JPH0678558B2 - 洗剤組成物の製造方法 - Google Patents
洗剤組成物の製造方法Info
- Publication number
- JPH0678558B2 JPH0678558B2 JP1190427A JP19042789A JPH0678558B2 JP H0678558 B2 JPH0678558 B2 JP H0678558B2 JP 1190427 A JP1190427 A JP 1190427A JP 19042789 A JP19042789 A JP 19042789A JP H0678558 B2 JPH0678558 B2 JP H0678558B2
- Authority
- JP
- Japan
- Prior art keywords
- weight
- water
- mixer
- powder
- rpm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims description 87
- 239000003599 detergent Substances 0.000 title claims description 52
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 239000007787 solid Substances 0.000 claims description 70
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 69
- 238000000034 method Methods 0.000 claims description 66
- 239000007788 liquid Substances 0.000 claims description 49
- 238000006386 neutralization reaction Methods 0.000 claims description 45
- 239000002253 acid Substances 0.000 claims description 35
- 239000003945 anionic surfactant Substances 0.000 claims description 32
- 239000002243 precursor Substances 0.000 claims description 28
- 239000000126 substance Substances 0.000 claims description 23
- 230000008569 process Effects 0.000 claims description 20
- 239000011230 binding agent Substances 0.000 claims description 14
- 230000003472 neutralizing effect Effects 0.000 claims description 12
- 238000010008 shearing Methods 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 5
- 239000003513 alkali Substances 0.000 claims description 4
- 239000000843 powder Substances 0.000 description 73
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 64
- 229910000029 sodium carbonate Inorganic materials 0.000 description 32
- 235000017550 sodium carbonate Nutrition 0.000 description 32
- 239000000047 product Substances 0.000 description 25
- 239000002245 particle Substances 0.000 description 23
- 238000005469 granulation Methods 0.000 description 19
- 230000003179 granulation Effects 0.000 description 19
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 16
- -1 alkylbenzene sulfonate Chemical class 0.000 description 16
- 235000019832 sodium triphosphate Nutrition 0.000 description 15
- 239000010457 zeolite Substances 0.000 description 15
- 239000003795 chemical substances by application Substances 0.000 description 14
- 239000004615 ingredient Substances 0.000 description 13
- 239000000344 soap Substances 0.000 description 13
- 229910021536 Zeolite Inorganic materials 0.000 description 12
- 238000001816 cooling Methods 0.000 description 12
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 12
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 12
- 239000004094 surface-active agent Substances 0.000 description 12
- 239000002736 nonionic surfactant Substances 0.000 description 11
- 150000003839 salts Chemical class 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 229910021532 Calcite Inorganic materials 0.000 description 8
- 238000011065 in-situ storage Methods 0.000 description 8
- 239000011541 reaction mixture Substances 0.000 description 8
- 239000005909 Kieselgur Substances 0.000 description 7
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 7
- 229910052783 alkali metal Inorganic materials 0.000 description 7
- 150000004996 alkyl benzenes Chemical class 0.000 description 7
- 229910000323 aluminium silicate Inorganic materials 0.000 description 7
- 229910052938 sodium sulfate Inorganic materials 0.000 description 7
- 235000011152 sodium sulphate Nutrition 0.000 description 7
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 6
- 230000002776 aggregation Effects 0.000 description 6
- 239000001768 carboxy methyl cellulose Substances 0.000 description 6
- 239000008187 granular material Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 230000000717 retained effect Effects 0.000 description 6
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 6
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 6
- 229910000632 Alusil Inorganic materials 0.000 description 5
- 238000005054 agglomeration Methods 0.000 description 5
- 150000001340 alkali metals Chemical class 0.000 description 5
