of water,
하이드록시에틸셀룰로오스(Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%와,Hydroxyethylcellulose (Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%,
카보머(Carbomer; 2% Solution) 10.0 ~ 15.0 wt%와,Carbomer (2% Solution) 10.0 ~ 15.0 wt% and,
천연염료 1.0 ~ 3.0 wt%와,1.0 to 3.0 wt% of natural dyes,
양파외피추출물 0.5 ~ 2.0 wt%와,0.5 to 2.0 wt% of onion skin extract,
소목추출물 0.5 ~ 2.0 wt%와,0.5 ~ 2.0 wt% of bovine extract and,
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%와,0.1 to 0.5 wt% of a fragrance selected from among vetiver fragrance, chestnut fragrance or eucalyptus fragrance,
95% 에탄올(Ethanol, 95%) 13.0 ~ 20.0 wt%와,95% ethanol (Ethanol, 95%) 13.0 to 20.0 wt%,
벤질알코올(Benzyl Alcohol) 5.0 ~ 12.0 wt%와,5.0 to 12.0 wt% of Benzyl Alcohol,
메틸피롤리돈(Methyl pyrrolidone) 5.0 ~ 10.0 wt%와,5.0 ~ 10.0 wt% of methyl pyrrolidone,
글리콜산(Glycolic acid) 2.0 ~ 6.0 wt%를 포함한다.It contains 2.0 to 6.0 wt% of glycolic acid.
이하, 상기 반려동물용 피부 저자극성 천연 염모제를 구성하는 각 성분들에 대한 구체적인 내용에 대해 살펴보도록 한다.Hereinafter, detailed contents of each component constituting the hypoallergenic natural hair dye for companion animals will be described.
1) 물(water)1) water
상기 물(water)은 천연 염모제를 구성하는 성분들을 용해시키기 위한 용매로서, 그 사용량이 40.0 wt% 미만인 경우에는 각 성분간의 균일 배합조성이 제대로 이루어지지 않아 염모제의 색상발현, 염착성 등의 전반적인 기능성이 떨어질 우려가 있고, 55.0 wt%를 초과하게 되는 경우에는 흐름성이 너무 높아 염색작업이 원활하게 이루어지지 않을 수 있으므로, 상기 물(water)은 염모제의 전체 중량에 대해 40.0 ~ 55.0 wt%의 범위내로 한정하는 것이 바람직하다.The water is a solvent for dissolving the components constituting the natural hair dye, and when the amount is less than 40.0 wt%, the uniform blending composition between the components is not properly achieved, so that the overall functionality such as color expression and dyeing properties of the hair dye is not achieved. There is a risk of dropping, and if it exceeds 55.0 wt%, the flowability is too high and the dyeing operation may not be performed smoothly, so the water is in the range of 40.0 to 55.0 wt% based on the total weight of the hair dye. It is desirable to limit it.
2) 하이드록시에칠셀룰로오스(Hydroxy ethylcellulose) 2) Hydroxy ethylcellulose
상기 하이드록시에칠셀룰로오스(Hydroxy ethylcellulose)는 셀룰로스에 가성소다를 작용시켜 알칼리셀룰로스로 만들어서 이것에 산화에칠렌을 반응시켜 중화, 정제, 건조, 파쇄해서 얻어진 수용성 고분자이다.Hydroxy ethylcellulose (Hydroxy ethylcellulose) is a water-soluble polymer obtained by neutralizing, refining, drying and crushing by reacting ethylene oxide with alkaline cellulose by reacting caustic soda on cellulose.
점도특성은 셀룰로스 본체의 중합도에 의존하며 냉수, 온수에 녹지만 일부를 제외하고 거의 모든 유기용제에 불용이다. 물에 첨가하면 점성 있는 액으로 되고, 일반적으로 농도가 2 배로 되면 점도는 거의 5 ~ 10 배로 된다. 분자량이 클수록 농도가 높을수록 구조점성이 증대된다. 수용액은 pH 2 ~ 12 범위에서 안정하고 특히 pH 4 ~ 11의 범위에서는 장기보존안정성이 뛰어나다.Viscosity characteristics depend on the degree of polymerization of the cellulose body and are soluble in cold water and hot water, but are insoluble in almost all organic solvents except for some. When added to water, it becomes a viscous liquid, and in general, when the concentration is doubled, the viscosity is almost 5 to 10 times. The higher the molecular weight, the higher the concentration, the higher the structural viscosity. The aqueous solution is stable in the range of pH 2 ~ 12, and particularly, has excellent long-term storage stability in the range of pH 4 ~ 11.
일반적으로 점증제, 피막형성제, 유화안정제 등으로 사용되며, 피막형성제로 사용될 경우 모발 등에 얇은 피막을 형성하여 부드럽게 감싸주는 역할을 한다.In general, it is used as a thickening agent, film-forming agent, emulsion stabilizer, etc. When used as a film-forming agent, it forms a thin film on the hair and gently wraps it.
상기 하이드록시에칠셀룰로오스(Hydroxy ethylcellulose)의 사용량이 0.3 wt% 미만인 경우에는 강아지 등의 반려동물의 털에 피막을 형성하여 부드럽게 감싸주는 역할이 미미하고, 1.5 wt%를 초과하게 되는 경우에는 효과의 변화가 미미하여 무의미하므로, 상기 하이드록시에칠셀룰로오스(Hydroxy ethylcellulose)의 사용량은 염모제의 전체 중량에 대해 0.3 ~ 1.5 wt%의 범위내로 한정하는 것이 바람직하다.When the amount of hydroxyethylcellulose is less than 0.3 wt%, the role of forming a film on the fur of companion animals such as dogs and gently wrapping it is insignificant, and when it exceeds 1.5 wt%, the effect is Since the change is insignificant and insignificant, the amount of the hydroxy ethylcellulose used is preferably limited to within the range of 0.3 to 1.5 wt% based on the total weight of the hair dye.
