KR102149452B1 - thermal grease and manufacturing method thereof - Google Patents

Abstract

This invention allows thermal grease to contain nano-sized aroma oil capsules to provide thermal grease users with the pharmacological efficacy of aroma oils, and to thermal grease to contain transition metal elements to irradiate far-infrared rays using transition metal elements. It promotes the user's biological activity by allowing it to be released, and 10 to 50% by weight of carrier oil, 5 to 40% by weight of dispersant, and thermoelectric as a filler to remove microorganisms that occur during long-term storage by adding bamboo vinegar liquid to thermal grease. Conductive particles, beryllium oxide (BeO) 5-20% by weight, additives 5-10% by weight, nano-sized aroma oil capsules 3-5% by weight, transition metal elements 4-8% by weight, bamboo vinegar solution 5-8% by weight The present invention relates to a thermal grease and a manufacturing method thereof.

Description

Thermal grease and manufacturing method thereof TECHNICAL FIELD

This invention allows the thermal grease to contain nano-sized aroma oil capsules to provide the pharmacological effect of the aroma oil to the computer device user, and the transition metal element to the thermal grease contains the transition metal element to emit far-infrared rays. The present invention relates to a thermal grease that promotes the user's biological activity by allowing it to be activated and removes harmful microorganisms that occur during long-term storage by adding bamboo vinegar to thermal grease, and a method of manufacturing the same.

The computer's central processing unit (CPU) is generating more heat per unit area as the size of the computer's central processing unit (CPU) is improving, while its size is getting smaller.

As the heat generated by the central processing unit (CPU) degrades the performance of the central processing unit (CPU) or causes errors, thermal grease is applied to the package surface of the central processing unit (CPU). ) To effectively dissipate the heat from the outside.

For reference, as an example of technology related to thermal grease, a technology related to a composition that has high shape retention characteristics, low viscosity, and can be stored at a normal temperature is disclosed in Korean Patent Laid-Open Publication No. 10-2017-0043459 (published date). It has been disclosed in "Additional one-component curing type thermally conductive silicone grease composition" of (April 21, 2017).

However, conventional thermal greases, including Publication No. 10-2017-0043459, have been verified for safety against electricity and fire, but have not been verified as to whether or not chemical components are harmful to the human body, so they can prevent nervous system disorders through skin contact or respiratory inhalation. Total Volatile Organic Compounds (TVOC), which is a carcinogen, may be generated, which may threaten user health.

Publication number 10-2017-0043459

An object of the present invention is to solve the conventional problems as described above, a thermal grease and a thermal grease that can provide a pharmacological effect of the aroma oil to a computer device user by including a nano-sized aromatic oil capsule in the thermal grease. It is to provide a manufacturing method.

Another object of the present invention is to provide a thermal grease and a method for producing the same, which promotes the biological activity of a user by allowing a transition metal element to be contained in a thermal grease to emit far infrared rays using the transition metal element.

Another object of the present invention is to provide a thermal grease and a method for manufacturing the same, capable of removing harmful microorganisms generated during long-term storage by adding bamboo vinegar liquid to thermal grease.

