KR102475897B1 - Mask cosmetic composition comprising Graviola antibiotic extract and method of preparing the same - Google Patents

Abstract

The present invention provides a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola having skin intensive care, skin lifting, pore convergence effect, and oil-moisture balance control effect, and a method for manufacturing the same, thereby providing antioxidant, antibacterial activity, and skin barrier activity. , It has excellent whitening effect and anti-inflammatory activity, so it is effective in mask manufacturing to improve skin wrinkles such as skin improvement, skin soothing and skin moisturizing.

Description

Cosmetic composition containing Graviola antibiotic extract and method for preparing the same {Mask cosmetic composition comprising Graviola antibiotic extract and method of preparing the same}

The present invention relates to a mask cosmetic composition containing Graviola extract as an active ingredient, and more particularly, skin intensive skin care, skin lifting, pore convergence effect, and skin wrinkle improvement containing Graviola antibacterial extract having an effect of controlling oil and moisture balance It relates to a mask cosmetic composition for use and a manufacturing method thereof.

As human skin ages, the secretion of various hormones that internally regulate metabolism decreases, and the function of immune cells and the activity of cells decrease, resulting in a decrease in the biosynthesis of immune proteins and biocomponent proteins necessary for the body. Intrinsic aging or chronologic aging caused externally by various contaminants and ultraviolet rays causes the skin to become thinner and its elasticity to decrease, and as it is exposed to ultraviolet rays, keratinocytes and keratinocytes in the epidermis Melanocytes are damaged by UVB (Ultra Violet B) and are affected by extrinsic aging or photo aging.

In particular, in modern society, due to hormonal abnormalities caused by excessive stress and sudden changes in the external environment, the vitality of the skin deteriorates more quickly due to the influence of air pollutants that exceed the skin's defense mechanism or stronger ultraviolet rays.

In chronological aging, characteristic clinical skin findings include fine wrinkles, atrophy of the dermis, and a decrease in the subcutaneous fat layer, while in the photoaging process, rough and deep wrinkles appear and abnormal elastotic materials accumulate, making the skin look like leather. thick and loose

In the cells constituting the skin, cell activity decreases due to endogenous aging or photoaging, and the signal transduction system becomes incomplete, increasing the biosynthesis of MMPs (matrix metalloproteinases), which are enzymes that decompose skin tissue, and reducing the biosynthesis of collagen, resulting in wrinkles. It is known that this occurs, elasticity decreases, and melanin production, which causes skin darkening, increases. Therefore, substances that can thicken the skin by proliferating skin cells or increasing the matrix substances constituting the skin, substances that can inhibit the biosynthesis of MMPs that degrade collagen, the matrix substances constituting the skin, and inhibition of melanin biosynthesis Substances that can do this have been found to alleviate skin symptoms such as wrinkles, loss of elasticity, and darkening of the skin.

On the other hand, mask-type packs in which non-woven fabric, cloth, or paper are cut into the shape of a face and only the eyes or mouth are incised are emerging one after another to provide cosmetic effects such as whitening, wrinkle removal, freckle removal, oil removal, and skin softening. Because of this, it is widely used.

A cosmetic mask is a thin mask molded to fit each part of the human face, and there are a face-type mask attached to the entire face and a form applied to a part of the face. When such a cosmetic mask is attached to the human facial skin Active ingredients of essence or nutrients can be forcibly permeated into the skin to obtain various cosmetic effects.

Recently, according to the environment-friendly and nature-oriented trend, active ingredients used in cosmetics are not only chemical substances but also plant-derived natural products based on their usefulness, and natural ingredients with fewer side effects on the skin are mixed in cosmetics in various forms. Accordingly, it is environmentally friendly and natural-oriented, so there are few side effects, and all of the key elements of skin health, such as antibacterial, antioxidant and anti-inflammatory effects, are excellent, so it is required to develop mask cosmetics made of natural materials that can enhance skin vitality. have.

KR 10-2015-0118078 A (2015.10.21.) KR 10-2015-0082813 A (2015.07.16.) KR 10-2015-0065560 A (2015.06.15.) KR 10-1458013 B1 (2014.10.29.) KR 10-0840440 B1 (2008.06.16.) KR 10-0444625 B1 (2004.08.06.)

Accordingly, the inventors of the present invention have made constant efforts to develop a mask cosmetic composition for improving skin wrinkles made of novel natural materials. As a result of research in the field of medicine, Graviola extract containing phytochemical and acetogenin, which are anti-cancer and antioxidant substances, has a skin soothing effect, skin barrier strengthening, whitening and anti-inflammatory effect. Aging effect, antibacterial activity, and skin cell proliferation improvement effect were confirmed, and an effective combination method of graviola extract, plant extract with skin stabilizing effect, and various peptides was identified so that these effects could be maximized. The present invention was completed by confirming the excellent skin vitality enhancing effect of cosmetics that can be used for improving masks.