3) 카보머(Carbomer; 2% Solution)3) Carbomer (2% Solution)
상기 카보머는 염모제에 첨가하여, 염색시 제제가 지나치게 흐르는 것을 방지하게 위해 사용된다.The carbomer is added to the hair dye and is used to prevent excessive flow of the preparation during dyeing.
상기 카보머는 화장품에서 가장 보편적으로 사용되고 있는 점증제, 상안정제로 아크릴산(Acrylic Acid)이 중합된 고분자 중합체로서, 알칼리 화합물로 중화되면 투명한 겔 형태로 점증되며 물을 흡수하고 유지하는 능력이 있다. 점증제, 혼합제, 에멀젼 안정제로 겔, 크림, 로션, 샴프 등 다양한 제품에 사용된다.The carbomer is a polymer polymer in which acrylic acid is polymerized as a thickener and phase stabilizer most commonly used in cosmetics. When neutralized with an alkali compound, the carbomer gradually increases in the form of a transparent gel and has the ability to absorb and retain water. It is used in various products such as gels, creams, lotions, and shampoos as a thickener, blending agent, and emulsion stabilizer.
상기 카보머의 사용량이 10.0 wt% 미만인 경우에는 점도가 낮아 지나치게 흐를 수 있고, 15.0 wt%를 초과하게 되는 경우에는 점도가 너무 높아 염색작업이 원활하게 이루어지지 않을 수 있으므로, 상기 카보머의 사용량은 염모제의 전체 중량에 대해 10.0 ~ 15.0 wt%의 범위내로 한정하는 것이 바람직하다.If the amount of carbomer is less than 10.0 wt%, the viscosity is low and may flow excessively, and if it exceeds 15.0 wt%, the viscosity is too high and the dyeing operation may not be performed smoothly, so the amount of carbomer is It is preferable to limit it within the range of 10.0 to 15.0 wt% based on the total weight of the hair dye.
4) 천연염료4) Natural dye
상기 천연염료에는 식물성 염료, 동물성 염료로 크게 구분된다.The natural dyes are largely classified into vegetable dyes and animal dyes.
상기 식물성 염료는 식물의 잎과 꽃, 열매, 나무껍질, 심재와 뿌리 등에서 추출한 염료를 말한다.The plant dye refers to a dye extracted from leaves and flowers, fruits, bark, heartwood and roots of plants.
상기 동물성 염료는 동물의 피, 조개류의 분비물, 오징어 먹물, 붉나무에 기생하는 벌레집 오배자, 선인장에 기생하는 벌레(코치닐) 등에서 얻을 수 있는 염료이다.The animal dyes are dyes that can be obtained from animal blood, secretions of shellfish, squid ink, worms nests parasitic on red trees, insects parasitic on cacti (cochinil), and the like.
본 발명은 상기 식물성 염료를 사용한다.The present invention uses the above vegetable dyes.
더욱 구체적으로는,More specifically,
쪽, 대청, 인도람, 송람, 소송목, 유구염 또는 패자 중 선택되는 어느 1종 이상의 보라계 염료; 황련, 황백, 히드라스티스, 산딸기나무, 치자, 샤프란 또는 홍목 중 선택되는 어느 1종 이상의 황색계 염료; 봉선화, 닭의 장풀, 두약 또는 산람 중 선택되는 어느 1종 이상의 홍색계 염료; 쑥의 녹색계염료 중 선택되는 단색성염료와,Any one or more purple dyes selected from indigo, daecheong, indoram, songram, lawsuit, yugyeom, or loser; Any one or more yellow dyes selected from yellow lotus, yellow white, hydratis, raspberry, gardenia, saffron, or redwood; Any one or more red dyes selected from balsam, chicken's long grass, tofu or sanlam; A monochromatic dye selected among green dyes of mugwort,
억새, 코스모스, 떡갈나무, 금은화, 칡, 토끼풀; 감초, 황금, 박하; 철쭉, 화금, 녹차; 양파, 동백잎, 봉선화, 괴화, 무궁화, 굴껍질, 피마자, 머위, 측백나무, 달맞이꽃, 은행나무, 녹차, 접시꽃, 호두나무, 호장근; 메밀, 무화과, 부들, 수둑, 천일홍, 익모초, 목련, 괴화; 칡, 새삼, 호두나무, 봉선화, 접시꽃; 적채, 자색고구마, 포도과피, 오미자, 갓, 유색미, 나무딸기, 블랙베리, 버찌, 미국자리공, 광나무, 함초, 담쟁이덩굴; 오배자, 상수리나무, 오리나무, 오이풀, 대추나무, 밤, 커피, 미역취, 박하, 호두나무, 메밀; 석류, 감, 호두나무, 대황; 지초; 호두나무; 코치닐, 호장근, 꼭두서니, 락, 원추리, 대황, 케르메스; 중 선택되는 다색성 염료 중에서 선택되는 것을 사용한다.Silver grass, cosmos, oak, gold and silver coins, arrowroot, shamrock; Licorice, golden, mint; Azaleas, hwageum, green tea; Onion, Camellia leaves, Balsam, Goehwa, Mugunghwa, Oyster bark, Castor, Butterbur, Japanese cypress, Evening primrose, Ginkgo biloba, Green tea, hollyhock, Walnut, Hojanggeun; Buckwheat, figs, cattails, suduk, cheonilhong, motherwort, magnolia, gohwa; Arrowroot, saesam, walnut, balsam, hollyhock; Red vegetables, purple sweet potatoes, grape skin, schisandra chinensis, mustard, colored rice, raspberries, blackberries, cherries, American sprigs, mineral trees, green tea, ivy; Obaeja, oak, alder, cucumber grass, jujube, chestnut, coffee, seaweed, mint, walnut, buckwheat; Pomegranate, persimmon, walnut, rhubarb; Branch; Walnut tree; Cochineal, Hojanggeun, Madder, Rock, Wonchuri, Rhubarb, Kermes; Among the polychromatic dyes selected from among them are used.
