JPWO2014200031A1 - Cleaning device and cleaning method for stirring member - Google Patents

Abstract

Provided is a cleaning device capable of enhancing the cleaning effect of a stirring member. In the stirring bar cleaning device (42), the stirring bar (36) after stirring the sample is inserted into the cleaning container main body (44), and stirring is performed from the small-diameter hole (78) serving as a detergent liquid discharge port provided on the side. By discharging the detergent liquid (86) onto the bar (36), the deposits adhering to the surface of the stirring bar (36) can be washed off with the detergent liquid (86). Thereafter, the cleaning liquid (72) is discharged from one end of the cleaning liquid lateral flow path (60) as the cleaning liquid discharge port of the cleaning liquid discharge head (48), and the detergent liquid (86) adhering to the surface of the stirring rod (36) can be washed away. it can. In this stirring bar cleaning device (42), it is possible to wash off the deposits attached to the surface of the stirring bar (36) and the detergent liquid in the cleaning container body, and a high cleaning effect can be obtained.

Description

  The present invention relates to a cleaning device that is provided in an analyzer and can clean a stirring member used when a reagent is mixed with a sample, and a cleaning method for the stirring member.

There is known an analyzer that performs analysis after adding a reagent to a container containing a specimen (sample) containing a biological sample and the like, and mixing the specimen and the reagent.
In this type of analyzer, when a sample and a reagent are mixed, a stirring rod is inserted into the container to stir the sample and the reagent, but the stirring rod (stirring member) to which the previous sample is attached When the next sample is stirred, the previous sample is mixed into the next sample (so-called contamination). Therefore, it is necessary to stir the next sample after washing the stirring rod.

JP 2000-266663 A. JP 2008-224245A.

In Patent Literature 1, the stirring member is washed with pure water and then washed with pure water to suppress the influence of the previous sample on the analysis result of the next sample.
However, the specimen cannot be sufficiently washed away simply by washing the stirring member with concentrated raw water and pure water.
In addition, when the raw water concentrated water is discharged from the discharge port, the raw water concentrated water containing impurities may adhere to the stirring member on the upper part of the discharge port. If the discharge port is at the same height, the raw water concentrated water adhering to the upper part of the stirring member may not be sufficiently washed away with pure water.
In Patent Document 2, as shown in FIGS. 7 and 8, after the detergent liquid is jetted and supplied from the detergent supply unit 85, cleaning water is jetted and supplied from the water supply unit 87 to wash the dispensing nozzle 301. Have been described. However, since the detergent supply part 85 and the water supply part 87 are provided at the same height, the detergent liquid adhering to the part above the detergent supply part 85 of the dispensing nozzle 301 can be sufficiently washed away with the cleaning liquid. There are cases where it is not possible.

  In consideration of the above-described facts, an object of the present invention is to provide a cleaning device and a method for cleaning a stirring member that can enhance the cleaning effect of the stirring member.

  The cleaning apparatus according to the first aspect of the present invention includes a cleaning container into which a stirring member for stirring the sample to be analyzed is inserted, and a detergent solution is discharged to the stirring member inserted into the cleaning container to A detergent liquid discharge port for washing off deposits adhering to the surface of the stirring member, and a detergent liquid discharge port disposed above the detergent liquid discharge port, and discharging the cleaning liquid to the stirring member to wash away the detergent liquid adhering to the surface of the stirring member And a cleaning liquid discharge port.

In the cleaning apparatus according to the first aspect, the stirring member after stirring the sample can be inserted into the cleaning container.
By discharging the detergent liquid from the detergent liquid discharge port, it is possible to wash away the deposits attached to the surface of the stirring member inserted into the cleaning container with the detergent liquid.
After washing off the adhering matter adhering to the surface of the stirring member with the detergent solution, the cleaning solution is discharged from the cleaning solution discharge port disposed above the detergent solution discharge port, and the detergent solution adhering to the surface of the stirring member Can be washed off.
As described above, in the cleaning device according to the first aspect, since the adhering matter adhering to the surface of the stirring member is washed away using the detergent liquid, a high cleaning effect can be obtained.
In addition, an even higher cleaning effect can be obtained by rotating the stirring member in the cleaning container.
Furthermore, in the cleaning apparatus according to the first aspect, since the cleaning liquid discharge port is disposed above the detergent liquid discharge port, the detergent liquid adhering to the surface above the detergent liquid discharge port of the stirring member is also the cleaning liquid. It can be washed off reliably.