As a means for achieving the above object, in the thermal grease, the thermal grease includes 10 to 50% by weight of a carrier oil, 5 to 40% by weight of a dispersant, and beryllium oxide (BeO) 5 which is a thermally conductive particle as a filler. It characterized in that it comprises ~20% by weight, 5 to 10% by weight of additives, 3 to 5% by weight of nano-sized aroma oil capsules, 4 to 8% by weight of transition metal elements, and 5 to 8% by weight of bamboo vinegar liquid.
In the present invention, the aroma oil capsule, as an organic solvent, dichloromethane (Dichloromethane, CH ₂ Cl ₂ ), a biodegradable polymer compound polycarboxyl lactose as a material for forming a wall material, and a core substance, aroma Oil is sequentially added to a homogenizer, polyvinyl alcohol as a dispersant for dispersing an aroma oil, and then stirred and mixed, and the mixing ratio of the constituents is dichloromethane. ) Based on 100 parts by weight, 3 to 6 parts by weight of polycarboxyl lactose, 3 to 6 parts by weight of aromatic oil, and 1.5 to 3 parts by weight of polyvinyl alcohol.
The size of the aroma oil capsule is formed in the 4 ~ 12㎛.
The transition metal element composition, based on the entire transition metal composition, V ₂ O ₅ is 0.5 ~ 2.5% by weight, Cr ₂ O ₃ is 0.5 ~ 2.5% by weight, MnO is 2 ~ 4% by weight, Co ₂ O ₃ is 2 to 4 wt%, NiSO ₄ 1 to 3 wt%, CuO 1 to 3 wt%, ZnO 2 to 4 wt%, GeO 2 to 4 wt%, Se powder 2.5 to 4.5 wt%, K ₂ O is 0.5 to 2.5 wt%, TiO ₂ is 2 to 4 wt%, As ₂ O ₃ is 0.5 to 2.5 wt%, Y ₂ O ₅ is 0.5 to 2.5 wt%, ZrO ₂ is 3.5 to 5.5 wt%, MoO ₃ Is 0.5 to 2.5 wt%, Ag powder is 0.5 to 2.5 wt%, Cd is 0.5 to 2.5 wt%, SnO ₂ 2 to 4 wt%, Sb ₂ O is 2 to 4 wt%, BaO is 0.5 to 2.5 wt%, WO ₃ is 0.5 to 2.5 wt%, PbO is 0.5 to 1 wt%, Bi ₂ O ₃ is 0.5 to 2.5 wt%, pozzolan is 12 to 17 wt%, tourmaline is 12 to 17 wt%, PE 4207 is 9 to 13 The weight percent and OD 6280 comprise 9 to 13 weight percent.
The transition metal element composition, based on the entire transition metal composition, ZnS is 3.5 to 5.5% by weight, LiO ₂ 2 to 4% by weight, B powder is 2 to 4% by weight, C powder is 2 to 4% by weight, NaCl Silver 5 to 7 wt%, MgO 2 to 4 wt%, SiO ₂ 6.5 to 8.5 wt%, P ₂ O ₅ 3.5 to 5.5 wt%, Tourmaline 6.5 to 8.5 wt%, Illite 16 to 20 wt% , PE 4207 is composed of 9 to 13% by weight and OD 6280, including 9 to 13% by weight.
The transition metal element composition is based on the entire transition metal composition, MnO ₂ is 4 to 6% by weight, CoO is 4 to 6% by weight, SiC is 7.5 to 9.5% by weight, GeO is 3 to 5% by weight, ZnO is 1.5 to 3.5 wt%, NiO 1.5 to 3.5 wt%, P ₂ O ₅ 1.5 to 3.5 wt%, TiO ₂ 1.5 to 3.5 wt%, Ag powder 1.5 to 3.5 wt%, SnO ₂ 1.5 to 3.5 wt% %, Sb ₂ O is 1.5 to 3.5% by weight, pozzolan is 10 to 15% by weight, tourmaline is 10 to 15% by weight, PE 4207 is 8 to 12% by weight, and OD 6280 is made of 8 to 12% by weight.
In another embodiment of the present invention, in a method for producing a thermal grease, forming a mixture by blending 10 to 50% by weight of a carrier oil and 5 to 40% by weight of a dispersant, and thermoelectricity in the mixture of the carrier oil and the dispersant Mixing and stirring 5 to 20% by weight of beryllium oxide (BeO) and 5 to 10% by weight of additives, as well as additionally mixing and stirring 3 to 5% by weight of nano-sized aromatic oil capsules, and transition It characterized in that it comprises the step of further mixing and stirring 4 to 8% by weight of metal elements, further mixing and stirring the bamboo vinegar solution 5 to 8% by weight, and the step of filling the mixed mixture into a container. do.
In the present invention, the method of manufacturing the nano-sized aroma oil capsule. Dichloromethane (CH ₂ Cl ₂ ) as an organic solvent, polycarboxyl lactose, a biodegradable polymer compound as a material for forming a wall material, and aroma oil as a core material, are sequentially added to a homogenizer. In order to form a mixed solution by adding polyvinyl alcohol as a dispersant for dispersing the aroma oil and forming the mixed solution, and to nanosizing the size of the aroma oil capsule, 25±5 The step of stirring and mixing for 3 to 5 hours at a stirring speed of 5,000 to 8,000 rpm under a temperature condition of ℃, and after the mixed solution is formed, dichloro, an organic solvent, for 2 to 3 hours at a temperature range of 40 to 60 ℃ under reduced pressure environment. Evaporating methane (Dichloromethane) to form a wall material by coating the polycarboxyl lactose layer on an aroma oil to solidify it, and washing 2-3 times with distilled water after removing dichloromethane, It comprises the step of obtaining a bead-shaped aroma oil capsule having a nano-sized size after filtering with a filter or removing the filtrate by precipitation for a predetermined time.

