KR20080104699A - Method for manufacturing fabric with an antibacterial function - Google Patents
Method for manufacturing fabric with an antibacterial function Download PDFInfo
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- KR20080104699A KR20080104699A KR1020070051834A KR20070051834A KR20080104699A KR 20080104699 A KR20080104699 A KR 20080104699A KR 1020070051834 A KR1020070051834 A KR 1020070051834A KR 20070051834 A KR20070051834 A KR 20070051834A KR 20080104699 A KR20080104699 A KR 20080104699A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
- A01N25/28—Microcapsules or nanocapsules
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
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Abstract
Description
도 1은 본 발명의 일 실시예에 따른 모기해충 퇴치기능을 가지는 섬유의 제조방법을 나타내는 공정 순서도1 is a process flow chart showing a method for producing a fiber having a mosquito pest control function according to an embodiment of the present invention.
도 2는 본 발명의 일 실시예에 따른 모기해충 퇴치기능을 가지는 섬유의 제조방법에서 모기해충 퇴치물질을 마이크로캡슐화한 상태를 보여주는 개략도Figure 2 is a schematic diagram showing a state of microencapsulating the mosquito pest control material in the method for producing a fiber having a mosquito pest control function according to an embodiment of the present invention.
<도면의 주요부분에 대한 부호의 설명><Description of the symbols for the main parts of the drawings>
10 : 코어 물질 20 : 월 물질10: core material 20: month material
본 발명은 모기해충 퇴치기능을 가지는 섬유의 제조방법에 관한 것으로서, 더욱 상세하게는 인체에 해가 없고 모기해충 퇴치에 탁월한 효능이 있는 천연 식물 추출 원료를 마이크로캡슐 형태로 만들어 이를 섬유에 염착(染着)하는 방식으로 모기해충 퇴치기능을 가지는 기능성 섬유를 제조하는 방법에 관한 것이다. The present invention relates to a method for producing a fiber having a mosquito pest control function, and more particularly, to make a natural capsule extract raw material that is harmless to the human body and has excellent efficacy in combating mosquito pests in the form of microcapsules and dyes it to the fiber (染) The present invention relates to a method for producing a functional fiber having a function of combating mosquito pests in a manner of wearing.
일반적으로 항균 또는 방충기능을 발휘하는 제품으로는 분무제, 유연제, 패치제 등 다양하다.In general, the product exhibiting antibacterial or insect repellent functions, such as a spray, a softener, a patch.
그러나, 기존의 제품들은 단독적인 효과에 그치거나, 마이크로캡슐화 기술이 도입되지 않은 제품으로 지속적인 효과가 떨어진다.However, existing products are not only effective effects alone, but also have a continuous effect on products without microencapsulation technology.
특히, 가정에서 많이 이용되고 있는 섬유유연제의 경우는 단순히 유연효과와 소취효과에 중점을 두고 시판되어지고 있으며, 근래에 항균효과가 가미된 섬유유연제(공개특허 특2003-0050969) 또는 모기 등의 해충퇴치기능을 갖는 마이크로캡슐을 이용한 섬유유연제(공개특허 특2003-0095106) 등이 출원되었으나, 대부분 30일 내외로 지속적인 해충퇴치 효과를 발휘하는데에는 그 한계가 있다. In particular, the fabric softeners that are widely used in homes are marketed with a focus on softening and deodorizing effects, and recently, such as pesticides such as fibrous softeners (published patent application 2003-0050969) or mosquitoes with antibacterial effects. Fibrous softeners using a microcapsule having a function of combating (Patent Publication No. 2003-0095106) and the like have been filed, but most of them have a limit to exhibit a continuous pest control effect within about 30 days.
또한, 기존의 해충퇴기기능을 나타내는 성분들의 경우 인체에 유해한 화학 성분들을 포함하고 있는 관계로 인체에 착용시 피부 등에 알레르기를 일으킬 소지가 높고, 또 기존의 제품들의 경우 섬유유연제로 사용되어졌을 때, 세탁헹굼시 방대한 물 희석량으로 인하여 궁극적으로 제품이 나타내고자 하는 소기의 목적을 달성하기에는 너무나도 부족하며, 유연 처리 후 남은 다량의 폐액은 그대로 버려지고 있는 실정이다. In addition, since the components exhibiting pest repellent function contain chemical components that are harmful to the human body, they are highly likely to cause allergies when worn on the human body, and when the existing products are used as fabric softeners, Due to the vast amount of water dilution during washing and rinsing, ultimately the product is too short to achieve its intended purpose, and a large amount of waste liquid remaining after the flexible treatment is discarded as it is.