  According to a second aspect of the present invention, in the cleaning device according to the first aspect, the detergent liquid discharge means for discharging the detergent liquid fed by the detergent liquid pump from the detergent liquid discharge port via the detergent liquid supply path; And a cleaning liquid discharge means for discharging the cleaning liquid fed by the cleaning liquid pump from the cleaning liquid discharge port via a cleaning liquid supply path different from the detergent liquid supply path.

  In the cleaning apparatus according to the second aspect, the detergent liquid discharging means for discharging the detergent liquid sent by the detergent liquid pump from the detergent liquid discharge port via the detergent liquid supply path, and the cleaning liquid sent by the cleaning liquid pump are used as the detergent liquid. The cleaning liquid discharge means for discharging from the cleaning liquid discharge port through a cleaning liquid supply path different from the supply path is provided, so that the detergent liquid and the cleaning liquid are not mixed, and the detergent liquid discharge means Only the cleaning liquid can be discharged from the cleaning liquid discharge port. Thereby, the stirring member can be efficiently cleaned with the minimum necessary detergent liquid and cleaning liquid.

  According to a third aspect of the present invention, in the cleaning device according to the first aspect or the second aspect, the detergent liquid discharge port is provided on a side wall of the cleaning container, and the cleaning container includes the detergent. A wall body that repels the detergent liquid discharged from the liquid discharge port toward the stirring member is disposed.

In the cleaning device according to the third aspect, since the detergent liquid discharge port is provided on the side wall of the cleaning container, the detergent liquid can be discharged in the lateral direction.
In the cleaning container, there is a wall body that repels the detergent liquid discharged from the detergent liquid discharge port toward the stirring member, so that the detergent liquid discharged from the detergent liquid discharge port is directly applied to the stirring member. At the same time, the wall can repel the detergent liquid toward the stirring member.
As a result, the detergent liquid discharged from the detergent liquid discharge port and directly applied thereto and the detergent liquid repelled by the wall body are hung on the stirring member. The amount of detergent solution to be applied can be increased.

  According to a fourth aspect of the present invention, in the cleaning device according to any one of the first to third aspects, the cleaning container includes a cylindrical body, and an upper opening of the cylindrical body The part is provided with a horizontal flow path for flowing the cleaning liquid in the horizontal direction, and the end of the horizontal flow path is a cleaning liquid discharge port for the cleaning liquid.

  In the cleaning device according to the fourth aspect, the cleaning container includes a cylindrical body, and the cleaning liquid flows in the horizontal direction in the horizontal flow path, and flows in the horizontal flow path provided in the upper opening of the cylindrical body. The detergent liquid that has flowed down from the end (cleaning liquid discharge port) and adhered to the stirring member is washed away.

  According to a fifth aspect of the present invention, in the cleaning device according to any one of the first to fourth aspects, the detergent liquid discharge port diffuses the detergent liquid toward the stirring member. Has a mouth.

  In the cleaning apparatus according to the fifth aspect, the detergent liquid can be ejected from the diffusion port provided in the detergent liquid discharge port toward the stirring member so as to be diffused. Thereby, a detergent liquid can be sprayed over a wide range with respect to a stirring member.

  According to a sixth aspect of the present invention, there is provided a cleaning method for a stirring member, wherein a stirring member for stirring a sample to be analyzed is inserted into a cleaning container, and a detergent liquid fed to the stirring member by a detergent liquid pump is used. A first step of washing out deposits discharged from the detergent liquid discharge port and adhering to the surface of the stirring member; and after the first step, the cleaning liquid fed to the stirring member by a cleaning liquid pump is used as the detergent liquid. And a second step of washing away the detergent solution discharged from the cleaning solution discharge port disposed above the discharge port and adhering to the surface of the stirring member.