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In the present invention, the thermal grease contains nano-sized aroma oil capsules to provide the pharmacological effect of the aroma oil to the computer device user, and the transition metal element is included in the thermal grease to irradiate far-infrared rays using the transition metal element. By allowing it to be released, the user's biological activity is promoted, and by adding bamboo vinegar liquid to thermal grease, it has the effect of removing microorganisms generated during long-term storage.

1 is an external perspective view of a thermal grease device filled with thermal grease of the present invention.

Hereinafter, in order to describe in detail enough that a person of ordinary skill in the art can easily implement the present invention, a preferred embodiment of the present invention will be described in detail with reference to the accompanying drawings. Other objects, features, and operational advantages, including the object, operation, and effect of the present invention, will become more apparent by the description of the preferred embodiment.

For reference, the embodiments disclosed herein have been presented by selecting the most preferable embodiments to aid understanding of those skilled in the art among various possible examples, and the technical idea of the present invention is necessarily limited or limited only by the presented embodiments. Rather, various changes, additions, and changes including equivalents or substitutes are possible within the scope of the technical idea of the present invention.

In addition, the expressions of terms or words used in the specification and claims of the present application are defined on the basis of the principle that the inventor can appropriately define the concept of terms in order to explain his or her invention in the best way. , It should not be interpreted as being limited to a conventional or dictionary meaning, and should be interpreted as a meaning and concept consistent with the technical idea of the present invention. As an example, the expression in the singular includes a plurality of expressions unless clearly defined otherwise in the context, and the expression about the direction is set based on the position expressed on the drawing for convenience of description, and is "connected" or "connected" The expression "become" includes not only direct connection or connection, but also connection or connection through other elements in the middle.

1 is an external perspective view of a thermal grease device filled with thermal grease according to the present invention.

As shown in Fig. 1, the thermal grease device is filled with thermal grease, a nozzle part 11 is formed at the front end, and a pair of semicircular ring handles 12 protruding from the outer peripheral surface of the rear end. The body (1) and the front end from the rear of the body (1) to extrude the grease inside the body (1) is inserted into the body (1) while maintaining a sealed state to enter the A piston (2) having a circular ring handle (21) formed at the rear end, and a cap (3) for sealing the nozzle part (11) to prevent the grease inside the body (1) from leaking out before use It is made including.

When the user inserts the middle finger and the index finger to the pair of semicircular ring handles 12 and puts the thumb on the circular ring handle 21, and then pushes the thumb while pulling the middle and index fingers , As the front end of the piston 2 enters the interior of the body 1, the thermal grease inside the body 1 is extruded so that the thermal grease is ejected through the nozzle 11, thereby enhancing the convenience of use.

The thermal grease of this invention is filled in the interior of the body (1) described above, and is 10 to 50% by weight of a carrier oil, 5 to 40% by weight of a dispersant, and 5 to 20% by weight of beryllium oxide (BeO), which is a thermally conductive particle as a filler. %, 5 to 10% by weight of additives, 3 to 5% by weight of nano-sized aroma oil capsules, 4 to 8% by weight of transition metal elements, and 5 to 8% by weight of bamboo vinegar liquid.

The method for producing a thermal grease according to the present invention comprises the steps of forming a mixture by blending 10 to 50% by weight of a carrier oil and 5 to 40% by weight of a dispersant, and beryllium oxide as thermally conductive particles in the mixture of the carrier oil and the dispersant. (BeO) mixing and stirring 5 to 20% by weight and 5 to 10% by weight of additives, additionally mixing and stirring 3 to 5% by weight of nano-sized aromatic oil capsules, and 4 to 8 of transition metal elements It comprises a step of stirring by further mixing and stirring the weight%, further mixing and stirring the bamboo vinegar solution 5-8% by weight, and the step of filling the mixed mixture into a container.

The nano-sized aroma oil capsules that are additionally mixed as described above are prepared as follows.