상기 단색성염료는 주성분이 인디고노이드류(Indigonoids)이며, 색상이 보라계인 쪽(요람), 대청, 인도람, 송람, 소송목, 유구염, 패자가 있고,The monochromatic dye has a main component of indigonoids, and has a purple color (cradle), Daecheong, Indiaram, Songram, suit tree, yuguyeom, and losers,
주성분이 카로티노이드류(Carotenoids)이며, 색상이 황색계인 치자, 샤프란, 홍목이 있고,The main component is carotenoids, and there are gardenia, saffron, and redwood that are yellow in color.
주성분이 알칼로이드류(Alkaloids), 베르베린(Berberrine)이며, 색상이 황색계인 황련, 황백, 히드라스티스, 산딸기나무가 있고,The main components are alkaloids and berberine, and there are yellow lotus, yellow white, hydratis, and raspberry trees.
주성분이 안토시안류(Anthocyans)이며, 색상이 홍색계인 봉선화, 닭의 장풀, 두약, 산람이 있고,The main component is Anthocyans, and there are red-colored balsam, chicken's long grass, bean paste, and sanlam.
주성분이 클로로필(Chlorophyll)이며, 색상이 녹색계인 쑥 등 녹엽이 있고,The main component is chlorophyll, and there are green leaves such as mugwort, which has a green color,
주성분이 칼콘류(Chalkones), 카르타민(Carthamin)이며, 색상이 황색계이거나 적색계인 홍화가 있다.The main constituents are Chalcones and Cartamine, and there are safflowers that are yellow or red in color.
상기 홍화의 경우, 추출방법에 따라 색소가 다르다. 물에서 추출할 경우에는 황색계이나, 알칼리에서 추출하면 적색계이다.In the case of the safflower, the pigment is different depending on the extraction method. It is yellow when extracted from water, but red when extracted with alkali.
상기 다색성염료는 주성분이 플라본류(Flavons)이며, 색상이 황색 ~ 갈색인 억새, 코스모스, 떡갈나무, 금은화, 칡, 토끼풀이 있고,The polychromatic dye is mainly composed of flavones, and has yellow to brown silver grass, cosmos, oak, gold and silver, arrowroot, and shamrock,
주성분이 플라바논류(Flavaons)이며, 색상이 황색 ~ 갈색인 감초, 황금, 박하가 있고,The main component is Flavaons, and there are licorice, gold, and mint with yellow to brown color.
주성분이 플라바놀류(Flavanols)이며, 색상이 황색 ~ 갈색인 철쭉, 화금, 녹차가 있고,The main ingredient is flavanols, and there are yellow to brown azaleas, hwageum, and green tea.
주성분이 쿠에르세틴이며, 색상이 적색 ~ 청색인 양파, 동백잎, 봉선화, 괴화, 무궁화, 굴껍질, 피마자, 머위, 측백나무, 달맞이꽃, 은행나무, 녹차, 접시꽃, 호두나무, 호장근이 있고,The main ingredient is quercetin, and there are red to blue onions, camellia leaves, balsam, gooseberries, hibiscus, oyster bark, castor, butterbur, cypress, evening primrose, ginkgo, green tea, hollyhock, walnut, and walnut root. ,
주성분이 루틴이며, 색상이 적색 ~ 청색인 메밀, 무화과, 부들, 수국, 천일홍, 익모초, 목련, 괴화가 있고,The main ingredient is rutin, and there are buckwheat, figs, cattails, hydrangea, Cheon-ilhong, motherwort, magnolia, and Goehwa in color red to blue.
주성분이 캠페롤이며, 색상이 적색 ~ 청색인 칡, 새삼, 호두나무, 봉선화, 접시꽃이 있고,The main ingredient is camperol, and there are arrowroot, saesam, walnut tree, balsam, and hollyhock flowers in red to blue color.
주성분이 안토시안류(Anthocyans)이며, 색상이 적색 ~ 청색인 적채, 자색고구마, 포도과피, 오미자, 갓, 유색미, 나무딸기, 블랙베리, 버찌, 미국자리공, 광나무, 함초, 담쟁이덩굴이 있고,The main component is Anthocyans, and there are red to blue red, purple sweet potatoes, grape skin, schisandra, goat, colored rice, raspberries, blackberries, cherries, American sprigs, light wood, green tea, and ivy.
주성분이 피로가롤탄닌계이며, 색상이 흑색(Fe)인 오배자, 상수리나무, 오리나무, 오이풀, 대추나무, 밤이 있고,The main component is pyrogarol tannin, and the color is black (Fe), and there are five baeja, oak, alder, cucumber grass, jujube, and chestnut.
주성분이 자규로탄닌계이며, 색상이 갈색(Al), 흑색(Fe)인 석류가 있고,There are pomegranates with brown (Al) and black (Fe) colors, and the main component is jagurotannin,
주성분이 커피탄닌계이며, 색상이 흑색(Fe)인 커피, 미역취, 박하, 호두나무, 메밀이 있고,The main ingredient is coffee tannin, and there are black (Fe) color coffee, seaweed odor, mint, walnut, and buckwheat.