In the stirring member cleaning method according to the sixth aspect, first, in the first step, a stirring member for stirring the sample to be analyzed is inserted into the cleaning container, and the stirring member is fed with a detergent liquid pump. The discharged detergent solution is discharged from the detergent solution discharge port, and the adhering matter adhering to the surface of the stirring member is washed away.
In the second step, after the cleaning of the stirring member with the detergent liquid is finished, the cleaning liquid fed by the cleaning liquid pump to the stirring member is discharged from the cleaning liquid discharge port disposed above the detergent liquid discharge port and stirred. Wash off the detergent solution adhering to the surface of the member.
Thus, in the washing | cleaning method of the stirring member which concerns on a 6th aspect, the deposit | attachment and detergent solution which adhered to the surface of the stirring member within a washing | cleaning container can be washed off, and a high cleaning effect can be acquired.
Further, since the cleaning liquid is discharged from the cleaning liquid discharge port disposed above the detergent liquid discharge port, the detergent liquid adhering to the upper surface of the stirring member relative to the detergent liquid discharge port can be surely washed off with the cleaning liquid.

  According to a seventh aspect of the present invention, in the cleaning method for a stirring member according to the sixth aspect, in the first step, the stirring member is rotated and the detergent member is fed with a detergent liquid pump while rotating the stirring member. The detergent liquid is discharged from the detergent liquid discharge port to wash away the adhering matter adhering to the surface of the stirring member. In the second step, the stirring member is rotated and the liquid is fed to the stirring member with a cleaning liquid pump. The washed liquid is discharged from a cleaning liquid discharge port disposed above the detergent liquid discharge port, and the detergent liquid adhering to the surface of the stirring member is washed away.

  In the cleaning method of the stirring member according to the seventh aspect, in the first step, the stirring member is discharged from the detergent liquid outlet through the detergent liquid fed by the detergent liquid pump to the stirring member while rotating the stirring member. In the second step, after the washing of the stirring member with the detergent liquid is finished, the washing liquid fed by the washing liquid pump to the stirring member while rotating the stirring member is washed in the second step. The detergent liquid discharged from the cleaning liquid discharge port disposed above the liquid discharge port and adhered to the surface of the stirring member is washed away.

Thus, in the cleaning method of the stirring member according to the seventh aspect, the adhering matter and the detergent liquid adhering to the surface of the stirring member can be washed off while rotating the stirring member, and a higher cleaning effect is obtained. Can do.
Further, since the cleaning liquid is discharged from the cleaning liquid discharge port disposed above the detergent liquid discharge port, the detergent liquid adhering to the upper surface of the stirring member relative to the detergent liquid discharge port can be surely washed off with the cleaning liquid.

  According to an eighth aspect of the present invention, in the method for cleaning a stirring member according to the sixth aspect or the seventh aspect, the detergent liquid fed by the detergent liquid pump is discharged through the detergent liquid supply path. The cleaning liquid discharged from the outlet and fed by the cleaning liquid pump is discharged from the cleaning liquid discharge port through a cleaning liquid supply path different from the detergent liquid supply path.

  In the cleaning method of the stirring member according to the eighth aspect, the detergent liquid fed by the detergent liquid pump is discharged from the detergent liquid discharge port via the detergent liquid supply path, and the cleaning liquid sent by the washing liquid pump is used as the detergent liquid supply path. Since the cleaning liquid is discharged from the cleaning liquid discharge port through a different cleaning liquid supply path, the detergent liquid and the cleaning liquid are not mixed, only the detergent liquid is discharged from the detergent liquid discharging means, and the cleaning liquid is discharged from the cleaning liquid discharge port. Only can be discharged. Thereby, the stirring member can be efficiently cleaned with the minimum necessary detergent liquid and cleaning liquid.

  As described above, since the cleaning apparatus according to the first aspect has the above-described configuration, it has an excellent effect that the cleaning effect of the stirring member can be enhanced. Moreover, it has the outstanding effect that the detergent liquid adhering to the surface of the stirring member can be reliably washed off with the cleaning liquid.

  Moreover, according to the washing | cleaning method of the stirring member which concerns on a 6th aspect, it has the outstanding effect that the washing | cleaning effect of a stirring member can be improved. Moreover, it has the outstanding effect that the detergent liquid adhering to the surface of the stirring member can be reliably washed off with the cleaning liquid.