Accordingly, an object of the present invention is to provide a mask cosmetic composition for improving skin wrinkles comprising a graviola extract as an active ingredient.

In addition, another object of the present invention is to provide a method for producing a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola.

In addition, another object of the present invention is to provide a mask comprising a mask cosmetic composition for improving skin wrinkles containing the graviola extract as an active ingredient.

In order to achieve the above object, the present invention is a graviola extract, portulaca extract, centella asiatica extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, eucalyptus leaf extract, mung bean extract, green tea extract, situation mushroom extract It provides a mask cosmetic composition for improving skin wrinkles comprising a graviola extract as an active ingredient.

In this case, the composition according to the present invention contains 1 to 10% by weight of the graviola extract and the portulaca extract, centella extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, and eucalyptus with respect to 100% by weight. It is characterized by including 0.1 to 5% by weight of leaf extract, mung bean extract, green tea extract, and Phellinus linteus extract, respectively.

In order to achieve the above-described other object, the present invention provides a method for producing a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola.

In order to achieve the above object, the present invention provides a mask comprising a mask cosmetic composition for improving skin wrinkles containing the graviola antibacterial extract.

As described above, the present invention provides a mask cosmetic composition for improving skin wrinkles containing an antibacterial Graviola extract as an active ingredient and a manufacturing method thereof. The composition of the present invention has excellent antioxidant, antibacterial activity, skin barrier activity, whitening effect and anti-inflammatory activity, so it is effective in preparing a mask for improving skin wrinkles such as skin improvement, skin soothing and skin moisturizing.

1 is a view showing a manufacturing process of a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola according to the present invention;
Figure 2 is an adenosine content test report of a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola according to the present invention.

Hereinafter, detailed descriptions of preferred embodiments of the present invention will be described with reference to the accompanying drawings. Specific details have been shown in the following description, which are provided only to help a more general understanding of the present invention, and are not intended to limit the present invention to specific embodiments, and all changes included in the spirit and technical scope of the present invention, It should be understood to include equivalents or alternatives. In the description of the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be omitted.

Unless defined otherwise, all terms used herein, including technical or scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. Terms such as those defined in commonly used dictionaries should be interpreted as having a meaning consistent with the meaning in the context of the related art, and unless explicitly defined in the present application, they should not be interpreted in an ideal or excessively formal meaning. don't

"Skin wrinkle improvement" used in the detailed description of the present invention means any action or effect that inhibits, delays, or improves skin damage or wrinkles, or improves the health condition of the skin.

The term “extract” refers to an active ingredient isolated from a natural product, that is, a material exhibiting a desired activity. The extract may be obtained through an extraction process using water, an organic solvent, or a mixed solvent thereof, and may include a dry powder thereof or any form formulated using the same. In addition, the extract includes fractionated extracts subjected to the extraction process.

1 is a view showing a method for manufacturing a mask cosmetic composition for improving skin wrinkles containing an antibacterial extract of Graviola according to the present invention, as shown in FIG. A mask cosmetic composition and a manufacturing method thereof are provided.

The graviola extract, which accounts for the largest portion of the mask cosmetic composition for skin wrinkle improvement containing the graviola antibacterial extract according to the present invention, is Portuguese for Soursop (Soursop), which is an anticancer and antioxidant phytochemicals ) and acetogenin. The Graviola extract used in the present invention uses an extract obtained from the fruit of Sueoshop. The graviola extract obtained from the fruit of Sueo Shop is effective in soothing stressed or problematic skin and provides a refreshing feeling without stickiness after use.

The mask cosmetic composition of the present invention is an herbal plant extract, which is another active ingredient, portulaca extract, centella asiatica extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, eucalyptus leaf extract, mung bean extract, green tea extract, Contains Phellinus Linteus extract.

The portulaca extract, centella asiatica extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, eucalyptus leaf extract, mung bean extract, green tea extract, and Phellinus linteus extract constituting the herbal plant extract used in the present invention are used for aromatherapy. It has a refreshing phytoncide fragrance to provide effects, and is intended to comfortably soothe skin irritated by stress.