주성분이 카테롤탄닌계이며, 색상이 갈색(Al), 흑색(Fe)인 감, 호두나무, 대황이 있고,The main component is caterol tannin, and there are brown (Al), black (Fe) persimmon, walnut, and rhubarb.
주성분이 시코닌이며, 색상이 자색(Al)인 지초가 있고,The main component is sikonin, and there is a branch with a purple color (Al),
주성분이 주글린이며, 색상이 갈색(Al)인 호두나무가 있고,The main component is zuglin, and there is a walnut tree with a brown color (Al),
주성분이 안트라퀴논류(Anthraquinones)이며, 색상이 적색, 흑색인 코치닐,호장근, 꼭두서니, 락, 원추리, 대황, 케르메스가 있고,The main ingredient is anthraquinones, and there are red and black cochineal, chowjanggeun, madder, rock, wonchuri, rhubarb, and kermes.
주성분이 브라실레인(Brazilin)이며, 색상이 적자색, 자색인 소목이 있다.The main component is Brasilin, and there are red-purple and purple-colored small trees.
상기 쿠에르세틴, 루틴, 캠페롤 성분은 플라보놀류(Flavonols)이고, The quercetin, rutin, and camperol components are flavonols,
상기 피로가롤탄닌계, 자규로탄닌계, 커피탄닌계, 카테롤탄닌계 성분은 탄닌류(Tannins)이고,The pyrogarol tannin-based, jagyro tannin-based, coffee tannin-based, and caterol tannin-based components are tannins,
상기 시코닌, 주글린 성분은 나프토퀴논류(Naphthoquinones)이다.The sikonin and juglin components are naphthoquinones.
상기 염료의 사용량이 1.0 wt% 미만인 경우에는 색상 발현이 제대로 이루어지지 않을 수 있고, 3.0 wt%를 초과하게 되는 경우에는 색상에 큰 변화가 없어 무의미하므로, 상기 염료의 사용량은 염모제의 전체 중량에 대해 1.0 ~ 3.0 wt%의 범위내로 한정하는 것이 바람직하다.If the amount of the dye is less than 1.0 wt%, color expression may not be properly achieved, and if it exceeds 3.0 wt%, there is no significant change in color and is meaningless, so the amount of the dye is based on the total weight of the hair dye. It is preferable to limit it within the range of 1.0 to 3.0 wt%.
5) 양파외피추출물5) Onion skin extract
상기 양파외피추출물은 모발 염색시 모발 손상을 최소화하면서 염색성이 우수하기 때문에 무매염으로 염색이 가능하도록 한다. 또한 피부조직에서 유해산소 물질의 생성이 적고, 유해산소는 빨리 제거하는 역할을 하기 때문에 산화 스트레스가 완화되어 조직 손상이 적게 나타난다. 이로써 피부자극을 완화시키는 역할을 한다.Since the onion skin extract has excellent dyeing properties while minimizing hair damage during hair dyeing, it is possible to dye without mordant. In addition, since there is little generation of harmful oxygen substances in the skin tissue and the role of removing harmful oxygen quickly, oxidative stress is alleviated, resulting in less tissue damage. This serves to relieve skin irritation.
상기 양파외피추출물은, The onion skin extract,
양파껍질을 세척하고, 암소에서 건조한 후 건식분쇄기로 분쇄하여 분말을 제조하고,Wash the onion skin, dry it in the dark, and pulverize it with a dry grinder to prepare a powder.
상기 양파껍질 분말을 정제수와 동 중량비로 혼합하고,Mixing the onion skin powder with purified water at the same weight ratio,
100 ℃에서 100 ~ 150 분 동안 가열하여 액상 추출을 하고,Liquid extraction is performed by heating at 100° C. for 100 to 150 minutes,
상기 액상 추출한 추출물을 글래스 필터(glass filter)로 필터링하고,Filtering the liquid extract extracted with a glass filter,
상기 필터링한 추출물을 회전감압농축기(Rotary evaporator)를 이용하여 63℃에서 15 시간 동안 감압농축하고,The filtered extract was concentrated under reduced pressure at 63° C. for 15 hours using a rotary evaporator,
상기 감압농축한 추출물을 동결건조기(Freeze dryer)로 건조하여 분말로 제조한 것을 사용한다.The extract concentrated under reduced pressure is dried with a freeze dryer to form a powder.
상기 양파외피추출물의 사용량이 0.5 wt% 미만인 경우에는 염색성이 떨어지고, 피부자극 완화 기능성이 떨어질 수 있고, 2.0 wt%를 초과하게 되는 경우에는 염색성 및 피부자극 완화 기능의 향상정도가 미미하여 무의미하므로, 상기 양파외피추출물의 사용량은 염모제의 전체 중량에 대해 0.5 ~ 2.0 wt%의 범위내로 한정하는 것이 바람직하다.If the amount of the onion skin extract is less than 0.5 wt%, the dyeing property may be deteriorated and the skin irritation relief function may be deteriorated. The amount of the onion skin extract is preferably limited to 0.5 to 2.0 wt% based on the total weight of the hair dye.
6) 소목추출물6) Cattle extract
상기 소목추출물은 염색효과와 모발보호효과를 갖는 것으로서,The somok extract has a dyeing effect and a hair protection effect,
상기 소목추출물은,The joiner extract,
분쇄한 소목 분말과 메탄올(Methanol)을 1 : 5 ~ 10 중량비로 혼합하고,Mix the pulverized joiner powder and methanol in a ratio of 1: 5 to 10 by weight,
33 ~ 34 ℃에서 20시간씩 3회 진탕하여 추출하고,Extract by shaking three times at 33 ~ 34 ℃ for 20 hours each,
추출물을 글래스 필터(glass filter)로 필터링하고,Filtering the extract with a glass filter,
상기 필터링한 추출물을 회전감압농축기(Rotary evaporator)를 이용하여 63℃에서 15 시간 동안 감압농축하고,The filtered extract was concentrated under reduced pressure at 63° C. for 15 hours using a rotary evaporator,
상기 감압농축한 추출물을 동결건조기(Freeze dryer)로 건조하여 분말로 제조된 것을 사용한다.The extract concentrated under reduced pressure is dried with a freeze dryer to form a powder.
