JPS5799545A - Preparation of chloroacetaldehyde - Google Patents
Preparation of chloroacetaldehydeInfo
- Publication number
- JPS5799545A JPS5799545A JP17617780A JP17617780A JPS5799545A JP S5799545 A JPS5799545 A JP S5799545A JP 17617780 A JP17617780 A JP 17617780A JP 17617780 A JP17617780 A JP 17617780A JP S5799545 A JPS5799545 A JP S5799545A
- Authority
- JP
- Japan
- Prior art keywords
- alkali
- chloroacetaldehyde
- acetaldehyde
- hydrogen chloride
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prevent the reduction in yield by the deterioration and increase the concentration, by neutralizing the formed hydrogen chloride as a by-product with an alkali into an alkali chloride in reacting acetaldehyde, etc. with chlorine to give chloroacetaldehyde which is a raw material for medicines.
CONSTITUTION: Acetaldehyde or para-acetaldehyde is reacted with chlorine to prepare chloroacetaldehyde. In the process, the formed hydrogen chloride as a by-product is neutralized with an alkali, preferably sodium hydroxide or calcium hydroxide, to give the alkali chloride, which is then separated by the filtration. The resultant filtrate is then distilled to afford the aimed compound. The molar amount of the alkali is 0.7W1.2times, preferably 0.85W1.0, that of the hydrogen chloride. The alkali may be added continuously or in portions to the reaction mixture.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP17617780A JPS5799545A (en) | 1980-12-12 | 1980-12-12 | Preparation of chloroacetaldehyde |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP17617780A JPS5799545A (en) | 1980-12-12 | 1980-12-12 | Preparation of chloroacetaldehyde |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5799545A true JPS5799545A (en) | 1982-06-21 |
Family
ID=16009001
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP17617780A Pending JPS5799545A (en) | 1980-12-12 | 1980-12-12 | Preparation of chloroacetaldehyde |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5799545A (en) |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS511688A (en) * | 1973-08-20 | 1976-01-08 | Townsend Engineering Co |
-
1980
- 1980-12-12 JP JP17617780A patent/JPS5799545A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS511688A (en) * | 1973-08-20 | 1976-01-08 | Townsend Engineering Co |
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