The herbal plant extract is preferably extracted using a solvent selected from water, lower alcohol having 1 to 4 carbon atoms, or a mixed solvent thereof, and more preferably ethanol or a mixture of ethanol and water. The suitable amount of the extraction solvent is not particularly limited, and is 1 to 10 times the weight of portulaca, centella, witch hazel, bamboo, chamomile flowers and leaves, rice bran, eucalyptus leaves, mung bean, green tea, and Sanghwang mushroom constituting oriental plants, More preferably, it is 5-8 times. However, the method of extracting the herbal plant extract, which is an active ingredient of the present invention, is not particularly limited.

As shown in Figure 1, the manufacturing method of the mask cosmetic composition for improving skin wrinkles containing the graviola antibacterial extract according to the present invention, 3-5 weight emulsifiers as the first mixture 10 with respect to 100% by weight of the final composition % and flavoring agent 0.1-0.5% by weight are added in order, completely dissolved (11), filtered, and then transferred to a mixer (13). Here, polysorbate 80 may be used as the emulsifier.

The second mixture 20 includes 35-60% by weight of purified water used as a solvent, 1-5% by weight of triethanolamine, 1-5% by weight of butylene glycol, 1-5% by weight of propylene glycol, 1-5% by weight of glycerin % by weight, 3-10% by weight of hyaluronic acid, 1-5% by weight of snail mucus filtrate, 0.01-0.1% by weight of adenosine, 0.5-2% by weight of olive oil, 1-5% by weight of hydrolyzed collagen, 1-5 wt% surfactant, 1-5 wt% 1,2-hexanediol, 1-5 wt% emulsifier, 0.1-5 wt% green tea extract, 0.1-5 wt% portulaca extract, 1-10 soushop fruit extract % by weight, bamboo extract 0.1-5% by weight, rice bran extract 0.1-5% by weight, centella asiatica extract 0.1-5% by weight, Phellinus linteus extract 0.1-5% by weight, witch hazel extract 0.1-5% by weight, chamomile flower/leaf extract 0.1-5% by weight, eucalyptus leaf extract 0.1-5% by weight, mung bean extract 0.1-5% by weight, allantoin 0.05-0.5% by weight, disodium EDTA 0.05-0.5% by weight, carbomer 0.05-0.5% by weight, octa 0.05-0.5% by weight of the peptide is sequentially added, dissolved and dispersed (21), passed through a filter (23), and transferred to an emulsifying machine.

Here, PEG-60 hydrogenated castor oil may be used as the surfactant, and triethanolamine and caprylic/capric triglyceride may be used as the emulsifier. On the other hand, glycerin is used as a skin moisturizer, olive oil is used as a moisture evaporation blocker, and 1,2-hexanediol is used as a preservative. In addition, disodium EDIT is used as a sequestering agent, carbomer is used as a thickener, and octapeptide is used as a skin protectant.

The first and second mixtures 10 and 20 transferred to the emulsifier are well mixed until completely fused (30). When mixing, the rotation speed of the homo mixer is 1500-2500 rpm and the rotation speed of the paddle mixer is 20-50 rpm.

Subsequently, the homo mixer is stopped and the paddle mixer starts defoaming by applying a vacuum while maintaining the rotation speed (31). The number of times of vacuum and defoaming can be performed 3-10 times.

The composition after vacuum and defoaming is placed in a storage tank, aged for 10 to 30 hours (33), and then transferred to and stored in a filling room (35).

Fundamental factors of skin trouble, such as hormonal imbalance, bacteria in hair follicles, factors related to various stresses due to lifestyle and irregular eating habits, sensitivity of sebaceous glands, occurrence of secondary harmful bacteria due to hygiene conditions, inflammatory reactions, and oxidative stress When this increases, their actions act more complexly, resulting in allergic reactions, poor blood circulation, and cell metabolism and growth inhibition. And these causes eventually cause skin troubles such as itching and inflammation.

Inflammatory response, one of the above secondary factors, is caused by stimulation of harmful bacteria, and regardless of this, it is also chronically caused by metabolic syndrome caused by a westernized lifestyle characterized by high calories and lack of exercise, and mental stress or It can also be caused temporarily by shock. The inflammatory reaction accelerates tissue degeneration, suppresses cell growth, and overly sensitizes the immune system, further stimulating allergic phenomena, thereby damaging the health of skin tissue.

The above factors (harmful bacteria, inflammation, and oxidative stress) cause skin trouble by complexly and synergistically acting together to cause a vicious cycle that continues and worsens. Therefore, the composition of the present invention, which provides excellent effects on all of the above complex factors, improves the skin by sterilization, soothes the skin, and moisturizes the skin, as well as increases the synthesis of collagen, which is destroyed due to cell function decline, It promotes blood circulation and provides very excellent effects in preventing aging.