Dichloromethane (CH ₂ Cl ₂ ) as an organic solvent, polycarboxyl lactose, a biodegradable polymer compound as a material for forming a wall material, and aroma oil as a core material, are sequentially added to a homogenizer. Then, polyvinyl alcohol is added as a dispersant for dispersing the aromatic oil, and then sufficiently stirred and mixed to form a mixed solution. The homogenizer is a type of grinder used to grind samples and is also called a homogenizer.

The mixing ratio of the above components is based on 100 parts by weight of dichloromethane, 3 to 6 parts by weight of polycarboxyl lactose, 3 to 6 parts by weight of aromatic oil, and 1.5 to 3 parts by weight of polyvinyl alcohol. Mix parts by weight.

If the amount of dichloromethane is less than 85 parts by weight, the aroma oil and polycarboxyl lactose are not well mixed, and if it exceeds 170 parts by weight, the outer wall material of the aroma oil There is a problem that formation becomes difficult.

If the amount of the polycarboxyl lactose is less than 3 parts by weight, the thickness of the outer wall material of the aroma oil is thin and easily breaks. If it exceeds 6 parts by weight, the thickness of the outer wall material of the aroma oil is too thick. There is a problem that it is formed thick so that the release of the aromatic oil becomes difficult.

When the mixing amount of the aromatic oil is less than 3 parts by weight, there is a problem that the thickness of the wall material of the aroma oil capsule becomes too thick, and when it exceeds 6 parts by weight, the thickness of the wall material of the aroma oil capsule is formed too thin. have.

If the amount of the polyvinyl alcohol is less than 1.5 parts by weight, the stability of the mixed solution is low, so that uniform mixing is not performed, so that the capsule formation is difficult. If the amount exceeds 3 parts by weight, There is a problem in that it is difficult to form capsules because the mixing is too good.

In order to nanosize the size of the aroma oil capsule while forming the above-described mixed solution, the mixture is sufficiently stirred and mixed for 3 to 5 hours at a stirring speed of 5,000 to 8,000 rpm under a temperature condition of 25±5°C.

If it is out of the threshold of the above temperature condition, the wall material is not formed outside the aromatic oil.

When the agitation speed is less than 5,000 rpm, the mixing of the components is difficult, resulting in a phenomenon that polycarboxyl lactose clumps, and when the stirring speed exceeds 8,000 rpm, it is formed outside the aroma oil. There is a problem that the wall material is broken,

When the agitation time is less than 3 hours, the coating of polycarboxyl lactose is not sufficiently performed, so that the formation of the wall material is difficult, and when the stirring time exceeds 5 hours, the wall material is formed. There is a problem that the wall material is cracked because it is coated too thinly.

After the mixed solution is formed, dichloromethane, an organic solvent, is evaporated for 2 to 3 hours in a temperature range of 40 to 60°C in a reduced pressure environment, so that the polycarboxyl lactose layer is coated on the aromatic oil to solidify. After the wall material is formed, the filtrate is removed by filtration with a filter or precipitation for a certain period of time, and then a bead-shaped aroma oil capsule having a nano-sized size is obtained.

Dichloromethane evaporation of the above-described mixed solution is carried out by installing a vacuum pump and a pressure measuring device on a homogenizer, raising the temperature of the homogenizer to a range of 40 to 60°C, and gradually reducing the pressure with a vacuum pump. Evaporation takes place. At this time, the evaporated dichloromethane is discharged to the outside by a vacuum pump, and dichloromethane discharged to the outside is obtained separately by a conventional method. More preferably, it is preferable to transfer the mixed solution to an Erlenmeyer flask having a certain capacity and to which a connection pipe is connected to a pressure gauge and a vacuum pump, seal it, and heat it to a temperature of 40 to 60°C to evaporate it.

Since dichloromethane may remain in the aroma oil capsule obtained after the wall material formation is completed through the above evaporation process, preferably, a washing process of washing 2 to 3 times with distilled water after removing dichloromethane is further performed. It is recommended to completely remove dichloromethane.

It is preferable that the size of the aroma oil capsule is formed to be 4 ~ 12㎛. When the size of the aroma oil capsule is less than 4 μm, the capsule is easily damaged and it is difficult to maintain the capsule state, and when the size of the aroma oil capsule exceeds 12 μm, it is difficult to release the aroma oil.

It is preferable that the thickness of the wall material of the aroma oil capsule is formed to 1.8 ~ 3.2㎛. When the thickness of the wall material of the aroma oil capsule is 1.8 μm, there is a problem that the wall material is easily broken, and when it exceeds 3.2 μm, it is difficult to release the aroma oil.