It is a top view of an analyzer provided with a washing device concerning a 1st embodiment of the present invention. It is a perspective view which shows the upper part vicinity of a stirring rod washing | cleaning apparatus. It is a disassembled perspective view which shows the upper part vicinity of a stirring rod washing | cleaning apparatus. It is a longitudinal cross-sectional view of a stirring rod cleaning apparatus. 4B is a cross-sectional view of the stirring rod cleaning device shown in FIG. It is CC sectional view taken on the line of the stirring rod washing | cleaning apparatus shown to FIG. 4A. It is a top view of the analyzer which has a stirring rod in a washing position. These are the longitudinal cross-sectional views of the stirring rod washing | cleaning apparatus of the analyzer which concerns on the 2nd Embodiment of this invention. It is a side view of a V jet spray nozzle. It is a top view of a V jet spray nozzle. It is a longitudinal cross-sectional view of the upper part vicinity of the stirring rod washing | cleaning apparatus of the analyzer which concerns on the 3rd Embodiment of this invention.

[First Embodiment]
A first embodiment of the present invention will be described with reference to FIGS.
[Overall configuration of analyzer]
As shown in FIG. 1, the analyzer 10 of the present embodiment collects a sample (liquid) to be analyzed from a cassette loading unit 16 for loading a cassette 14 containing a plurality of sample containers 12 and a sample container 12. A pipette device 24 equipped with a pipette 22 for injecting into the cell 20, a pipette washing device 26 for washing the pipette 22, a turntable 28 provided with a plurality of cells 20 in the circumferential direction, and a reagent nozzle 30 for injecting a reagent into the cell 20. , A reagent liquid tank 34 storing the reagent, a reagent nozzle cleaning device 35 for cleaning the reagent nozzle 30, and a stirring rod 36 (to be described later) for stirring the sample and the reagent injected into the cell 20 2), a cell washing device 40 for washing the cell 20, a stirring rod washing device 42 for washing the stirring rod 36, and a reagent mixed therein And a analytical sensor 43 or the like for analyzing the charges.

The stirring device 38 includes an arm 38A that rotatably supports a stirring rod 36 that extends downward at a lower portion of the tip. The arm 38A rotates a horizontal movement device (not shown) that moves the arm 38A in the longitudinal direction, a vertical movement device (not shown) that moves the arm 38A in the vertical direction, and a stirring rod 36 (see FIG. 2) described later. A rotating device (motor) 39 is provided.
As shown in FIG. 2, the stirring rod 36 is formed of a round bar-like member, and includes a stirring portion 36 </ b> A that is pressed into a flat shape slightly above the lower end. The upper end of the stirring rod 36 is connected to the rotating shaft of a rotating device (not shown in FIG. 2) 39.

[Stirring bar cleaning device]
As shown in FIGS. 2 to 3, the stirring rod cleaning device 42 includes a cylindrical cleaning container main body 44 that is erected vertically.
As shown in FIG. 3, a substantially rectangular notch 46 having a groove shape is formed on the upper side of the cleaning container main body 44 on the arrow R direction side in FIG.

A cleaning liquid discharge head 48 is attached to the notch 46.
The cleaning liquid discharge head 48 is formed in a substantially rectangular parallelepiped shape and includes a block-shaped main body portion 50 that fits into the notch 46. The main body 50 has a substantially half of one end in the longitudinal direction (arrow L direction side) fitted into the notch 46 and fixed with an adhesive or the like.
The cleaning container main body 44 and the cleaning liquid discharge head 48 of the present embodiment are made of synthetic resin, but may be made of metal such as stainless steel as long as they are not altered by the sample or reagent.

A rectangular wide groove 52 extending in the vertical direction is formed on one end side in the longitudinal direction of the main body 50. In addition, both sides of the wide groove 52 of the main body 50 are side walls 54.
A narrow groove 56 narrower than the wide groove 52 is formed at the center of the bottom of the wide groove 52 so as to extend in the vertical direction.
In an intermediate portion in the groove depth direction of the narrow groove 56 (portion coincident with the central axis of the cylindrical cleaning container main body 44), the stirring portion 36A of the stirring rod 36 is arcuate so as not to contact the cleaning liquid discharge head 48. The concave relief 58 is formed in both groove walls.