상기 소목추출물의 사용량이 0.5 wt% 미만인 경우에는 염색효과와 모발보호효과가 미미하고, 2.0 wt%를 초과하게 되는 경우에는 염색효과와 모발보호효과의 상승정도가 미미하여 무의미하므로, 상기 소목추출물의 사용량은 염모제의 전체 중량에 대해 0.5 ~ 2.0 wt%의 범위내로 한정하는 것이 바람직하다.If the amount of the joiner extract is less than 0.5 wt%, the dyeing effect and the hair protection effect are insignificant, and if it exceeds 2.0 wt%, the degree of increase of the dyeing effect and the hair protection effect is insignificant, so the amount of the joiner extract is used. It is preferable to limit it within the range of 0.5 to 2.0 wt% based on the total weight of the silver hair dye.
7) 향료7) spices
상기 향료는 강아지 등의 동물들이 좋아하는 흙냄새, 꽃냄새, 풀냄새를 유사하게 풍기는 향료를 사용한다.The fragrance is a fragrance that resembles the smell of soil, flowers, and grass that animals such as dogs like.
보다 구체적으로는 베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택하여 사용한다.More specifically, it is used by selecting one of vetiver fragrance, chestnut flower fragrance, or eucalyptus fragrance.
상기 베티버(Vetiver) 향료는 흙냄새와 유사한 냄새를 풍기는 것으로서, 인도와 벵골이 원산지인 베티버(Vetiver)로부터 추출된 향료이다. 그리고 상기 유칼립투스 향료는 풀냄새를 풍긴다.The Vetiver fragrance has a smell similar to the earthy odor, and is a fragrance extracted from Vetiver, which is originated from India and Bengal. And the eucalyptus fragrance gives off the smell of grass.
상기 향료의 사용량이 0.1 wt% 미만인 경우에는 향의 발산이 미미하고, 0.5 wt%를 초과하는 경우에는 향이 너무 강하여 거부감이 생길 수 있으므로, 상기 향료의 사용량은 염모제의 전체 중량에 대해 0.1 ~ 0.5 wt%의 범위내로 한정하는 것이 바람직하다.If the amount of the perfume is less than 0.1 wt%, the scent emission is insignificant, and if it exceeds 0.5 wt%, the scent may be too strong and a feeling of rejection may occur.The amount of the perfume is 0.1 to 0.5 wt% based on the total weight of the hair dye. It is preferable to limit it within the range of %.
8) 95% 에탄올(Ethanol, 95%)8) 95% ethanol (Ethanol, 95%)
상기 95% 에탄올은 상기 물(water)과 함께 분말 천연염료를 녹이는 용매로서, 그 사용량이 13.0 wt% 미만인 경우에는 천연염료가 균일하게 퍼지지 않는 문제가 있고, 20.0 wt%를 초과하게 되는 경우에는 필요 이상의 사용으로 인해 무의미하므로, 상기 95% 에탄올은 염모제의 전체 중량에 대해 13.0 ~ 20.0 wt%의 범위내로 한정하는 것이 바람직하다.The 95% ethanol is a solvent that dissolves the powdered natural dye together with the water, and if the amount is less than 13.0 wt%, there is a problem that the natural dye does not spread evenly, and it is necessary if it exceeds 20.0 wt%. Since it is meaningless due to the above use, the 95% ethanol is preferably limited to within the range of 13.0 to 20.0 wt% based on the total weight of the hair dye.
9) 벤질알코올(Benzyl Alcohol)9) Benzyl Alcohol
상기 벤질알코올은 천연염료의 염착속도를 향상시키기 위한 용매로서, 그 사용량이 5.0 wt% 미만인 경우에는 염착속도 향상이 거의 일어나지 않고, 12.0 wt%를 초과하게 되는 경우에는 염착속도 향상 정도가 미미하여 무의미하므로, 상기 벤질알코올은 염모제의 전체 중량에 대해 5.0 ~ 12.0 wt%의 범위내로 한정하는 것이 바람직하다.The benzyl alcohol is a solvent for improving the dyeing speed of natural dyes, and if the amount is less than 5.0 wt%, the dyeing speed is hardly improved, and if it exceeds 12.0 wt%, the degree of dyeing speed improvement is insignificant and meaningless. , The benzyl alcohol is preferably limited to 5.0 to 12.0 wt% of the total weight of the hair dye.
10) 메틸피롤리돈(Methyl pyrrolidone)10) Methyl pyrrolidone
상기 메틸피롤리돈(Methyl pyrrolidone)은 점성이 있는 고분자물질의 표면장력을 낮춰주는 용매로서, 그 사용량이 5.0 wt% 미만으로 사용하게 되는 경우에는 표면장력을 낮춰 젖음성을 향상시키는 기능이 떨어지고, 10.0 wt%를 초과하게 되는 경우에는 상기 젖음성 향상 정도가 미미하여 무의미하므로, 상기 메틸피롤리돈(Methyl pyrrolidone)은 염모제의 전체 중량에 대해 5.0 ~ 10.0 wt%의 범위내로 한정하는 것이 바람직하다.The methyl pyrrolidone (Methyl pyrrolidone) is a solvent that lowers the surface tension of a viscous polymer material, and when the amount is less than 5.0 wt%, the function of improving wettability by lowering the surface tension decreases, 10.0 When the weight% is exceeded, the degree of improvement of the wettability is insignificant and thus the degree of improvement of the wettability is insignificant. Therefore, the methyl pyrrolidone is preferably limited to 5.0 to 10.0 wt% based on the total weight of the hair dye.