The effects revealed for the above aromatic oils are as follows.

-It promotes blood circulation and makes metabolism active.

-It relieves tension by releasing atrophy and tight muscles.

-It regulates endocrine disorders (hormone distribution).

-It promotes blood circulation, removes waste products from the walls of blood vessels, and activates intestinal function.

-It helps prevent colds and other diseases by cultivating physical resistance.

-Helps recover from fatigue and improves physical condition.

-It properly restores muscle relaxation and atrophy and removes waste products.

Meanwhile, the transition metal element to be further mixed is prepared as follows.

First, V ₂ O ₅ , Cr ₂ O ₃ , MnO, Co ₂ O ₃ , NiSO ₄ , CuO, ZnO, GeO and Se are prepared by mixing water with powder. Here, additionally K ₂ O, TiO ₂ , As ₂ O ₃ , Y ₂ O ₅ , ZrO ₂ , MoO ₃ , Ag powder, Cd, SnO ₂ , Sb ₂ O, BaO, WO ₃ , PbO, Bi ₂ O ₃ , Pozzolan, tourmaline, PE 4207, or OD 6280.

Unlike the general far-infrared emission member, the transition metal element composition thus prepared not only contains a wide variety of elements, but also V, Cr, Mn, Co, Ni, Cu, Zn, Ti, Zr, Mo, Ag, Cd, W By including various kinds of transition metal elements, such as, it can cope with most of the elements contained in the human body, can penetrate deep into the human body, and emit far-infrared rays in the wavelength range corresponding to the human body wave, thereby enhancing the therapeutic effect of the human body. Can be maximized.

More specifically, the transition metal element composition is, based on the entire transition metal composition, V ₂ O ₅ is 0.5 to 2.5% by weight, Cr ₂ O ₃ is 0.5 to 2.5% by weight, MnO is 2 to 4% by weight, Co ₂ O ₃ is 2 to 4 wt%, NiSO ₄ is 1 to 3 wt%, CuO is 1 to 3 wt%, ZnO is 2 to 4 wt%, GeO is 2 to 4 wt%, Se powder is 2.5 to 4.5 wt% %, K ₂ O 0.5 to 2.5 wt%, TiO ₂ 2 to 4 wt%, As ₂ O ₃ 0.5 to 2.5 wt%, Y ₂ O ₅ 0.5 to 2.5 wt%, ZrO ₂ 3.5 to 5.5 wt% %, MoO ₃ is 0.5 ~ 2.5% by weight, Ag powder is 0.5 ~ 2.5% by weight, Cd is 0.5 ~ 2.5% by weight, SnO ₂ 2 ~ 4% by weight, Sb ₂ O is 2 ~ 4% by weight, BaO is 0.5 ~ 2.5% by weight, WO ₃ is 0.5 ~ 2.5% by weight, PbO is 0.5 ~ 1% by weight, Bi ₂ O ₃ is 0.5 ~ 2.5% by weight, pozzolan is 12 ~ 17% by weight, tourmaline is 12 ~ 17% by weight, PE 4207 Silver may be 9 to 13% by weight and OD 6280 may be 9 to 13% by weight. Within this range, it is possible to emit far-infrared rays in a wavelength range of about 2 to 50 μm closest to the human body wave, and thus, a resonance phenomenon with a human cell material may be increased.

In addition, the transition metal element composition described above can be prepared by mixing water with ZnS. In addition, LiO ₂ , B powder, C powder, NaCl, MgO, SiO ₂ , P ₂ O ₅ , tourmaline, illite, PE 4207, or OD 6280 may include one or more.

More specifically, the above-described transition metal element composition, based on the entire transition metal composition, ZnS is 3.5 to 5.5% by weight, LiO ₂ 2 to 4% by weight, B powder is 2 to 4% by weight, C powder is 2 to 4 Wt%, NaCl 5-7 wt%, MgO 2-4 wt%, SiO ₂ 6.5 ~ 8.5 wt%, P ₂ O ₅ 3.5 ~ 5.5 wt%, Tourmaline 6.5 ~ 8.5 wt%, Illite 16 ~ 20% by weight, PE 4207 may be 9 to 13% by weight, and OD 6280 may be 9 to 13% by weight. Within this range, it is possible to emit far-infrared rays in a wavelength range of about 2 to 50 μm closest to the human body wave, and thus, a resonance phenomenon with a human cell material may be increased.

