JPS6316008A - Production of filtration filter - Google Patents
Production of filtration filterInfo
- Publication number
- JPS6316008A JPS6316008A JP15925186A JP15925186A JPS6316008A JP S6316008 A JPS6316008 A JP S6316008A JP 15925186 A JP15925186 A JP 15925186A JP 15925186 A JP15925186 A JP 15925186A JP S6316008 A JPS6316008 A JP S6316008A
- Authority
- JP
- Japan
- Prior art keywords
- filter
- solvent
- synthetic resin
- ceramic
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001914 filtration Methods 0.000 title claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 239000000919 ceramic Substances 0.000 claims abstract description 17
- 229920003002 synthetic resin Polymers 0.000 claims abstract description 10
- 239000000057 synthetic resin Substances 0.000 claims abstract description 10
- 239000002904 solvent Substances 0.000 claims abstract 10
- 239000012528 membrane Substances 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims description 5
- 239000011159 matrix material Substances 0.000 claims 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 239000007788 liquid Substances 0.000 abstract description 6
- 229920002492 poly(sulfone) Polymers 0.000 abstract description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract description 2
- 230000002572 peristaltic effect Effects 0.000 abstract description 2
- 239000011148 porous material Substances 0.000 abstract description 2
- 241001515965 unidentified phage Species 0.000 abstract description 2
- 239000012466 permeate Substances 0.000 abstract 2
- 244000052616 bacterial pathogen Species 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 210000001072 colon Anatomy 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 description 4
- 230000001954 sterilising effect Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 239000002510 pyrogen Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
【発明の詳細な説明】
〔産業上の利用分野〕
本発明は、除菌やパイロジエンの除去に用いる濾過フィ
ルターの製造方法に関する。DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a method for manufacturing a filter used for sterilization and pyrogen removal.
従来より、多孔質セラミッスクは高い耐熱性のために、
加熱滅菌可能であると共に、剛性が高く、構造体として
部品化することができるため、滅菌の必要がある濾過に
用いるフィルターとして使用されてきた。Traditionally, porous ceramic disks have been used for their high heat resistance.
It can be heat sterilized, has high rigidity, and can be made into components as a structural body, so it has been used as a filter for filtration that requires sterilization.
〔発明が解決しようとした、問題点
〕多孔質のセラミックスフィルターは除菌やパイロジエ
ンの除去など除去を目的とした場合には、濾過に加え、
高い吸着能を有するために高い性能を有したが、濾液中
の有用物質の回収を目的とした場合には、セラミックス
の吸着能は、有用物質の回収率を低下させる要因であっ
た。[Problem that the invention sought to solve] When the porous ceramic filter is used for purposes such as sterilization or pyrogen removal, it can be used in addition to filtration.
Although ceramics had high performance due to their high adsorption capacity, when the purpose was to recover useful substances in the filtrate, the adsorption capacity of ceramics was a factor that reduced the recovery rate of useful substances.
本発明は、前記問題点を解決するために、濾過中の液体
が、直接セラミックスに接触することを防止する、合成
樹脂を、セラミックス表面に付着させた濾過フィルター
の製造方法を提供するものである。In order to solve the above-mentioned problems, the present invention provides a method for manufacturing a filter in which a synthetic resin is attached to the ceramic surface to prevent the liquid being filtered from coming into direct contact with the ceramic. .