- 239000002585 base Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- 239000012467 final product Substances 0.000 description 5
- 239000008247 solid mixture Substances 0.000 description 5
- 239000004711 α-olefin Substances 0.000 description 5
- 239000005995 Aluminium silicate Substances 0.000 description 4
- 102000004190 Enzymes Human genes 0.000 description 4
- 108090000790 Enzymes Proteins 0.000 description 4
- 239000004115 Sodium Silicate Substances 0.000 description 4
- 235000012211 aluminium silicate Nutrition 0.000 description 4
- 150000008064 anhydrides Chemical class 0.000 description 4
- 239000000440 bentonite Substances 0.000 description 4
- 229910000278 bentonite Inorganic materials 0.000 description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 150000004665 fatty acids Chemical class 0.000 description 4
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 229910052594 sapphire Inorganic materials 0.000 description 4
- 239000010980 sapphire Substances 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 4
- 229910052911 sodium silicate Inorganic materials 0.000 description 4
- QJRVOJKLQNSNDB-UHFFFAOYSA-N 4-dodecan-3-ylbenzenesulfonic acid Chemical compound CCCCCCCCCC(CC)C1=CC=C(S(O)(=O)=O)C=C1 QJRVOJKLQNSNDB-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 235000012216 bentonite Nutrition 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000001045 blue dye Substances 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 229910017053 inorganic salt Inorganic materials 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000010451 perlite Substances 0.000 description 3
- 235000019362 perlite Nutrition 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 229910000503 Na-aluminosilicate Inorganic materials 0.000 description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 239000002519 antifouling agent Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007850 fluorescent dye Substances 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 239000011976 maleic acid Substances 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 2
- 229920005646 polycarboxylate Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000000429 sodium aluminium silicate Substances 0.000 description 2
- 235000012217 sodium aluminium silicate Nutrition 0.000 description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
- 101100361281 Caenorhabditis elegans rpm-1 gene Proteins 0.000 description 1
- 241001137251 Corvidae Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000011276 addition treatment Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
- 229940092714 benzenesulfonic acid Drugs 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 239000004067 bulking agent Substances 0.000 description 1
- 235000012241 calcium silicate Nutrition 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 235000013351 cheese Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000112 cooling gas Substances 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 229940075057 doral Drugs 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 150000004687 hexahydrates Chemical class 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 235000014366 other mixer Nutrition 0.000 description 1
- 239000004482 other powder Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003138 primary alcohols Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 235000019794 sodium silicate Nutrition 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 125000001273 sulfonato group Chemical class [O-]S(*)(=O)=O 0.000 description 1
- 230000000153 supplemental effect Effects 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- POWFTOSLLWLEBN-UHFFFAOYSA-N tetrasodium;silicate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])[O-] POWFTOSLLWLEBN-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- MECHNRXZTMCUDQ-RKHKHRCZSA-N vitamin D2 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)/C=C/[C@H](C)C(C)C)=C\C=C1\C[C@@H](O)CCC1=C MECHNRXZTMCUDQ-RKHKHRCZSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB888817386A GB8817386D0 (en) | 1988-07-21 | 1988-07-21 | Detergent compositions & process for preparing them |