In addition, the transition metal element composition may be prepared by mixing water with MnO ₂ , CoO, SiC, GeO, ZnO and NiO. In addition to this, it may include one or more of P ₂ O ₅ , TiO ₂ , Ag powder, SnO ₂ , Sb ₂ O, pozzolan, tourmaline, PE 4207 or OD 6280.

More specifically, the transition metal element composition described above is based on the total transition metal composition, MnO ₂ is 4 to 6% by weight, CoO is 4 to 6% by weight, SiC is 7.5 to 9.5% by weight, GeO is 3 to 5% by weight %, ZnO is 1.5 to 3.5% by weight, NiO is 1.5 to 3.5% by weight, P ₂ O ₅ is 1.5 to 3.5% by weight, TiO ₂ is 1.5 to 3.5% by weight, Ag powder is 1.5 to 3.5% by weight, SnO ₂ is 1.5 to 3.5 wt%, Sb ₂ O 1.5 to 3.5 wt%, pozzolan 10 to 15 wt%, tourmaline 10 to 15 wt%, PE 4207 8 to 12 wt% and OD 6280 8 to 12 wt% I can. Within this range, it is possible to emit far-infrared rays in a wavelength range of about 2 to 50 μm closest to the human body wave, and thus, a resonance phenomenon with a human cell material may be increased.

On the other hand, the bamboo vinegar liquid contained in the thermal grease according to an embodiment of the present invention is acidic with a pH of 3 to 4, and the aged bamboo vinegar liquid obtained by standing for at least 3 months or a distilled bamboo vinegar liquid obtained by distilling the thick bamboo vinegar liquid after standing for a short period of time is used. . The above-described bamboo vinegar solution is known to have strong sterilization and antibacterial power, so it can kill microorganisms present in thermal grease and maintain a clean state for a long time.

In order to check whether the bamboo vinegar solution used as the natural additive exhibits an antibacterial effect, an antimicrobial test for thermal grease was performed using E. coli, and the results are shown in Table 1 below.

Blank Bamboo vinegar Remark Initial E. coli concentration (CFU/mL) 1.2 × 10 ⁴ 1.2 × 10 ⁴ E. coli concentration after 4 hours (CFU/mL) 3.0 × 10 ⁴ <10 Bacterial reduction rate (%) - 99.9

As can be seen in Table 1, it can be confirmed that the bamboo vinegar solution exhibits an antibacterial effect in the thermal grease.

1: body 2: piston
3: cap

Claims (8)