As shown in FIG. 4, a cleaning liquid lateral flow path 60 having a circular cross section is formed in the main body 50 from one end side to the other end side along the longitudinal direction. One end of the cleaning liquid lateral flow path 60 communicates with the narrow groove 56, and the portion opened to the narrow groove 56 corresponds to the cleaning liquid discharge port of the present invention.
On the lower surface of the other end side of the main body 50 of the cleaning liquid discharge head 48, there are a large diameter hole 63A into which the first connection pipe 62 connected to the cleaning liquid lateral flow path 60 is inserted, and a small diameter hole 63B having a smaller diameter than the first connection pipe 62. Is formed. The first connection pipe 62 is inserted into the large-diameter hole 63A and is fixed to the main body 50 with an adhesive or the like.

  One end of a first tube 64 is connected to the first connection pipe 62, and a first electromagnetic valve 66, a cleaning liquid pump 68, and a cleaning liquid tank 70 are provided on the other end side of the first tube 64. The cleaning liquid tank 70 stores a cleaning liquid (rinsing liquid) 72 for washing away a later-described detergent liquid 86 attached to the stirring rod 36. The cleaning liquid can be washed away from the detergent liquid adhering to the stirring bar 36, and any type of water (ion-exchanged water, distilled water, etc.) can be used as long as it does not affect the analysis result.

A large-diameter hole 76 into which the second connection pipe 74 is inserted and a small-diameter hole 78 having a smaller diameter than the second connection pipe 74 are formed in the side portion of the cleaning container main body 44. The second connection pipe 74 is inserted into the large-diameter hole 76 and is fixed to the cleaning container main body 44 with an adhesive or the like.
In addition, the opening part inside the container of the small diameter hole 78 is corresponded to the detergent liquid discharge outlet of this invention.
One end of a second tube 79 is connected to the second connection pipe 74, and a detergent liquid pump 82 and a detergent liquid tank 84 are provided on the other end side of the second tube 79. A second electromagnetic valve 80 may be provided between the second tube 79 and the detergent liquid pump 82 as indicated by a two-dot chain line in FIG. 4A as necessary. The detergent liquid tank 84 stores a detergent liquid 86 for removing deposits adhering to the stirring rod 36. The detergent solution 86 is not particularly limited as long as it can remove deposits attached to the stirring bar 36 from the stirring bar 36, and a neutral detergent solution, an alkaline detergent solution, an acidic detergent solution, or the like is used. be able to.

As shown in FIGS. 3 and 4, a wall body 88 having a substantially L-shaped cross section and extending downward is provided on the lower surface on one end side of the main body 50. The wall 88 is disposed at a right angle with the first wall 88A on one end side in the width direction of the first wall 88A and the first wall 88A provided at a position facing the small-diameter hole 78. 2 wall portions 88B.
The first wall portion 88A and the second wall portion 88B are arranged with a gap from the stirring rod 36 (and the stirring portion 36A), and do not come into contact with the stirring rod 36.

As shown in FIG. 4, a bottom plate 90 is fixed to the lower end of the cleaning container main body 44 with an adhesive or the like. A joint 94 is fixed to the hole 92 formed in the center of the bottom plate 90 with an adhesive or the like. One end of a waste liquid tube 96 is connected to the joint 94, and the other end of the waste liquid tube 96 is inserted into a waste liquid tank (not shown).
Devices that are driven in the analyzer 10 (for example, a rotating device (motor) 39 that rotates the stirring rod 36, a first electromagnetic valve 66, a cleaning liquid pump 68, a second electromagnetic valve 80, a detergent liquid pump 82, etc.) Is configured to be controlled by a control device (not shown) in which a control program is stored.

(Function, effect)
First, an outline of a sample analysis process by the analyzer 10 of the present embodiment will be described.
In the analyzer 10 of this embodiment, the pipette 22 of the pipette device 24 collects a sample (liquid) from a predetermined sample container 12 and injects the collected sample into a predetermined cell 20 of the turntable 28. The turntable 28 rotates in the direction opposite to the clockwise direction (the direction opposite to the arrow CW direction), and the reagent is injected from the reagent nozzle 30 into the cell 20 into which the sample has been injected.