In addition, the conventional antibacterial agent should minimize the time it stays on the skin due to toxicity and irritation, and there is a problem of causing resistance. There is no problem even if formed, and it has a characteristic that resistance does not occur.

This point is well shown in the examples for evaluating the effectiveness of the mask cosmetic composition for improving skin wrinkles containing the antibacterial extract of Graviola according to the present invention.

Efficacy evaluation according to an embodiment of the present invention is a test for the content of adenosine, in which the effect of improving skin wrinkles is confirmed. As shown in Figure 2, the mask cosmetic composition for improving skin wrinkles containing the antibacterial extract of Graviola shows a test result of 102.20%, far exceeding the test standard of 90%.

As described above, since the mask cosmetic composition for improving skin wrinkles containing the antibacterial extract of Graviola according to the present invention contains more than the standard adenosine having a skin wrinkle improvement effect, skin intensive care effect, lifting effect, pore convergence effect, and It can be effectively used in the manufacture of masks with oil-moisture balance control effects.

In addition, for the mask cosmetic composition containing the graviola extract used in the present invention, antibacterial activity test, skin antibacterial peptide expression increase confirmation test, skin barrier resilience test, whitening effect confirmation test, anti-inflammatory effect confirmation test and antioxidant effect confirmation test conducted.

Example 1: Antibacterial activity test

The control group was a product using ordinary purified water, and was carried out using Propionibacterium acnes to measure the sterilization effect. The test method was carried out according to the Halo test, in which a specimen was placed on a nutrient medium coated with acne bacteria and observed how much restraint band was generated around the specimen.

Treat 30 mg of the sample on a sterilized paper disc, place it in the center of the plate medium inoculated with the bacterial solution, and then incubate for 72 hours in anaerobic conditions using an anaerobic jar at (35 ± 1) Inhibition zone formed The diameter of was measured. As a result of measuring the antibacterial activity of the sample under this test condition, an 11 mm low zone was formed against the P. acnes bacteria used in the test.

In order to find out the antibacterial effect on the sample (essence), a halo test was conducted to measure the size of the inhibition zone. As a result, the sample formed an inhibition zone of 11 mm against P. acnes.

As described above, the mask cosmetic composition for improving skin wrinkles containing the antibacterial extract of Graviola according to the present invention has excellent antibacterial activity and can be effectively used for manufacturing a mask having an intensive skin care effect as well as improving skin wrinkles.

Example 2: Test for confirming the increase in the expression of antibacterial peptides in the skin

Graviola extract was treated with human keratinocytes (keratinocytes) to confirm the expression of antimicrobial peptides (CAMP; Cathelicidin AntiMicrobial Peptide, LL-37) expressed in skin cells themselves.

Example 3: Skin barrier resilience test

Graviola extract's ability to enhance cell proliferation was confirmed in keratinocytes and fibroblasts.

Example 4: Whitening effect confirmation test

The effect of inhibiting melanin production in melanosomes of melanocytes was confirmed.

Example 5: Anti-inflammatory effect confirmation test

In order to confirm the possibility of developing products for skin inflammatory diseases such as atopy and psoriasis, the effect of inhibiting mast cell degranulation and the production of inflammatory cytokines TNF-a and IL-8 of keratinocytes was confirmed.

Example 6: Antioxidant effect confirmation test

The free radical scavenging activity of the graviola extract was measured or the effect of increasing superoxide dismutase (SOD) activity in keratinocytes and fibroblasts was confirmed.

The mask cosmetic composition of the present invention can be prepared in any formulation conventionally prepared in the art, and in addition to the oriental herbal plant extract of the present invention, it contains a dermatologically acceptable medium or base that is commonly used in the field of dermatology. It can be prepared in the form of an adjuvant that can be applied or applied systemically.

In addition, the mask cosmetic composition of the present invention is a moisture evaporation blocker, binder, emulsification stabilizer, skin moisturizer, surfactant, preservative, skin protectant and metal ion sequestering agent in addition to the graviola extract and herbal plant extract. Ordinarily used in cosmetics It may contain adjuvants commonly used in the field of cosmetology or dermatology, such as any other ingredient known as In addition, the above components may be introduced in an amount generally used in the field of dermatology. Meanwhile, the cosmetic composition of the present invention does not use parabens, which are cosmetic preservatives, at all.

In the mask using the cosmetic composition according to the present invention, the mask cosmetic composition for improving skin wrinkles may include a graviola extract in an amount of 1 to 10% by weight based on 100% by weight of the total product, and herbal plant extracts in an amount of 0.1 to 10% by weight, respectively It is preferably included in an amount of 5% by weight.