11) 글리콜산(Glycolic acid)11) Glycolic acid
상기 글리콜산은 pH 조절제로서, 적정 범위의 pH를 조절하기 위하여 염모제의 전체 중량에 대해 2.0 ~ 6.0 wt%의 범위내에서 사용한다. The glycolic acid is a pH adjusting agent, and is used within the range of 2.0 to 6.0 wt% based on the total weight of the hair dye in order to adjust the pH in an appropriate range.
구체적인 배합예는 다음의 표 1과 같다.Specific mixing examples are shown in Table 1 below.
0.8
0.8
1.0
1.0
1.5
1.5
0.7
0.7
0.5
0.5
12.5
12.5
13.0
13.0
14.0
14.0
11.0
11.0
10.0
10.0
베티버(Vetiver) 향료
Vetiver fragrance
0.2
0.2
0.1
0.1
0.3
0.3
0.4
0.4
0.5
0.5
14.0
14.0
15.0
15.0
13.0
13.0
16.0
16.0
13.0
13.0
8.0
8.0
9.0
9.0
6.0
6.0
5.0
5.0
5.0
5.0
8.0
8.0
9.0
9.0
6.0
6.0
5.0
5.0
6.0
6.0
4.0
4.0
4.0
4.0
6.0
6.0
5.3
5.3
6.0
6.0
* 상기 표 1의 천연염료는 쪽, 대청, 인도람, 송람, 소송목, 유구염 또는 패자 중 선택되는 어느 1종 이상의 보라계 염료; 황련, 황백, 히드라스티스, 산딸기나무, 치자, 샤프란 또는 홍목 중 선택되는 어느 1종 이상의 황색계 염료; 봉선화, 닭의장풀, 두약 또는 산람 중 선택되는 어느 1종 이상의 홍색계 염료; 쑥의 녹색계염료 중 선택되는 단색성염료와,* The natural dyes in Table 1 above include any one or more purple dyes selected from indigo, daecheong, indoram, songram, somok, yugu salt, or loser; Any one or more yellow dyes selected from yellow lotus, yellow white, hydratis, raspberry, gardenia, saffron, or redwood; Any one or more red dyes selected from balsam, rooster plant, tofu or sanlam; A monochromatic dye selected among green dyes of mugwort,
억새, 코스모스, 떡갈나무, 금은화, 칡, 토끼풀; 감초, 황금, 박하; 철쭉, 화금, 녹차; 양파, 동백잎, 봉선화, 괴화, 무궁화, 굴껍질, 피마자, 머위, 측백나무, 달맞이꽃, 은행나무, 녹차, 접시꽃, 호두나무, 호장근; 메밀, 무화과, 부들, 수둑, 천일홍, 익모초, 목련, 괴화; 칡, 새삼, 호두나무, 봉선화, 접시꽃; 적채, 자색고구마, 포도과피, 오미자, 갓, 유색미, 나무딸기, 블랙베리, 버찌, 미국자리공, 광나무, 함초, 담쟁이덩굴; 오배자, 상수리나무, 오리나무, 오이풀, 대추나무, 밤, 커피, 미역취, 박하, 호두나무, 메밀; 석류, 감, 호두나무, 대황; 지초; 호두나무; 코치닐, 호장근, 꼭두서니, 락, 원추리, 대황, 케르메스; 소목 중 선택되는 다색성 염료 중에서 선택하여 사용한다.Silver grass, cosmos, oak, gold and silver coins, arrowroot, shamrock; Licorice, golden, mint; Azaleas, hwageum, green tea; Onion, Camellia leaves, Balsam, Goehwa, Mugunghwa, Oyster bark, Castor, Butterbur, Japanese cypress, Evening primrose, Ginkgo biloba, Green tea, hollyhock, Walnut, Hojanggeun; Buckwheat, figs, cattails, suduk, cheonilhong, motherwort, magnolia, gohwa; Arrowroot, saesam, walnut, balsam, hollyhock; Red vegetables, purple sweet potatoes, grape skin, schisandra chinensis, mustard, colored rice, raspberries, blackberries, cherries, American sprigs, mineral trees, green tea, ivy; Obaeja, oak, alder, cucumber grass, jujube, chestnut, coffee, seaweed, mint, walnut, buckwheat; Pomegranate, persimmon, walnut, rhubarb; Branch; Walnut tree; Cochineal, Hojanggeun, Madder, Rock, Wonchuri, Rhubarb, Kermes; It is used by selecting from pleochroic dyes selected among joinery.
이하, 본 발명에 따른 반려동물용 피부 저자극성 천연 염모제에 대한 기능성 실험을 살펴보고자 한다.Hereinafter, a functional experiment for the hypoallergenic natural hair dye for companion animals according to the present invention will be described.
[시험예 1][Test Example 1]
< 피부 자극성 테스트 실험 ><Skin irritation test experiment>
피부자극이란 시험물질을 피부에 최대 4 시간까지 적용하였을 때 피부에 나타나는 가역적 손상으로 피부조직의 국소염증반응에 의해 일어나며 주요 임상증상은 홍반, 부종, 가려움, 통증을 포함하는 가역적인 반응이 특징이다.Skin irritation is a reversible damage to the skin when a test substance is applied to the skin for up to 4 hours.It is caused by a local inflammatory reaction of the skin tissue, and the main clinical symptoms are characterized by reversible reactions including erythema, swelling, itching, and pain. .