따라서, 본 발명은 이와 같은 점을 감안하여 안출한 것으로서, 모기해충 퇴치에 탁월한 효능이 있는 천연 식물 추출 원료를 제조하여 마이크로캡슐 형태로 만들어 이를 섬유에 직접 염착(染着)하는 방식을 구현함으로써, 장기간에 걸쳐 모기 해충 퇴치기능을 발휘할 수 있도록 한 모기해충 퇴치기능을 가지는 섬유의 제조방법을 제공하는데 그 목적이 있다. Therefore, the present invention has been made in view of such a point, by preparing a natural plant extract raw material having excellent efficacy in combating mosquito pests to form a microcapsule form and implements a method of dyeing directly to the fiber (染着), It is an object of the present invention to provide a method for producing a fiber having a mosquito pest control function that can exert a mosquito pest control function over a long period of time.
또한, 본 발명은 인체에 전혀 해가 없는 천연 식물 추출 원료를 사용함으로써, 양호한 인체 안정성을 도모할 수 있고, 또 환경 친화적으로 사용할 수 있는 해충퇴치기능을 가지는 섬유의 제조방법을 제공하는데 다른 목적이 있다. Another object of the present invention is to provide a method for producing a fiber having a pest control function which can achieve good human stability and can be used environmentally by using a natural plant extract raw material which is harmless to the human body. have.
상기 목적을 달성하기 위한 본 발명의 일 실시예에 따른 해충퇴치기능을 가지는 섬유의 제조방법은 수분함량이 0.5∼5중량%인 천연 식물의 추출물 0.5 ∼ 50 중량%와 식물성 유지 0.5 ∼ 50 중량%를 혼합한 다음, 10 ~ 30일간 숙성하여 오일상 혼합물을 형성하는 1 단계; 상기 오일상 혼합물의 수분함량을 0.5 ∼ 5 중량% 범위로 유지하여, 천연 식물의 추출물의 코어 주위를 식물성 유지가 감싸고 있는 셀 구조를 형성하는 마이크로캡슐을 형성하는 2 단계; 상기 마이크로캡슐과 프리덱스 또는 우레탄 바인더 또는 수지 바인더를 1:1 ∼ 1:3 비율로 혼합한 후, 섬유에 염착하는 3 단계; 를 포함하는 것을 특징으로 한다. Method for producing a fiber having a pest control function according to an embodiment of the present invention for achieving the above object 0.5 to 50% by weight of the extract of natural plants and 0.5 to 50% by weight of vegetable fats and oils Mixing, then aged 1 to 30 days to form an oil phase mixture; Maintaining the water content of the oil phase mixture in the range of 0.5 to 5% by weight to form microcapsules forming a cell structure in which vegetable oil is wrapped around the core of the extract of the natural plant; Mixing the microcapsules with a predex or urethane binder or a resin binder in a ratio of 1: 1 to 1: 3, and then dyeing the fibers; Characterized in that it comprises a.
또한, 상기 천연 식물은 허브, 아로마, 구몬초, 제라늄, 계피, 쑥, 향나무 및 토마토 중에서 선택된 1종 또는 2종 이상의 혼합물인 것을 특징으로 한다. In addition, the natural plant is characterized in that the mixture of one or two or more selected from herbs, aromas, Kumoncho, geranium, cinnamon, mugwort, juniper and tomatoes.
또한, 상기 바인더는 우레탄, 수지 및 프리텍스 중에서 선택된 것을 특징으로 한다.In addition, the binder is characterized in that selected from urethane, resin and pretex.
또한, 상기 섬유는 천연섬유 또는 합성섬유인 것을 특징으로 한다. In addition, the fiber is characterized in that the natural fiber or synthetic fiber.
또한, 상기 천연 섬유는 마이크로캡슐과 바인더 혼합물에 천연 섬유를 담궈놓은 다음, 건조하는 것을 특징으로 한다. In addition, the natural fiber is characterized in that the natural fiber is immersed in a mixture of microcapsules and binder, and then dried.