In thermal grease,
The thermal grease is 10 to 50% by weight of a carrier oil, 5 to 40% by weight of a dispersant, 5 to 20% by weight of beryllium oxide (BeO), which is a thermally conductive particle as a filler, 5 to 10% by weight of an additive, and a nano-sized aromatic oil capsule A thermal grease comprising 3 to 5% by weight, 4 to 8% by weight of transition metal elements, and 5 to 8% by weight of bamboo vinegar. The method of claim 1,
The aroma oil capsule is a homogenizer of dichloromethane (CH ₂ Cl ₂ ) as an organic solvent, polycarboxyl lactose, a biodegradable polymer compound as a material for forming a wall material, and aroma oil as a core material. (Homogenizer) is sequentially added, polyvinyl alcohol as a dispersant for dispersing aroma oil, and then stirred and mixed, and the mixing ratio of the components is 100 parts by weight of dichloromethane. On the other hand, a thermal grease comprising 3 to 6 parts by weight of polycarboxyl lactose, 3 to 6 parts by weight of aromatic oil, and 1.5 to 3 parts by weight of polyvinyl alcohol. The method of claim 1,
Thermal grease, characterized in that the size of the aroma oil capsule is formed in a 4 ~ 12㎛. The method of claim 1,
The transition metal element composition, based on the entire transition metal composition, V ₂ O ₅ is 0.5 ~ 2.5% by weight, Cr ₂ O ₃ is 0.5 ~ 2.5% by weight, MnO is 2 ~ 4% by weight, Co ₂ O ₃ is 2 to 4 wt%, NiSO ₄ 1 to 3 wt%, CuO 1 to 3 wt%, ZnO 2 to 4 wt%, GeO 2 to 4 wt%, Se powder 2.5 to 4.5 wt%, K ₂ O is 0.5 to 2.5 wt%, TiO ₂ is 2 to 4 wt%, As ₂ O ₃ is 0.5 to 2.5 wt%, Y ₂ O ₅ is 0.5 to 2.5 wt%, ZrO ₂ is 3.5 to 5.5 wt%, MoO ₃ Is 0.5 to 2.5 wt%, Ag powder is 0.5 to 2.5 wt%, Cd is 0.5 to 2.5 wt%, SnO ₂ 2 to 4 wt%, Sb ₂ O is 2 to 4 wt%, BaO is 0.5 to 2.5 wt%, WO ₃ is 0.5 to 2.5 wt%, PbO is 0.5 to 1 wt%, Bi ₂ O ₃ is 0.5 to 2.5 wt%, pozzolan is 12 to 17 wt%, tourmaline is 12 to 17 wt%, PE 4207 is 9 to 13 Thermal grease, characterized in that comprising 9 to 13% by weight and OD 6280. The method of claim 1,
The transition metal element composition, based on the entire transition metal composition, ZnS is 3.5 to 5.5% by weight, LiO ₂ 2 to 4% by weight, B powder is 2 to 4% by weight, C powder is 2 to 4% by weight, NaCl Silver 5 to 7 wt%, MgO 2 to 4 wt%, SiO ₂ 6.5 to 8.5 wt%, P ₂ O ₅ 3.5 to 5.5 wt%, Tourmaline 6.5 to 8.5 wt%, Illite 16 to 20 wt% , PE 4207 is 9 to 13% by weight and OD 6280 is a thermal grease comprising 9 to 13% by weight. The method of claim 1,
The transition metal element composition is based on the entire transition metal composition, MnO ₂ is 4 to 6% by weight, CoO is 4 to 6% by weight, SiC is 7.5 to 9.5% by weight, GeO is 3 to 5% by weight, ZnO is 1.5 to 3.5 wt%, NiO 1.5 to 3.5 wt%, P ₂ O ₅ 1.5 to 3.5 wt%, TiO ₂ 1.5 to 3.5 wt%, Ag powder 1.5 to 3.5 wt%, SnO ₂ 1.5 to 3.5 wt% %, Sb ₂ O is 1.5 to 3.5% by weight, pozzolan is 10 to 15% by weight, tourmaline is 10 to 15% by weight, PE 4207 is 8 to 12% by weight, and OD 6280 is composed of 8 to 12% by weight. Thermal grease characterized by. In the manufacturing method of thermal grease,
Blending 10 to 50% by weight of a carrier oil and 5 to 40% by weight of a dispersant to form a mixture,
Mixing and stirring 5 to 20% by weight of beryllium oxide (BeO) and 5 to 10% by weight of an additive in the mixture of the carrier oil and the dispersant;
Further mixing and stirring 3 to 5% by weight of nano-sized aroma oil capsules,
Further mixing and stirring 4 to 8% by weight of a transition metal element, and
Further mixing and stirring the bamboo vinegar solution 5-8% by weight,
A method for producing a thermal grease comprising the step of filling a container with the mixture having been mixed. The method of claim 7,
The nano-sized aroma oil capsule manufacturing method.
Dichloromethane (CH ₂ Cl ₂ ) as an organic solvent, polycarboxyl lactose, a biodegradable polymer compound as a material for forming a wall material, and aroma oil as a core material, are sequentially added to a homogenizer. And forming a mixed solution by adding polyvinyl alcohol as a dispersant for dispersing the aroma oil;
In order to nanosize the size of the aroma oil capsule while forming the mixed solution, stirring and mixing for 3 to 5 hours at a stirring speed of 5,000 to 8,000 rpm under a temperature condition of 25 ± 5 °C, and
After the mixed solution is formed, dichloromethane, an organic solvent, is evaporated for 2 to 3 hours in a temperature range of 40 to 60°C in a reduced pressure environment, so that the polycarboxyl lactose layer is coated on the aromatic oil to solidify. To form a wall material, and
Washing 2-3 times with distilled water after removing dichloromethane, and
A method for producing a thermal grease comprising the step of obtaining a bead-shaped aroma oil capsule having a nano-sized size after filtering with a filter or by sedimenting for a predetermined time to remove the filtrate.

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