상기 피부 자극성 테스트는 백색 토기를 이용한 드레이즈 테스트를 이용한다.The skin irritation test uses a Draise test using white earthenware.
먼저 표 1의 배합예 1에 따라 제조된 천연염모제를 시험예로 하고, 비교예로는 상기 천연염모제에 사용된 원료를 사용하되, 천연염료, 양파외피추출물, 소목추출물 및 향료의 성분을 P-페닐렌디아민으로 대체하여 제조된 염모제를 사용한다.First, a natural hair dye prepared according to Formulation Example 1 in Table 1 is used as a test example, and as a comparative example, the raw materials used for the natural hair dye are used, but the components of natural dyes, onion skin extract, cattlewood extract and fragrance are P- A hair dye prepared by replacing with phenylenediamine is used.
토끼의 피부에 상기 시험예에 따른 천연염모제와 비교예에 따른 염모제를 각각 바른 후, 12시간, 24시간에 홍반 및 가피형성의 유무를 관찰하였다.After applying the natural hair dye according to the test example and the hair dye according to the comparative example to the skin of the rabbit, the presence or absence of erythema and crust formation was observed at 12 and 24 hours.
관찰결과, 12시간 경과 후 시험예에 따른 천연염모제에서는 무반응이 관찰되었으나, 비교예에 따른 염모제에서는 경계가 뚜렷하나 약한 홍반이 관찰되었다.As a result of observation, after 12 hours, no reaction was observed in the natural hair dye according to the test example, but in the hair dye according to the comparative example, the boundary was clear but weak erythema was observed.
그리고 24시간 경과 후에는 시험예에 따른 천연염모제에서는 무반응이 관찰되었으나, 비교예에 따른 염모제에서는 뚜렷한 홍반이 관찰되었다. 가피형성에 대해서는 시험예 및 비교예 모두에서 관찰되지 않았다.In addition, after 24 hours, no reaction was observed in the natural hair dye according to the test example, but distinct erythema was observed in the hair dye according to the comparative example. Crust formation was not observed in both Test Examples and Comparative Examples.
이와 같은 시험결과, 본 발명에 따른 천연 염모제가 종래 시판되고 있는 염모제와 비교하여 피부자극성이 현저히 낮다는 것을 확인할 수 있었다.As a result of such a test, it was confirmed that the natural hair dye according to the present invention has significantly lower skin irritation compared to the conventionally marketed hair dye.
본 발명에 따른 반려동물용 피부 저자극성 천연 염모제는 피부자극성이 매우 낮고 동물들이 좋아하는 향을 포함하고 있어 반려동물 염색에 매우 유용하여 산업상 이용가능성이 크다.The hypoallergenic natural hair dye for companion animals according to the present invention has a very low skin irritation and contains a scent that animals like, so it is very useful for dyeing companion animals and has high industrial applicability.
Claims (5)
천연염료 1.0 ~ 3.0 wt%,
양파외피추출물 0.5 ~ 2.0 wt% 및
소목추출물 0.5 ~ 2.0 wt%
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%를 포함하여 100.0 wt%를 구성하는 것을 특징으로 하는 반려동물용 피부 저자극성 천연 염모제.
With respect to the total weight of the hair dye,
1.0 to 3.0 wt% of natural dye,
Onion skin extract 0.5 ~ 2.0 wt% and
Beefwood extract 0.5 ~ 2.0 wt%
Vetiver (Vetiver) fragrance, chestnut flower fragrance or eucalyptus fragrance selected from 0.1 to 0.5 wt%, including 100.0 wt% of a companion animal skin hypoallergenic natural hair dye, characterized in that the composition.
하이드록시에틸셀룰로오스(Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%와,
카보머(Carbomer; 2% Solution) 10.0 ~ 15.0 wt%와,
천연염료 1.0 ~ 3.0 wt%와,
양파외피추출물 0.5 ~ 2.0 wt%와,
소목추출물 0.5 ~ 2.0 wt%와,
베티버(Vetiver) 향료, 밤꽃향료 또는 유칼립투스 향료 중 선택되는 향료 0.1 ~ 0.5 wt%와,
95% 에탄올(Ethanol, 95%) 13.0 ~ 20.0 wt%와,
벤질알코올(Benzyl Alcohol) 5.0 ~ 12.0 wt%와,
메틸피롤리돈(Methyl pyrrolidone) 5.0 ~ 10.0 wt%와,
글리콜산(Glycolic acid) 2.0 ~ 6.0 wt%를 포함하는 것을 특징으로 하는 반려동물용 피부 저자극성 천연 염모제.
40.0 to 55.0 wt% of water,
Hydroxyethylcellulose (Hydroxy ethylcellulos) 0.3 ~ 1.5 wt%,
Carbomer (2% Solution) 10.0 ~ 15.0 wt% and,
1.0 to 3.0 wt% of natural dyes,
0.5 to 2.0 wt% of onion skin extract,
0.5 ~ 2.0 wt% of bovine extract and,
0.1 to 0.5 wt% of a fragrance selected from among vetiver fragrance, chestnut fragrance or eucalyptus fragrance,
95% ethanol (Ethanol, 95%) 13.0 to 20.0 wt%,
5.0 to 12.0 wt% of Benzyl Alcohol,
5.0 ~ 10.0 wt% of methyl pyrrolidone,
Glycolic acid (Glycolic acid), characterized in that it contains 2.0 ~ 6.0 wt% of skin hypoallergenic natural hair dye for companion animals.