  Thereafter, the turntable 28 rotates in the clockwise direction (arrow CW direction), and the arm 38A moves as shown in FIG. 1 so that the stirring bar 36 is positioned above the cell 20 into which the sample and the reagent are injected. . Thereafter, the stirring bar 36 is inserted into the cell 20, and the sample and the reagent are mixed by rotating the stirring bar 36.

After the sample and the reagent are mixed, the stirring rod 36 is pulled up above the cell 20, and the cell 20 mixed with the sample and the reagent rotates the turntable 28 in the direction opposite to the clockwise direction, and the analysis sensor 43. The analysis sensor 43 performs analysis of a sample that is disposed at a position opposite to and in which a reagent is mixed.
After the analysis is completed, the turntable 28 is rotated clockwise, and the cell containing the sample is cleaned by the cell cleaning device 40.

(Washing the stirring bar)
Next, the cleaning of the stirring bar 36 of this embodiment will be described below.
(1) The stirring bar 36 after stirring the sample and the reagent is located at the center of the stirring bar 36 connected to the rotating device 39 above the washing container main body 44 indicated by a dotted line, as shown in FIGS. The shaft and the central axis of the cleaning container main body 44 are moved so as to coincide with each other.

(2) The stirring bar 36 is lowered, and the cleaning part (at least the part immersed in the sample) of the stirring bar 36 is inserted into the cleaning container main body 44. In addition, the washing | cleaning site | part of the stirring rod 36 is arrange | positioned below the small diameter hole 78 from which the detergent liquid 86 is discharged (refer FIG. 4).

(3) When the arrangement of the stirring bar 36 is completed, the detergent solution 86 is discharged from the small diameter hole 78 toward the stirring bar 36, and at least the cleaning portion is washed with the detergent solution 86. The detergent liquid 86 that has hit the wall 88 is repelled by the wall 88 and hits the stirring bar 36.
As described above, the detergent liquid 86 is discharged onto the stirring bar 36, so that deposits such as a sample attached to the stirring bar 36 are washed away with the detergent liquid 86. At this time, the stirring rod 36 may be in a stationary state (non-rotating state), but by rotating (for example, several tens to several hundreds of rotations / minute), a higher cleaning effect than in the case where the stirring rod 36 is stationary. Thus, the deposits can be washed out efficiently and reliably.
The detergent liquid 86 used for cleaning the stirring bar 36 is discharged to a waste liquid tank (not shown) through a waste liquid tube 96.

  The discharge time and the discharge amount of the detergent liquid 86 are set in advance so that the adhered matter such as the sample attached to the stirring rod 36 is sufficiently washed away (for example, the discharge time of the detergent liquid 86 is about 1 second. The discharge amount of the detergent liquid 86 is about 1 cc). Here, “the adhering material such as the sample adhering to the stirring bar 36 is sufficiently washed out” means that the adhering material such as the sample adhering to the stirring bar 36 affects the analysis result of the next sample. It means not (less than the measurement limit of the analyzer).

(4) When the discharge of the detergent liquid 86 is completed, the cleaning liquid 72 is discharged from the terminal of the cleaning liquid lateral flow path 60 (the end of the present invention). The cleaning liquid 72 discharged from the terminal of the cleaning liquid lateral flow path 60 falls and travels along the side surface of the wall body 88 and the stirring bar 36 and reaches the cleaning portion of the stirring bar 36 disposed below the terminal of the cleaning liquid cross flow path 60. The detergent solution 86 applied and adhered to the stirring bar 36 is washed away. At this time, by rotating the stirring rod 36, the detergent solution 86 attached to the stirring rod 36 can be washed out more efficiently and reliably than when the stirring rod 36 is not rotated.

Further, the cleaning liquid 72 discharged from the terminal of the cleaning liquid lateral flow path 60 can wash away the detergent liquid 86 attached not only to the stirring rod 36 but also to the wall 88 and the inner peripheral surface of the cleaning container main body 44. That is, since the stirring bar 36 is rotating, the detergent liquid 86 adhering to the wall 88 and the inner peripheral surface of the cleaning container main body 44 is efficiently and reliably washed by the cleaning liquid 72 splashed upon the stirring bar 36. Can be dropped.
The cleaning liquid 72 used for cleaning the stirring rod 36 is discharged to a waste liquid tank (not shown) through a waste liquid tube 96.