The mask of the present invention may further contain at least one active ingredient exhibiting the same or similar function in addition to the mask cosmetic composition for improving skin wrinkles.

On the other hand, as described above, the present invention, as described above, a method for manufacturing a mask cosmetic composition for improving skin wrinkles containing a graviola extract as an active ingredient, which includes dissolving the first and second mixtures separately, mixing them step by step, and cooling them to provide.

As described above, the cosmetic composition of the present invention has excellent skin intensive care effects such as antibacterial activity, sterilization effect, skin barrier recovery ability, whitening effect, anti-inflammatory effect and antioxidant effect, as well as skin lifting effect, pore convergence effect, and oil-moisture balance control effect. Confirmed.

Meanwhile, in the detailed description of the present invention, specific embodiments have been described, but various modifications are possible without departing from the scope of the present invention. Therefore, the scope of the present invention should not be limited to the described embodiments and should not be defined, but should be defined by not only the scope of the claims to be described later, but also those equivalent to the scope of these claims.

As described above, the present invention provides a mask cosmetic composition for improving skin wrinkles containing a graviola extract as an active ingredient and a manufacturing method thereof, and the composition of the present invention has antibacterial activity, sterilization effect, skin barrier recovery ability, whitening effect, anti-inflammatory It has excellent skin intensive care effects such as skin effect and antioxidant effect, as well as skin lifting effect, pore convergence effect, and oil-moisture balance control effect.

Claims (6)

A mask containing graviola extract, including graviola extract, portulaca extract, centella asiatica extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, eucalyptus leaf extract, mung bean extract, green tea extract, and Phellinus linteus extract. cosmetic composition.
According to claim 1,
Based on 100% by weight of the composition, 1 to 10% by weight of the Graviola extract and the portulaca extract, centella extract, witch hazel extract, bamboo extract, chamomile flower and leaf extract, rice bran extract, eucalyptus leaf extract, mung bean extract, green tea extract , A mask cosmetic composition comprising 0.1 to 5% by weight of Phellinus linteus extract, respectively.
A mask comprising the mask cosmetic composition of claim 1.
A first step in which 3-5% by weight of an emulsifier and 0.1-0.5% by weight of a flavoring agent are sequentially added to 100% by weight of the final composition, completely dissolved and dispersed, and the filtered first mixture is transferred to a mixer;
35-60% by weight of purified water, 1-5% by weight of triethanolamine, 1-5% by weight of butylene glycol, 1-5% by weight of propylene glycol, 1-5% by weight of glycerin, 3-10% by weight of hyaluronic acid % by weight, snail secretion filtrate 1-5%, adenosine 0.01-0.1% by weight, olive oil 0.5-2% by weight, hydrolyzed collagen 1-5% by weight, surfactant 1-5% by weight, 1,2 -Hexanediol 1-5% by weight, emulsifier 1-5% by weight, green tea extract 0.1-5% by weight, portulaca extract 0.1-5% by weight, sooshop fruit extract 1-10% by weight, bamboo extract 0.1-5% by weight, Rice bran extract 0.1-5% by weight, Centella asiatica extract 0.1-5% by weight, Sanghwang mushroom extract 0.1-5% by weight, Witch hazel extract 0.1-5% by weight, Chamomile flower/leaf extract 0.1-5% by weight, Eucalyptus leaf extract 0.1-5% by weight 5 wt%, mung bean extract 0.1-5 wt%, allantoin 0.05-0.5 wt%, disodium EDTA 0.05-0.5 wt%, carbomer 0.05-0.5 wt%, and octapeptide 0.05-0.5 wt% were added in order. A second step of transferring the second mixture, which was then dissolved and dispersed and filtered, to the emulsifier;
A third step of mixing the first and second mixing agents transferred to the emulsifier;
a fourth step of vacuuming and defoaming the mixture mixed in the third step; and
The fifth step of storing the composition after vacuum and defoaming in the fourth step in a storage tank, aging it for 10-30 hours, and then transferring and storing it in a filling room; Manufacturing a mask cosmetic composition containing an antibacterial extract of Graviola, characterized in that it consists of Way.
The method of claim 4, wherein the third step,
A method for producing a mask cosmetic composition containing an antibacterial extract of Graviola, characterized in that the rotation speed of the homo mixer is mixed at 1500-2500 rpm and the rotation speed of the paddle mixer is 20-50 rpm.
The method of claim 5, wherein the fourth step,
The homo mixer is stopped, and the paddle mixer is a method for producing a mask cosmetic composition containing a graviola antibacterial extract, characterized in that performing vacuum and defoaming 3-10 times while maintaining the number of revolutions.

Images