JPS54122231A - Preparation of benzyltributylammonium chloride - Google Patents
Preparation of benzyltributylammonium chlorideInfo
- Publication number
- JPS54122231A JPS54122231A JP2747578A JP2747578A JPS54122231A JP S54122231 A JPS54122231 A JP S54122231A JP 2747578 A JP2747578 A JP 2747578A JP 2747578 A JP2747578 A JP 2747578A JP S54122231 A JPS54122231 A JP S54122231A
- Authority
- JP
- Japan
- Prior art keywords
- benzyl chloride
- tributylamine
- chloroform
- reacting
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare the title compound useful as a cationic surfactant, a cationic dye, a phase transfer catalyst, etc., in high yield, by reacting tributylamine with benzyl chloride using easily recoverable chloroform as the reaction solvent.
CONSTITUTION: Benzyltributylammonium chloride is prepared by reacting (A) tributylamine with (B) benzyl chloride using (C) cloroform as reaction solvent. The amount of (B) component is slightly excees to the equivalent of (A), and the molar ratio of (C) to (A)+(B) is about 2-3 to 1. The chloroform can be recovered with a recovery of as high as 95%, by distillation or azeotropic distillation with water.
EFFECT: Homogenous reaction system. Decomposition of benzyl chloride does not take place.
USE: Especially useful as a catalyst for the production of medicines, pesticides, etc.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2747578A JPS54122231A (en) | 1978-03-10 | 1978-03-10 | Preparation of benzyltributylammonium chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2747578A JPS54122231A (en) | 1978-03-10 | 1978-03-10 | Preparation of benzyltributylammonium chloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS54122231A true JPS54122231A (en) | 1979-09-21 |
| JPS5744657B2 JPS5744657B2 (en) | 1982-09-22 |
Family
ID=12222131
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2747578A Granted JPS54122231A (en) | 1978-03-10 | 1978-03-10 | Preparation of benzyltributylammonium chloride |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS54122231A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002079185A1 (en) * | 2001-03-30 | 2002-10-10 | Nippon Soda Co., Ltd. | Process for producing (dioxolenon-4-yl)methyl ester derivative |
| JP2014024811A (en) * | 2012-07-27 | 2014-02-06 | Nippon Soda Co Ltd | Method of producing 1h-tetrazole derivative |
-
1978
- 1978-03-10 JP JP2747578A patent/JPS54122231A/en active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002079185A1 (en) * | 2001-03-30 | 2002-10-10 | Nippon Soda Co., Ltd. | Process for producing (dioxolenon-4-yl)methyl ester derivative |
| JP2014024811A (en) * | 2012-07-27 | 2014-02-06 | Nippon Soda Co Ltd | Method of producing 1h-tetrazole derivative |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5744657B2 (en) | 1982-09-22 |
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