  The discharge time and the discharge amount of the cleaning liquid 72 are set in advance so that at least the detergent liquid 86 adhering to the stirring rod 36 is sufficiently washed away (for example, the discharge time of the cleaning liquid 72 is about 2 seconds, the cleaning liquid 72 The discharge amount is 1cc or more). Here, “the detergent solution 86 adhering to the stirring bar 36 is sufficiently washed off” means that the detergent solution 86 adhering to the stirring bar 36 is washed away so as not to affect the analysis result of the next sample. (Below the measurement limit of the analyzer).

(5) The stirring rod 36 from which the detergent solution 86 has been washed away by the cleaning liquid 72 is raised and moved above the cleaning container main body 44 and used for stirring the next sample.
As described above, in the stir bar cleaning device 42 of the analyzer 10 of the present embodiment, the adhering matter adhering to the stir bar 36 is washed away with the detergent liquid 86, and then the detergent solution 86 adhering to the stir bar 36 is washed with the cleaning liquid 72. In this case, the analysis result of the next sample is not affected by the previous sample.
Further, in the stirring rod cleaning device 42 of the present embodiment, since the liquid supply path for the detergent liquid 86 and the liquid supply path for the cleaning liquid 72 are provided independently of each other, the detergent liquid 86 and the cleaning liquid 72 are supplied to the cleaning container. The detergent liquid 86 and the cleaning liquid 72 are not mixed until they are discharged into the main body 44, and the detergent liquid 86 and the cleaning liquid 72 are not used wastefully. The stirring rod 36 can be cleaned efficiently and reliably.

[Second Embodiment]
Next, a second embodiment of the present invention will be described with reference to FIG.
As shown in FIG. 6, in the stirring rod cleaning device 42 of the present embodiment, a V jet spray nozzle 98 is attached to the tip of the second connection pipe 74.

As shown in FIG. 6B and FIG. 6C, the detergent liquid 86 is sprayed from the V jet spray nozzle 98 toward the cleaning portion of the stirring rod 36 so as to diffuse like a fan. As shown in FIG. 6B, the vertical diffusion angle θ1 is set wider than the horizontal diffusion angle θ2 as shown in FIG. 6C, and at a higher pressure than in the first embodiment. Detergent liquid 86 hits the stirring rod 36. In addition, the jet hole (diameter) sectional area (not shown) of the V jet spray nozzle 98 is set smaller than the (inner diameter) sectional area of the second connection pipe 74.
For this reason, the stirring rod cleaning device 42 of the second embodiment can obtain a higher cleaning effect than the stirring rod cleaning device 42 of the first embodiment.

[Third Embodiment]
Next, a stirring bar cleaning device 42 according to a third embodiment of the present invention will be described with reference to FIG.
As shown in FIG. 7, the stir bar cleaning device 42 of the analyzer 10 of the present embodiment is different from the first embodiment in that the cleaning container main body 44 is not provided with a notch 46, and the cleaning liquid discharge head. 48 is also not attached.

A first connection pipe 62 and a second connection pipe 74 are inserted from the upper opening of the cleaning container main body 44. The tip of the first connection pipe 62 is disposed above the tip of the second connection pipe 74, and the cleaning liquid 72 is discharged from the tip of the first connection pipe 62 toward the rotating stirring rod 36. The detergent solution 86 can be discharged from the tip of the second connection pipe 74 toward the rotating stirring rod 36.
Therefore, similarly to the stirring bar cleaning device 42 of the first embodiment, the stirring bar cleaning device 42 of the present embodiment can reliably clean the stirring bar 36.

In the above embodiment, water is used as the cleaning liquid. However, the cleaning liquid may be a liquid other than water, and any liquid that does not affect the analysis result may be used.
As shown in FIG. 2, in the stirring rod cleaning device 42 of the first embodiment, a substantially T-shaped opening is formed in the upper part of the cleaning container main body 44. However, the present invention is not limited to this, and the cleaning container It is only necessary that a small round hole or the like that allows the stirring rod 36 to be inserted into the inside of the cleaning container main body 44 is opened above the main body 44.