또한, 상기 합성 섬유는 60 ~ 80 ℃의 물에 카치온화제(인덱스)과 합성 섬유를 혼합하여 20분 정도 삶고 이를 탈수, 건조한 후 마이크로캡슐과 바인더 혼합물에 천연 섬유를 담궈놓은 다음, 건조하는 것을 특징으로 한다. In addition, the synthetic fiber is boiled for about 20 minutes by mixing a cationic agent (index) and synthetic fibers in water of 60 ~ 80 ℃, dehydrated, dried, soaking the natural fibers in a microcapsule and binder mixture, and then dried. It is done.
이하, 첨부한 도면을 참조하여 본 발명의 일 실시예에 따른 모기해충 퇴치기능을 가지는 섬유의 제조방법을 상세히 설명하면 다음과 같다. Hereinafter, with reference to the accompanying drawings will be described in detail a method for producing a fiber having a mosquito pest control function according to an embodiment of the present invention.
도 1은 본 발명의 일 실시예에 따른 모기해충 퇴치기능을 가지는 섬유의 제조방법을 나타내는 공정 순서도이고, 도 2는 본 발명의 일 실시예에 따른 모기해충 퇴치기능을 가지는 섬유의 제조방법에서 모기해충 퇴치물질을 마이크로캡슐화한 상태를 보여주는 개략도이다. 1 is a process flow chart showing a method of manufacturing a fiber having a mosquito pest control function according to an embodiment of the present invention, Figure 2 is a method of manufacturing a fiber having a mosquito pest control function according to an embodiment of the present invention. Schematic showing microencapsulation of pest control material.
도 1과 도 2에 도시한 바와 같이, 상기 모기해충 퇴치기능을 가지는 섬유를 제조하는 과정은 기본적으로 천연 식물로부터 추출한 액상의 물질을 마이크로캡슐화하고, 이를 섬유에 염착하는 과정으로 이루어져 있으며, 이에 따라 모기해충 퇴치기능의 천연 약제를 서서히 방출하는 마이크로캡슐의 특징을 통해 효과적으로 모기해충을 퇴치할 수 있는 실용적인 섬유 및 의류를 구현할 수 있다. As shown in Figure 1 and 2, the process of producing a fiber having a mosquito pest control function consists of the process of microencapsulating the liquid material extracted from the natural plant, and dyeing the fiber, thereby Therefore, through the features of the microcapsules that slowly release the natural medicine of mosquito pest control function can implement a practical fiber and clothing that can effectively combat mosquito pests.
본 발명에서 사용하는 모기해충 기피 천연 식물은 허브, 아로마, 구몬초, 제라늄, 계피, 쑥, 향나무, 토마토 등으로 식용 또는 약용으로 알려져 있으며, 그 특유의 향기로 모기 등의 해충을 쫓는 성질이 있다. Mosquito repellent natural plants used in the present invention is known as edible or medicinal as herbs, aromas, Kumoncho, geranium, cinnamon, mugwort, juniper, tomatoes, etc., has a characteristic of chasing pests such as mosquitoes with its unique scent. .
먼저, 1단계로서 위의 천연 식물로부터 액상 성분을 추출하고, 이렇게 추출한 액상 성분을 원심분리기나 증류기 등을 사용하여 수분의 70% 이상을 증발시킨 다음, 이것을 피마자유 등과 같은 식물성 유지와 1:1 ~ 1:3 의 비율로 혼합 희석하고, 계속해서 10 ~ 30일간 숙성시켜 오일 형태로 만드는 단계를 수행한다. First, liquid phase components are extracted from the above natural plants as a first step, and the extracted liquid components are evaporated at least 70% of water using a centrifugal separator or a distiller, and then mixed with vegetable oils such as castor oil and 1: 1. The mixture is diluted in a ratio of 1: 3, and then aged for 10 to 30 days to form an oil.
여기서, 액상 성분 추출시, 쑥이나 토마토 등과 같이 수분이 많은 식물인 경우에는 녹즙기를 사용하여 액상으로 추출하고, 계피나 향나무 등과 같이 마른 식물인 경우에는 액탕기에 물과 원재료 식물을 1:1 비율로 넣고 약 100℃ 정도의 온도에서 3시간 정도 삶아서 액상을 추출한다. Here, in the case of extracting the liquid component, in case of watery plants such as wormwood or tomatoes, extract the liquid using green juice, and in the case of dry plants such as cinnamon or juniper, water and raw material plants in a liquid bath in a 1: 1 ratio. Put it in a boiled for about 3 hours at a temperature of about 100 ℃ to extract the liquid.
이때, 상기 천연 식물은 한가지 성분을 단독으로 적용할 수 있고, 또는 두가지 이상을 혼합한 형태도 적용할 수 있다. At this time, the natural plant may be applied to one component alone, or a mixture of two or more may be applied.
다음, 2단계로서 혼합 및 숙성된 오일 형태의 모기해충 퇴치물질을 증류기 등으로 다시 수분을 완전히 제거하고, 수분이 제거된 모기해충 퇴치물질을 마이크로캡슐과 결합하는 단계를 수행한다. Next, as a second step, the mosquito pest control material in the oil form mixed and matured is completely removed again using a distillation machine, and the mosquito pest control material from which the water is removed is combined with the microcapsules.
예를 들면, 도 2에서 볼 수 있는 바와 같이 분말 형태의 모기해충 퇴치물질을 코어 물질(10)로 하고, 이러한 코어 물질(10)을 외부를 형성하는 고분자 물질로 이루어진 월 물질(20)로 둘러싸는 단계를 수행한다. For example, as shown in FIG. 2, the mosquito pest control material in powder form is used as the
이러한 마이크로캡슐의 경우 직경이 수 ~ 수십㎛ 크기를 갖는 초미세 입자 형태로 제조될 수 있다. Such microcapsules may be prepared in the form of ultrafine particles having a diameter of several tens of micrometers.
여기서, 내부의 모기해충 퇴치물질을 외부의 고분자 물질로 감싸는 마이크로캡슐화 방법은 당해 기술분야에서 통상적으로 알려져 있는 방법이라면 특별히 제한 되지 않고 채택될 수 있다. Here, the microencapsulation method of wrapping the internal mosquito pest control material with the external polymer material may be adopted without particular limitation as long as it is a method commonly known in the art.
다음, 3단계로서 위의 2단계에서 제조한 마이크로캡슐과 우레탄 바인더 또는 수지 바인더 또는 프리덱스 바인더를 1:1 ~ 1:3 비율로 희석한 후, 섬유에 염착하는 단계를 수행한다. Next, after diluting the microcapsules and urethane binders or resin binders or predex binders prepared in step 2 in a ratio of 1: 1 to 1: 3 as three steps, dyeing the fibers is performed.
이때, 섬유 염착 방법으로는 천연 섬유 염착 방법과 합성 섬유 염착 방법을 선택적으로 적용할 수 있다. In this case, as the fiber dyeing method, a natural fiber dyeing method and a synthetic fiber dyeing method may be selectively applied.
상기 천연 섬유에 염착하는 방법의 경우 마이크로캡슐과 우레탄 바인더 또는 수지 바인더를 1:1로 희석한 후, 이것을 물 100ℓ 대비 5 ~ 50으로 희석한 다음, 그 속에 천연 섬유를 5 ~ 10 분간 담궈 놓고, 적당한 시간이 경과한 후에 천연 섬유를 꺼내어 탈수, 건조하면 마이크로캡슐 형태의 해충퇴치물질이 포함되어 있는 천연 섬유를 얻을 수 있다. In the case of dyeing the natural fibers in a 1: 1 dilution of the microcapsules and urethane binder or resin binder, and then dilute this to 5 to 50 to 100 liters of water, and then immersed the natural fibers in 5 to 10 minutes After the proper time has elapsed, the natural fiber is taken out, dehydrated and dried to obtain a natural fiber containing a microcapsule-type pest control material.
또한, 상기 합성 섬유에 염착하는 방법의 경우 준비과정으로 합성 섬유를 카치온화제(인덱스)를 첨가한 온도 60 ~ 80℃의 물에 약 20분간 삼는 과정을 먼저 수행한다. In addition, in the case of dyeing the synthetic fibers in the preparation process is first performed for about 20 minutes to prepare the synthetic fibers in water at a temperature of 60 ~ 80 ℃ the addition of a cationic agent (index).
계속해서 삶은 합성 섬유를 탈수, 건조한 후, 이것을 1:1로 희석한 마이크로캡슐과 우레탄 바인더 또는 수지 바인더를 물 100ℓ 대비 5 ~ 50으로 희석한 용액 속에 넣고 5 ~ 10 분간 담궈놓은 다음 탈수, 건조하면 마이크로캡슐 형태의 모기해충 퇴치물질이 포함되어 있는 합성 섬유를 얻을 수 있다. After dehydrating and drying the boiled synthetic fibers continuously, put the microcapsules and urethane binder or resin binder diluted 1: 1 in a solution diluted 5 to 50 with respect to 100 l of water, soak for 5 to 10 minutes, and then dehydrate and dry. Synthetic fibers containing microcapsule-type mosquito pest control materials can be obtained.
이와 같이, 천연 식물로부터 해충퇴치성분을 추출하고 이것을 마이크로캡슐화하여 섬유에 염착하여 사용함으로써, 의류에 적용하는 경우 오랜 기간이 경과되 어도 마이크로캡슐의 물질 방출 속도 제어특성에 의해 모기해충 퇴치기능을 계속적으로 유지할 수 있는 등 실용성을 높일 수 있고, 또 인체에 전혀 해가 없는 천연 식물 추출물이기 때문에 누구나 안심하고 사용할 수 있다. In this way, by extracting the pest control ingredients from natural plants, and microencapsulated it to be used for dyeing the fiber, even if a long time when applied to the clothing to control the mosquito pest control function by controlling the release rate of the microcapsules Anyone can use it with peace of mind because it is a natural plant extract that can improve its practicality and can harm it.
이상에서 설명한 바와 같이 본 발명은 천연 식물에서 추출한 원료를 마이크로캡슐화하여 섬유에 염착하는 새로운 형태의 모기해충 퇴치기능을 가지는 섬유 제조방법을 제공함으로써, 모기해충 탈취기능을 장기간 지속적으로 발휘할 수 있는 장점이 있으며, 특히 인체에 무해한 천연 식물로부터 추출한 성분을 사용하기 때문에 우수한 인체 안정성을 도모할 수 있고, 또 친환경적으로 사용할 수 있는 효과가 있다. As described above, the present invention provides a fiber manufacturing method having a new type of mosquito pest control function that micro-encapsulates the raw material extracted from natural plants and dyes the fiber, and thus, the mosquito pest deodorizing function can be continuously exerted for a long time. There is, in particular, because it uses components extracted from natural plants harmless to the human body can achieve excellent human stability, and there is an effect that can be used environmentally friendly.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010117191A2 (en) * | 2009-04-06 | 2010-10-14 | Yuhan-Kimberly, Limited | Absorbent article comprising an encapsulated plant extract exhibiting an insecticidal effect |
| KR101271877B1 (en) * | 2011-11-09 | 2013-06-05 | (주)한성헬스피아 | Fabrics coated by chamaecyparis obtusa extract and manufacturing method thereof |
| KR101353374B1 (en) * | 2011-03-15 | 2014-01-27 | 박수언 | anti-bacterial the fibers process |
| KR20170024774A (en) * | 2015-08-26 | 2017-03-08 | (주)엔바이오 | Fabric treatment composition having functing of tick prevention |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH06346373A (en) * | 1993-06-07 | 1994-12-20 | Daiwa Kagaku Kogyo Kk | Method for processing synthetic fiber with blood-sucking insect pest-repelling agent |
| JPH11290427A (en) | 1998-04-11 | 1999-10-26 | Eco Nakajima:Kk | Sanitary sheet |
| JP2000166399A (en) | 1998-12-11 | 2000-06-20 | Unitika Ltd | Agricultural and horticultural insecticidal mesh sheet |
| JP2001032172A (en) | 1999-07-12 | 2001-02-06 | Seiichi Sano | Mugwort-containing fiber sheet |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010117191A2 (en) * | 2009-04-06 | 2010-10-14 | Yuhan-Kimberly, Limited | Absorbent article comprising an encapsulated plant extract exhibiting an insecticidal effect |
| WO2010117191A3 (en) * | 2009-04-06 | 2011-03-31 | Yuhan-Kimberly, Limited | Absorbent article comprising an encapsulated plant extract exhibiting an insecticidal effect |
| KR101105574B1 (en) * | 2009-04-06 | 2012-01-17 | 유한킴벌리 주식회사 | Absorbent articles comprising an encapsulated plant extract showing insecticidal effect |
| KR101353374B1 (en) * | 2011-03-15 | 2014-01-27 | 박수언 | anti-bacterial the fibers process |
| KR101271877B1 (en) * | 2011-11-09 | 2013-06-05 | (주)한성헬스피아 | Fabrics coated by chamaecyparis obtusa extract and manufacturing method thereof |
| KR20170024774A (en) * | 2015-08-26 | 2017-03-08 | (주)엔바이오 | Fabric treatment composition having functing of tick prevention |
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