| GB8817386.9 | 1988-07-21 | ||
| GB8910087.9 | 1989-05-03 | ||
| GB898910087A GB8910087D0 (en) | 1988-07-21 | 1989-05-03 | Detergent compositions and process for preparing them |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0333199A JPH0333199A (ja) | 1991-02-13 |
| JPH0678558B2 true JPH0678558B2 (ja) | 1994-10-05 |
Family
ID=26294187
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1190427A Expired - Fee Related JPH0678558B2 (ja) | 1988-07-21 | 1989-07-21 | 洗剤組成物の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0352135B1 (xx) |
| JP (1) | JPH0678558B2 (xx) |
| BR (1) | BR8903627A (xx) |
| DE (1) | DE68918522T2 (xx) |
| ES (1) | ES2063826T3 (xx) |
| HK (1) | HK142995A (xx) |
| IN (1) | IN170991B (xx) |
| PH (1) | PH26671A (xx) |
| TR (1) | TR27078A (xx) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8818613D0 (en) * | 1988-08-05 | 1988-09-07 | Paterson Zochonis Uk Ltd | Detergents |
| US5269962A (en) * | 1988-10-14 | 1993-12-14 | The Clorox Company | Oxidant composition containing stable bleach activator granules |
| GB9001285D0 (en) * | 1990-01-19 | 1990-03-21 | Unilever Plc | Detergent compositions and process for preparing them |
| GB9012613D0 (en) * | 1990-06-06 | 1990-07-25 | Unilever Plc | Soap powder compositions |
| WO1992001035A1 (en) * | 1990-07-10 | 1992-01-23 | The Procter & Gamble Company | Process for making a high bulk density detergent composition |
| CA2027518A1 (en) * | 1990-10-03 | 1992-04-04 | Richard L. Tadsen | Process for preparing high density detergent compositions containing particulate ph sensitive surfactant |
| ES2118783T3 (es) * | 1991-03-28 | 1998-10-01 | Unilever Nv | Composiciones detergentes y procedimiento para su preparacion. |
| DE69220773T2 (de) * | 1992-02-14 | 1998-02-12 | Procter & Gamble | Verfahren zur Herstellung von Detergenskörnchen durch Neutralisation von Sulfonsäuren |
| DE4216629A1 (de) * | 1992-05-20 | 1993-11-25 | Henkel Kgaa | Verfahren zur Herstellung aniontensidhaltiger Wasch- und Reinigungsmittel |
| DK0578872T3 (da) * | 1992-07-15 | 1999-06-23 | Procter & Gamble | Detergentsammensætninger |
| DE4232874A1 (de) * | 1992-09-30 | 1994-03-31 | Henkel Kgaa | Verfahren zur Herstellung von Tensidgranulaten |
| US5703037A (en) * | 1994-04-20 | 1997-12-30 | The Procter & Gamble Company | Process for the manufacture of free-flowing detergent granules |
| EP0678573B1 (en) * | 1994-04-20 | 2000-11-29 | The Procter & Gamble Company | Process for the manufacture of free-flowing detergent granules |
| US5573697A (en) * | 1995-05-31 | 1996-11-12 | Riddick; Eric F. | Process for making high active, high density detergent granules |
| US5565422A (en) * | 1995-06-23 | 1996-10-15 | The Procter & Gamble Company | Process for preparing a free-flowing particulate detergent composition having improved solubility |
| US6521585B1 (en) * | 1995-11-06 | 2003-02-18 | Kao Corporation | Method for producing crystalline alkali metal silicate granules and granular high density detergent |
| GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
| DE19600466A1 (de) * | 1996-01-09 | 1997-07-10 | Henkel Kgaa | Verfahren zur Herstellung von granularen Wasch- oder Reinigungsmitteln bzw. Komponenten hierfür |
| TW397862B (en) * | 1996-09-06 | 2000-07-11 | Kao Corp | Detergent granules and method for producing the same, and high-bulk density detergent composition |
| DE19700776A1 (de) * | 1997-01-13 | 1998-07-16 | Henkel Kgaa | Granulares Waschmittel mit verbessertem Fettauswaschvermögen |
| DE19709991C2 (de) | 1997-03-11 | 1999-12-23 | Rettenmaier & Soehne Gmbh & Co | Waschmittelpreßling und Verfahren zu seiner Herstellung |
| DE19710254A1 (de) | 1997-03-13 | 1998-09-17 | Henkel Kgaa | Wasch- oder reinigungsaktive Formkörper für den Gebrauch im Haushalt |
| GB9711359D0 (en) * | 1997-05-30 | 1997-07-30 | Unilever Plc | Detergent powder composition |
| WO1998054289A1 (en) | 1997-05-30 | 1998-12-03 | Unilever Plc | Free-flowing particulate detergent compositions |
| GB9711831D0 (en) * | 1997-06-06 | 1997-08-06 | Unilever Plc | Cleaning compositions |