  Although the embodiment of the present invention has been described above, the present invention is not limited to the above, and it is needless to say that the present invention can be variously modified and implemented without departing from the spirit of the present invention. is there.

10 Analyzer 36 Stir bar (stirring member)
42 Stir bar cleaning device (cleaning device)
44 Cleaning container body (cleaning container, cylindrical body)
60 Cleaning fluid lateral flow path (transverse flow path, cleaning liquid discharge port)
62 1st connection pipe (cleaning liquid discharge means)
64 Tube (cleaning liquid discharge means)
66 1st solenoid valve (cleaning liquid discharge means)
68 Cleaning liquid pump (cleaning liquid discharge means)
70 Cleaning liquid tank (cleaning liquid discharge means)
72 Cleaning liquid 74 Second connection pipe (detergent liquid discharge means)
78 Small hole (detergent outlet)
79 Tube (detergent solution discharge means)
80 Second solenoid valve (detergent solution discharge means)
82 Detergent liquid pump (detergent liquid pump, detergent liquid discharge means)
84 Detergent liquid tank (detergent liquid discharge means)
86 Detergent solution 88 Wall 90 Bottom plate (cleaning container)
98 Jet spray nozzle (diffusion port)

Claims (8)

A cleaning container into which a stirring member for stirring the sample to be analyzed is inserted;
A detergent liquid discharge port for discharging the detergent liquid to the stirring member inserted into the cleaning container to wash away the adhering matter adhering to the surface of the stirring member;
A cleaning liquid discharge port that is disposed above the detergent liquid discharge port and discharges the cleaning liquid to the stirring member to wash off the detergent liquid adhering to the surface of the stirring member;
Cleaning device equipped with. Detergent liquid discharge means for discharging the detergent liquid fed by the detergent liquid pump from the detergent liquid discharge port via the detergent liquid supply path;
A cleaning liquid discharge means for discharging the cleaning liquid fed by the cleaning liquid pump from the cleaning liquid discharge port via a cleaning liquid supply path different from the detergent liquid supply path;
The cleaning apparatus according to claim 1. The detergent liquid discharge port is provided on a side wall of the cleaning container,
The cleaning apparatus according to claim 1, wherein a wall body that repels the detergent liquid discharged from the detergent liquid discharge port toward the stirring member is disposed in the cleaning container. The cleaning container includes a cylindrical body,
The upper opening part of the said cylindrical body is provided with the horizontal flow path which flows the said washing | cleaning liquid to a horizontal direction, The flow end of the said horizontal flow path is made into the washing | cleaning liquid discharge outlet of the said washing | cleaning liquid. The cleaning apparatus according to any one of claims.   The cleaning device according to any one of claims 1 to 4, wherein the detergent liquid discharge port includes a diffusion port that diffuses the detergent solution toward the stirring member. A stirring member for stirring the sample to be analyzed was inserted into the cleaning container, and the detergent liquid fed by the detergent liquid pump to the stirring member was discharged from the detergent liquid discharge port and adhered to the surface of the stirring member. A first step of washing off the deposits;
After the first step, the detergent adhered to the surface of the stirring member by discharging the cleaning liquid sent to the stirring member by the cleaning liquid pump from the cleaning liquid discharge port disposed above the detergent liquid discharge port. A second step of washing off the liquid;
Cleaning method for stirring member having In the first step, while rotating the agitating member, the detergent liquid fed by the detergent liquid pump to the agitating member is discharged from the detergent liquid discharge port, and the adhering matter adhering to the surface of the agitating member is removed. Wash off,
In the second step, while the stirring member is rotated, the cleaning liquid sent to the stirring member by a cleaning liquid pump is discharged from a cleaning liquid discharge port disposed above the detergent liquid discharge port, and the stirring is performed. Washing off the detergent solution adhering to the surface of the member,
The method for cleaning a stirring member according to claim 6. Discharging the detergent liquid fed by the detergent liquid pump from the detergent liquid outlet through the detergent liquid supply path,
The method for cleaning a stirring member according to claim 6 or 7, wherein the cleaning liquid fed by the cleaning liquid pump is discharged from the cleaning liquid discharge port via a cleaning liquid supply path different from the detergent liquid supply path.

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