Ｃ実施例〕
以下図面に基づいて、本発明の好適な一実施例を以下に
説明する。平均孔径２μｍに調製された、厚さ２．５鳳
鳳のアルミナセラミックスフィルタ−図に示す濾過装置
に取りつけ、原液槽２内に貯えられた１０％ポリサルホ
ン／ジメチルホルムアミド溶液を、ペリスタリンクポン
プ３を介して透過させ、セラミックスフィルターの両表
面を軽く拭き取った後、水中に投じ３０秒間放置し、表
面にポリサルホン膜を形成し、第１図に示す濾過装置の
原液槽２内の液体を水と交換し、ポンプ３によって前記
１０％ポリサルホン／ジメチルホルムアミドを浸透させ
たセラミックスフィルター１を透過させたところ、ジメ
チルホルムアミドのみが水に溶解、除去された。この様
にして作成された濾過フィルター１は、大腸菌を透過さ
せないが、バクテリオファージ並びにＤＮＡを吸着せず
に、透過させる事が明らかであった。C Embodiment] A preferred embodiment of the present invention will be described below based on the drawings. A 2.5 mm thick alumina ceramic filter prepared to have an average pore diameter of 2 μm is attached to the filtration device shown in the figure, and the 10% polysulfone/dimethylformamide solution stored in the stock solution tank 2 is passed through the peristaltic pump 3. After lightly wiping both surfaces of the ceramic filter, it is placed in water and left for 30 seconds to form a polysulfone film on the surface, and the liquid in the stock solution tank 2 of the filtration device shown in Figure 1 is mixed with water. When the water was replaced and passed through the ceramic filter 1 impregnated with the 10% polysulfone/dimethylformamide using the pump 3, only dimethylformamide was dissolved in the water and removed. It was clear that the filtration filter 1 prepared in this manner did not allow E. coli to pass through it, but allowed bacteriophage and DNA to pass through it without adsorbing it.
上記構成、作用によれば、有用物質を吸着することなく
、濾過を実行することができ、有用物質の回収率を著し
く向上させることができる。According to the above structure and operation, filtration can be performed without adsorbing useful substances, and the recovery rate of useful substances can be significantly improved.
図面は、本発明による濾過フィルターの製造方法を実施
するための、濾過装置の構成を示す図である。
１、セラミックスフィルター
２、 原ン夜槽
３、ペリスタリンクポンプ
以上The drawings are diagrams showing the configuration of a filtration device for carrying out the method for manufacturing a filtration filter according to the present invention. 1. Ceramic filter 2. Haran night tank 3. Peristalink pump or higher
Claims (2)
た合成樹脂を塗布し、その合成樹脂を溶解せず、第一の
溶媒と、混合可能な第二の溶媒にて第一の溶媒を抽出除
去し、合成樹脂を多孔質膜として、上記多孔質セラミッ
クス表面に定着せしめることを特徴とした濾過フィルタ
ーの製造方法。(1) Apply a synthetic resin dissolved in a first solvent to the surface of the porous ceramic, and remove the first solvent using a second solvent that is miscible with the first solvent without dissolving the synthetic resin. A method for manufacturing a filtration filter, which comprises extracting and removing the synthetic resin, and fixing the synthetic resin as a porous membrane on the surface of the porous ceramic.
一の溶媒に溶解した合成樹脂を浸透させ、その合成樹脂
を溶解せず第一の溶媒と、混合可能な第二の溶媒にて第
一の溶媒を抽出除去し、セラミックスのマトリックス中
に、合成樹脂のマトリックスを形成せしめることを特徴
とした、特許請求の範囲第１項記載の濾過フィルターの
製造方法。(2) A synthetic resin dissolved in a first solvent is infiltrated into the matrix of the porous ceramic, and a second solvent is mixed with the first solvent without dissolving the synthetic resin. 2. A method for manufacturing a filtration filter according to claim 1, wherein the solvent is extracted and removed to form a synthetic resin matrix in a ceramic matrix.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15925186A JPS6316008A (en) | 1986-07-07 | 1986-07-07 | Production of filtration filter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15925186A JPS6316008A (en) | 1986-07-07 | 1986-07-07 | Production of filtration filter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6316008A true JPS6316008A (en) | 1988-01-23 |
Family
ID=15689662
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP15925186A Pending JPS6316008A (en) | 1986-07-07 | 1986-07-07 | Production of filtration filter |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6316008A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20200110297A (en) * | 2018-01-15 | 2020-09-23 | 도레이 카부시키가이샤 | Tubular integrally molded article and method of manufacturing tubular integrally molded article |
-
1986
- 1986-07-07 JP JP15925186A patent/JPS6316008A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20200110297A (en) * | 2018-01-15 | 2020-09-23 | 도레이 카부시키가이샤 | Tubular integrally molded article and method of manufacturing tubular integrally molded article |
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