천연염료는 쪽, 대청, 인도람, 송람, 소송목, 유구염 또는 패자 중 선택되는 어느 1종 이상의 보라계 염료; 황련, 황백, 히드라스티스, 산딸기나무, 치자, 샤프란 또는 홍목 중 선택되는 어느 1종 이상의 황색계 염료; 봉선화, 닭의장풀, 두약 또는 산람 중 선택되는 어느 1종 이상의 홍색계 염료; 쑥의 녹색계염료 중 선택되는 단색성염료와,
억새, 코스모스, 떡갈나무, 금은화, 칡, 토끼풀; 감초, 황금, 박하; 철쭉, 화금, 녹차; 양파, 동백잎, 봉선화, 괴화, 무궁화, 굴껍질, 피마자, 머위, 측백나무, 달맞이꽃, 은행나무, 녹차, 접시꽃, 호두나무, 호장근; 메밀, 무화과, 부들, 수둑, 천일홍, 익모초, 목련, 괴화; 칡, 새삼, 호두나무, 봉선화, 접시꽃; 적채, 자색고구마, 포도과피, 오미자, 갓, 유색미, 나무딸기, 블랙베리, 버찌, 미국자리공, 광나무, 함초, 담쟁이덩굴; 오배자, 상수리나무, 오리나무, 오이풀, 대추나무, 밤, 커피, 미역취, 박하, 호두나무, 메밀; 석류, 감, 호두나무, 대황; 지초; 호두나무; 코치닐, 호장근, 꼭두서니, 락, 원추리, 대황, 케르메스; 중 선택되는 다색성 염료 중에서 선택되는 것임을 특징으로 하는 반려동물용 피부 저자극성 천연 염모제.
The method according to claim 1 or 2,
The natural dyes include any one or more purple dyes selected from indigo, daecheong, indoram, songram, somok, yugyeom, or loser; Any one or more yellow dyes selected from yellow lotus, yellow white, hydratis, raspberry, gardenia, saffron, or redwood; Any one or more crimson dyes selected from balsam, rooster grass, tofu or sanlam; A monochromatic dye selected among green dyes of mugwort,
Silver grass, cosmos, oak, gold and silver coins, arrowroot, shamrock; Licorice, golden, mint; Azaleas, hwageum, green tea; Onion, Camellia leaves, Balsam, Goehwa, Mugunghwa, Oyster bark, Castor, Butterbur, Japanese cypress, Evening primrose, Ginkgo biloba, Green tea, hollyhock, Walnut, Hojanggeun; Buckwheat, figs, cattails, suduk, cheonilhong, motherwort, magnolia, gohwa; Arrowroot, saesam, walnut, balsam, hollyhock; Red vegetables, purple sweet potatoes, grape skin, schisandra chinensis, mustard, colored rice, raspberries, blackberries, cherries, American sprigs, mineral trees, green tea, ivy; Obaeja, oak, alder, cucumber grass, jujube, chestnut, coffee, seaweed, mint, walnut, buckwheat; Pomegranate, persimmon, walnut, rhubarb; Branch; Walnut tree; Cochineal, Hojanggeun, Madder, Rock, Wonchuri, Rhubarb, Kermes; Hypoallergenic natural hair dye for companion animals, characterized in that it is selected from polychromatic dyes selected from among.
양파외피추출물은 양파껍질을 세척하고, 암소에서 건조한 후 건식분쇄기로 분쇄하여 분말을 제조하고,
상기 양파껍질 분말을 정제수와 동 중량비로 혼합하고,
100 ℃에서 100 ~ 150 분 동안 가열하여 액상 추출을 하고,
상기 액상 추출한 추출물을 글래스 필터(glass filter)로 필터링하고,
상기 필터링한 추출물을 회전감압농축기(Rotary evaporator)를 이용하여 63℃에서 15 시간 동안 감압농축하고,
상기 감압농축한 추출물을 동결건조기(Freeze dryer)로 건조하여 분말로 제조한 것을 특징으로 하는 반려동물용 피부 저자극성 천연 염모제.
The method according to claim 1 or 2
The onion skin extract is washed with onion skin, dried in the dark, and pulverized with a dry grinder to prepare a powder.
Mixing the onion skin powder with purified water at the same weight ratio,
Liquid extraction is performed by heating at 100° C. for 100 to 150 minutes,
Filtering the liquid extract extracted with a glass filter,
The filtered extract was concentrated under reduced pressure at 63° C. for 15 hours using a rotary evaporator,
The skin hypoallergenic natural hair dye for companion animals, characterized in that the extract concentrated under reduced pressure is dried with a freeze dryer to form a powder.
소목추출물은 분쇄한 소목 분말과 메탄올(Methanol)을 1 : 5 ~ 10 중량비로 혼합하고,
33 ~ 34 ℃에서 20시간씩 3회 진탕하여 추출하고,
추출물을 글래스 필터(glass filter)로 필터링하고,
상기 필터링한 추출물을 회전감압농축기(Rotary evaporator)를 이용하여 63℃에서 15 시간 동안 감압농축하고,
상기 감압농축한 추출물을 동결건조기(Freeze dryer)로 건조하여 분말로 제조한 것을 특징으로 하는 반려동물용 피부 저자극성 천연 염모제.
The method according to claim 1 or 2
Beefwood extract is mixed with pulverized joiner powder and methanol in a ratio of 1: 5 to 10 by weight,
Extract by shaking three times at 33 ~ 34 ℃ for 20 hours each,
Filtering the extract with a glass filter,
The filtered extract was concentrated under reduced pressure at 63° C. for 15 hours using a rotary evaporator,
The skin hypoallergenic natural hair dye for companion animals, characterized in that the extract concentrated under reduced pressure is dried with a freeze dryer to form a powder.
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