| GB9711829D0 (en) | 1997-06-06 | 1997-08-06 | Unilever Plc | Detergent compositions |
| PL342240A1 (en) * | 1998-02-10 | 2001-06-04 | Unilever Nv | Detergent composition for production of laundry washing tablets |
| US6576605B1 (en) * | 1998-10-28 | 2003-06-10 | The Procter & Gamble Company | Process for making a free flowing detergent composition |
| WO2001014511A1 (en) * | 1999-08-20 | 2001-03-01 | Kao Corporation | Process for preparing high-bulk density detergent compositions |
| DE10232304B4 (de) * | 2002-07-17 | 2005-10-27 | Henkel Kgaa | Neutralisation im Mischer |
| AU2003263591A1 (en) | 2002-09-06 | 2004-03-29 | Kao Corporation | Detergent particles |
| CN101068912A (zh) * | 2004-11-30 | 2007-11-07 | 株式会社Lg生活健康 | 改善衣物触感的洗衣洗涤剂组合物及其制备方法 |
| DE102005005499A1 (de) * | 2005-02-04 | 2006-08-17 | Henkel Kgaa | Verfahren zur Herstellung von Wasch- oder Reinigungsmitteln |
| EP1918361A4 (en) * | 2005-07-12 | 2008-10-15 | Kao Corp | DETERGENT PELLET AND MANUFACTURING METHOD THEREOF |
| EP1832648A1 (en) * | 2006-03-08 | 2007-09-12 | Unilever Plc | Laundry detergent composition and process |
| KR101392380B1 (ko) | 2007-02-21 | 2014-05-07 | 주식회사 엘지생활건강 | 산성형태의 수용성 고분자를 함유하는 분말세제 입자 및그의 제조방법 |
| BR112023026713A2 (pt) | 2021-06-24 | 2024-03-12 | Unilever Ip Holdings B V | Composição de limpeza em dose unitária |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ZA72295B (en) * | 1971-02-01 | 1973-09-26 | Colgate Palmolive Co | Method for neutralization of detergent acid |
| GB1404317A (en) * | 1971-10-23 | 1975-08-28 | Bell Chemicals Pty Ltd | Manufacture of detergent powders |
| JPS6072998A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 粉末物性に優れた界面活性剤粉体組成物の製造法 |
| JPS6072999A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 超濃縮粉末洗剤の製法 |
| ES8607378A1 (es) * | 1984-08-06 | 1986-05-16 | Kao Corp | Una composicion detergente en polvo de gran densidad |
| JPS6169897A (ja) * | 1984-09-14 | 1986-04-10 | 花王株式会社 | 流動性の改良された高密度の粒状洗剤の製法 |
| US4734224A (en) * | 1986-09-15 | 1988-03-29 | The Dial Corporation | Dry neutralization process for detergent slurries |
| JPH01121400A (ja) * | 1987-11-04 | 1989-05-15 | Nippon Gosei Senzai Kk | 高嵩密度洗浄剤の製造方法並びに洗浄剤組成物 |
| JPH01142000A (ja) * | 1987-11-28 | 1989-06-02 | Nippon Gosei Senzai Kk | 高級アルコール系高密度洗浄剤の製造方法並びに洗浄剤組成物 |
-
1989
- 1989-07-20 IN IN205/BOM/89A patent/IN170991B/en unknown
- 1989-07-21 TR TR00939/89A patent/TR27078A/xx unknown
- 1989-07-21 JP JP1190427A patent/JPH0678558B2/ja not_active Expired - Fee Related
- 1989-07-21 DE DE68918522T patent/DE68918522T2/de not_active Expired - Fee Related
- 1989-07-21 PH PH38981A patent/PH26671A/en unknown
- 1989-07-21 ES ES89307452T patent/ES2063826T3/es not_active Expired - Lifetime
- 1989-07-21 BR BR898903627A patent/BR8903627A/pt not_active IP Right Cessation
- 1989-07-21 EP EP89307452A patent/EP0352135B1/en not_active Revoked
-
1995
- 1995-09-07 HK HK142995A patent/HK142995A/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| ES2063826T3 (es) | 1995-01-16 |
| EP0352135A1 (en) | 1990-01-24 |
| EP0352135B1 (en) | 1994-09-28 |
| TR27078A (tr) | 1994-10-18 |
| HK142995A (en) | 1995-09-15 |
| BR8903627A (pt) | 1990-03-13 |
| PH26671A (en) | 1992-09-15 |
| DE68918522T2 (de) | 1995-03-09 |
| IN170991B (xx) | 1992-06-27 |
| DE68918522D1 (de) | 1994-11-03 |
| JPH0333199A (ja) | 1991-02-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH0678558B2 (ja) | 洗剤組成物の製造方法 | |
| KR920000114B1 (ko) | 세제조성물 및 그 제조방법 | |
| JP2918710B2 (ja) | 洗剤組成物とその調製方法 | |
| CA1337513C (en) | Detergent compositions and process for preparing them | |
| KR950004824B1 (ko) | 세제조성물 및 그 제조방법 | |
| US5929021A (en) | Process for preparing a granular detergent | |
| CA2242420C (en) | Process for the production of a detergent composition | |
| WO1995002036A1 (en) | Detergent composition or component containing anionic surfactant and process for its preparation | |
| KR920000113B1 (ko) | 세제조성물의 제조방법 | |
| US5736502A (en) | Process for preparing detergent compositions | |
| JPH0762160B2 (ja) | 粘土を含有する高嵩密度の洗剤粉末の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |