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JP5910284B2 - Coating method for threaded joint for steel pipe and threaded joint product for steel pipe - Google Patents

Coating method for threaded joint for steel pipe and threaded joint product for steel pipe Download PDF

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JP5910284B2
JP5910284B2 JP2012097525A JP2012097525A JP5910284B2 JP 5910284 B2 JP5910284 B2 JP 5910284B2 JP 2012097525 A JP2012097525 A JP 2012097525A JP 2012097525 A JP2012097525 A JP 2012097525A JP 5910284 B2 JP5910284 B2 JP 5910284B2
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box
threaded joint
pin
seal
female
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JP2013224707A (en
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孝将 川井
孝将 川井
高橋 一成
一成 高橋
博 近常
博 近常
吉川 正樹
正樹 吉川
順 高野
順 高野
拓也 長濱
拓也 長濱
植田 正輝
正輝 植田
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JFE Steel Corp
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Description

本発明は、鋼管用ねじ継手の皮膜形成方法および鋼管用ねじ継手製品に関し、詳しくは、一般に油井やガス井の探査や生産に使用されるチュービングおよびケーシングを包含する油井管すなわちOCTG(oil country tubular goods)、ライザー管、ならびにラインパイプなどの鋼管を接続するためのねじ継手を、耐ゴーリング性とシール性とに優れたものとなしうる鋼管用ねじ継手の皮膜形成方法、および該方法によるねじ継手製品である鋼管用ねじ継手製品に関する。   TECHNICAL FIELD The present invention relates to a method for forming a film of a threaded joint for steel pipes and a threaded joint product for steel pipes. More particularly, the present invention relates to an oil well tubular or OCTG (oil country tubular) that generally includes tubing and casing used for exploration and production of oil wells and gas wells. goods), a method for forming a film of a threaded joint for steel pipes, and a threaded joint for the threaded joints for connecting steel pipes such as riser pipes and line pipes, which have excellent galling resistance and sealability The present invention relates to a steel pipe threaded joint product.

ねじ継手は、油井管など産油産業設備に使用される鋼管の接続に広く使用されている。オイルやガスの探索や生産に使用される鋼管の接続には、従来API(米国石油協会)規格に規定された標準的なねじ継手が典型的には使用されてきた。しかし、近年、原油や天然ガスの井戸は深井戸化が進み、垂直井から水平井や傾斜井等が増えていることから、掘削・生産環境は苛酷化している。また、海洋や極地等々劣悪な環境での井戸の開発が増加していることなどから、耐圧縮性能、耐曲げ性能、外圧シール性能など、ねじ継手への要求性能は多様化している。そのためプレミアムジョイントと呼ばれる高性能の特殊ねじ継手を使用することが増加しており、その性能への要求もますます増加している。   Threaded joints are widely used to connect steel pipes used in oil industry equipment such as oil well pipes. Conventionally, a standard threaded joint specified in the API (American Petroleum Institute) standard has been typically used for connecting steel pipes used for oil and gas exploration and production. However, in recent years, the wells for crude oil and natural gas have been deepened, and the number of vertical wells, horizontal wells, inclined wells, etc. has increased, and the drilling and production environment has become severe. In addition, the demand for screw joints such as compression resistance, bending resistance, and external pressure seal performance has been diversified due to the increasing development of wells in poor environments such as the ocean and polar regions. For this reason, the use of high-performance special threaded joints called premium joints is increasing, and the demands on the performance are also increasing.

プレミアムジョイントは、通常、例えば図1及び図2に示される様に、各パイプの両端部に形成したピン(雄)1と、該ピン1に結合させるボックス(雌)2とを有してなる。ピン1とボックス2には、相互対応部分として、テーパねじ3と、これに連なる非ねじ部9に設けられたシール部(詳しくはメタルタッチシール部)4と、前記非ねじ部9の端部側に設けられたショルダ部(詳しくはトルクショルダ部)5とが形成されている。   The premium joint usually has pins (male) 1 formed at both ends of each pipe and a box (female) 2 coupled to the pins 1 as shown in FIGS. 1 and 2, for example. . The pin 1 and the box 2 have a taper screw 3 as a mutually corresponding portion, a seal portion (specifically, a metal touch seal portion) 4 provided on a non-screw portion 9 connected thereto, and an end portion of the non-screw portion 9. A shoulder portion (specifically, a torque shoulder portion) 5 provided on the side is formed.

テーパねじ3はねじ継手をタイトに固定するために重要であり、シール部4は、ボックス2とピン1とがメタル‐メタル接触することでシール性を確保する役目を担い、ショルダ部5はねじ継手の締付け中にストッパの役目を担うショルダ面となる。尚、図1のように、シール部4が、前記非ねじ部9の一部で対向面と半径方向に金属接触して流体をシールするように設計されたねじ継手は、ラジアルシール型のねじ継手と呼ばれる。前記ラジアルシール型のねじ継手において、シール部4は、図2に示される様に、対応し合うピン1とボックス2の同一尺度図面同士を、ねじ継手の締付完了時の状態を模す形に重ね合わせたときに雌雄双方の非ねじ部9が干渉し合う領域として設計され、該干渉し合う領域の管軸方向長さLsで以てシール接触長Lsが定義される。また、図2の例では、非ねじ部9は雄側の外周面が曲面形状とされ、雌側の内周面がテーパ形状とされている。該テーパ形状を成す円錐の母線が管軸方向7となす角度θで以てシールテーパ角θが定義される。又、ねじ継手を締め付けていったとき雌側シール部内周面と最初に接触する雄側シール部外周面内点で以てシールポイントSPが定義される。そして、前記非ねじ部9の雄側外周面(曲面形状)が管軸方向断面内で成す曲線の、前記シールポイントSP対応位置での、曲率半径Rで以てピン1のシール半径Rが定義される。   The taper screw 3 is important for tightly fixing the threaded joint, and the seal portion 4 plays a role of ensuring sealing performance by the metal-metal contact between the box 2 and the pin 1, and the shoulder portion 5 is a screw The shoulder surface serves as a stopper during tightening of the joint. In addition, as shown in FIG. 1, the threaded joint designed so that the seal portion 4 seals the fluid by making a metal contact with the opposing surface in the radial direction at a part of the non-threaded portion 9 is a radial seal type screw. Called a joint. In the radial seal type threaded joint, as shown in FIG. 2, the seal portion 4 is a shape that simulates the state at the completion of tightening of the threaded joint by using the same scale drawings of the corresponding pin 1 and box 2. Is designed as a region where the male and female non-threaded portions 9 interfere with each other, and the seal contact length Ls is defined by the tube axis direction length Ls of the interfering regions. In the example of FIG. 2, the non-threaded portion 9 has a male-side outer peripheral surface having a curved shape and a female-side inner peripheral surface having a tapered shape. The seal taper angle θ is defined by the angle θ formed by the conical bus forming the taper shape and the tube axis direction 7. Further, when the threaded joint is tightened, the seal point SP is defined by the inner point of the outer peripheral surface of the male seal portion that first contacts the inner peripheral surface of the female side seal portion. Then, the seal radius R of the pin 1 is defined by the curvature radius R of the curve formed by the male outer peripheral surface (curved surface shape) of the non-threaded portion 9 in the cross section in the tube axis direction at the position corresponding to the seal point SP. Is done.

ラジアルシール型のねじ継手ではねじ締付時にシール部4の摺動距離が長くなるためゴーリング(焼き付き)が発生し易くなるという問題がある。
前記問題に対処した従来技術として、油井管用ねじ継手の気密性を確保すると同時に、油井管用ねじ表面に耐ゴーリング性能・耐摩耗性能に優れたリン酸塩系の皮膜を形成すべく、Cr≧0.08質量%、Mo≧0.02質量%を含有するCr−Mo鋼を使用した油井管を対象として、前記皮膜形成をする一連の化成処理の前に予めピン(雄)ねじ又はボックス(雌)ねじのどちらか一方のねじ継手表面に、ショットブラスト等により、平均表面粗さRaが10μm以下の凹凸加工を施すこと(特許文献1参照)が挙げられる。
In the radial seal type threaded joint, there is a problem that goling (seizure) is likely to occur because the sliding distance of the seal portion 4 becomes long when the screw is tightened.
As a conventional technique that addresses the above problems, Cr ≧ 0 in order to ensure the hermeticity of the threaded joint for oil well pipes and to form a phosphate-based film with excellent galling resistance and wear resistance performance on the surface of the oil well pipe threads. For oil well pipes using Cr-Mo steel containing 0.08% by mass and Mo ≧ 0.02% by mass, a pin (male) screw or box (female ) The surface of either one of the screw joints is subjected to uneven processing with an average surface roughness Ra of 10 μm or less by shot blasting or the like (see Patent Document 1).

特開2002−364786号公報JP 2002-364786 A

然しながら、発明者らは、前記従来技術を吟味し、以下の様な課題があることが分った。
即ち、例えば図3に示す様に、リン酸塩系(例えばリン酸Mn)の皮膜は、単体(モード1)では耐摩耗性に乏しく、一方、皮膜の下地材である母材(モード3)は耐ゴーリング性に乏しいのに対し、皮膜と母材との混合領域(モード2)は、リン酸Mnが潤滑性向上に貢献し、母材が耐摩耗性に貢献する為、耐摩耗性と耐ゴーリング性が共に良好であり、前記モード2の厚みが大きいほど優れた耐ゴーリング性が持続する。ところが、前記従来技術により皮膜形成前にショットブラストで母材に表面粗さ(Ra≦10μm)を付与すると、図5に示す様に、点状凸部20が多数分散してねじ継手締付時に点接触状態を成し、斯かる多数分散した点接触箇所の間を縫う形でリークパス21が生じ易くなって、シール性が悪化し易くなる。シール性の悪化を抑制するためにショットブラスト後の表面粗さを小さくした条件では、前記モード2の厚みが薄くなり、耐ゴーリング性が低下してしまう。
However, the inventors examined the prior art and found that there were the following problems.
That is, for example, as shown in FIG. 3, a phosphate-based film (for example, Mn phosphate) has poor wear resistance when used alone (mode 1), while a base material (mode 3) that is the base material of the film. Is poor in galling resistance, but in the mixed region of the film and the base material (mode 2), Mn phosphate contributes to improvement of lubricity, and the base material contributes to wear resistance. Both galling resistance is good, and the larger the thickness of the mode 2, the better the galling resistance is maintained. However, when surface roughness (Ra ≦ 10 μm) is imparted to the base material by shot blasting prior to film formation according to the conventional technique, a large number of dot-like convex portions 20 are dispersed as shown in FIG. A point contact state is formed, and a leak path 21 is likely to be formed by sewing between such a large number of dispersed point contact locations, and the sealing performance is likely to deteriorate. Under the condition that the surface roughness after shot blasting is made small in order to suppress the deterioration of the sealing property, the thickness of the mode 2 becomes thin and the galling resistance is lowered.

つまり、従来技術による耐摩耗性・耐ゴーリング性の改善手法(雄雌いずれか一方へのショットブラストによるRa(≦10μm)付与→リン酸塩系皮膜付与)はシール性の悪化を招来し易いという課題があった。   In other words, the conventional technique for improving wear resistance and galling resistance (Ra (≦ 10 μm) imparted by shot blasting to either male or female → imparting a phosphate-based film) is likely to cause deterioration of the sealing performance. There was a problem.

発明者らは前記課題を解決する為に、十分なシール性を確保しつつ耐摩耗性・耐ゴーリング性を改善する手段を工夫し、本発明を成した。即ち本発明は以下の通りである。
(1) 相対応する雌雄のテーパねじを有してねじ継手を成す雌雄のうちの雄側であるピンと雌側であるボックスとを備え、ねじ継手締付時に、雌雄双方に設けられたショルダ部にて前記ピンと前記ボックスとが軸方向に当接し、且つ前記ショルダ部と前記テーパねじとの間に設けられたシール部にて前記ピンと前記ボックスとが半径方向に金属接触して流体をシールする構造とされた鋼管用ねじ継手の前記ピン又は前記ボックスにリン酸塩系の最表層皮膜処理を施す鋼管用ねじ継手の皮膜形成方法であって、前記最表層皮膜処理をする前に、該最表層皮膜処理をされる側である前記ピン側又は前記ボックス側のシール部に、切削により管軸方向の平均表面粗さRaを1.0μm以上5.0μm以下とする周方向の溝を付与し、或いは更に前記溝の凹凸を潰さない程度の小さな凹凸をショットブラストにて付与し、その後前記最表層皮膜処理を行うことを特徴とする、シール性を確保しつつ耐摩耗性・耐ゴーリング性を改善した、鋼管用ねじ継手の皮膜形成方法。
(2) 前記切削にはポイントカットツールを用い、該ポイントカットツールの先端形状、管半径方向切削量及び管軸方向送りを制御することにより、前記周方向の溝を付与することを特徴とする前記(1)に記載の鋼管用ねじ継手の皮膜形成方法。
(3) 前記金属接触をさせる領域の管軸方向長さであるシール接触長Lsに対し、前記ポイントカットツールの1回転当たりの管軸方向送りをLs/10以下とすることを特徴とする前記(2)に記載の鋼管用ねじ継手の皮膜形成方法。
(4) 相対応してねじ継手を成す雌雄のうちの雄側のテーパねじを有するピンと雌側のテーパねじを有するボックスとを備え、ねじ継手締付時に、雌雄双方に設けられたショルダ部にて前記ピンと前記ボックスとが軸方向に当接し、且つ雌雄双方に設けられたショルダ部とテーパねじ部との間の非ねじ部内のシール部にて前記ピンと前記ボックスとが半径方向に金属接触して流体をシールする構造とされた鋼管用ねじ継手製品であって、前記(1)〜(3)の何れかに記載の鋼管用ねじ継手の皮膜形成方法によりリン酸塩系皮膜を形成されてなり、前記リン酸塩系皮膜とその下地材である母材との界面の管軸方向の平均表面粗さRaが1.0〜5.0μmであることを特徴とする鋼管用ねじ継手製品。
(5) 前記ピン外面内のシール部は管軸方向断面内でピンのシール半径Rが1.0inch以上の円弧形状であり、前記ボックス内面内のシール部は管軸方向断面内でボックスのシールテーパ角θが3.0〜10.0度の直線形状であることを特徴とする前記(4)に記載の鋼管用ねじ継手製品。
In order to solve the above-mentioned problems, the inventors have devised means for improving wear resistance and galling resistance while ensuring sufficient sealing performance, and have made the present invention. That is, the present invention is as follows.
(1) A shoulder portion provided on both males and males at the time of tightening the screw joint, comprising male and female pins and female side boxes of male and female males and females having corresponding male and female taper screws. The pin and the box abut on each other in the axial direction, and the pin and the box make a metal contact in the radial direction to seal the fluid at a seal portion provided between the shoulder portion and the taper screw. a structure has been the pin or film-forming method of a threaded joint for steel pipes subjected to the outermost layer coating treatment of phosphate-based on the box tubular threaded joint, prior to the outermost layer coating process, the most A circumferential groove with an average surface roughness Ra in the tube axis direction of 1.0 μm or more and 5.0 μm or less is given to the seal portion on the pin side or the box side, which is the side subjected to the surface film treatment, by cutting. Or even more Small irregularities so as not to crush roughening at shot blasting, then the and performs outermost layer film treatment, and improved wear resistance, galling resistance while securing sealing performance, a steel pipe A method of forming a film on a threaded joint.
(2) A point cut tool is used for the cutting, and the circumferential groove is provided by controlling a tip shape of the point cut tool, a pipe radial direction cutting amount, and a pipe axis direction feed. The film formation method of the threaded joint for steel pipes as described in said (1).
(3) The tube axis direction feed per rotation of the point cut tool is set to Ls / 10 or less with respect to the seal contact length Ls which is the length in the tube axis direction of the region in which the metal is brought into contact. The film formation method of the threaded joint for steel pipes as described in (2).
(4) A pin having a male taper screw and a box having a female taper screw of males and females forming a threaded joint correspondingly, and a box having a female taper screw are mounted on the shoulder portion provided to both the male and female when tightening the threaded joint. The pin and the box are in contact with each other in the axial direction, and the pin and the box are in metal contact in the radial direction at the seal portion in the non-threaded portion between the shoulder portion and the taper screw portion provided on both the male and female. A steel pipe threaded joint product having a structure for sealing a fluid, wherein a phosphate-based film is formed by the film forming method for a steel pipe threaded joint according to any one of (1) to (3) above. A threaded joint product for steel pipes, characterized in that the average surface roughness Ra in the pipe axis direction at the interface between the phosphate-based film and the base material that is the base material is 1.0 to 5.0 μm.
(5) The seal portion in the outer surface of the pin has an arc shape with a seal radius R of the pin being 1.0 inch or more in the cross section in the tube axis direction, and the seal portion in the inner surface of the box is the seal of the box in the cross section in the tube axis direction. The threaded joint product for steel pipes according to (4) above, which has a linear shape with a taper angle θ of 3.0 to 10.0 degrees.

本発明によれば、前記皮膜処理の前に該皮膜処理をされる側である前記ピン又は前記ボックスのシール部に、切削により管軸方向の平均表面粗さRaを1.0μm以上5.0μm以下とする周方向の溝を付与し、その後前記皮膜処理を行うこととしたから、十分なシール性を確保しつつ耐摩耗性・耐ゴーリング性を向上させることができる。   According to the present invention, an average surface roughness Ra in the tube axis direction is 1.0 μm or more and 5.0 μm by cutting the pin or the seal portion of the box on the side subjected to the film treatment before the film treatment. Since the following circumferential grooves are provided and then the film treatment is performed, it is possible to improve wear resistance and galling resistance while ensuring sufficient sealing performance.

ラジアルシール型のプレミアムジョイントの例を示す断面模式図である。It is a cross-sectional schematic diagram which shows the example of a radial seal type premium joint. 図1のA部拡大図である。It is the A section enlarged view of FIG. リン酸Mn皮膜形成部の断面構造を示す模式図である。It is a schematic diagram which shows the cross-section of a phosphoric acid Mn film formation part. 本発明の実施形態の例を示す断面模式図(a)及び平面模式図(b)である。1A and 1B are a schematic cross-sectional view (a) and a schematic plan view (b) showing an example of an embodiment of the present invention. 従来技術の問題点を示す平面模式図である。It is a plane schematic diagram which shows the problem of a prior art.

本発明において、図1、図2に示した様な、相対応する雌雄のテーパねじ3を有してねじ継手を成す雌雄のうちの雄側であるピン1と雌側であるボックス2とを備え、ねじ継手締付時に、雌雄双方に設けられたショルダ部5にて前記ピン1と前記ボックス2とが軸方向に当接し、且つ前記ショルダ部5と前記テーパねじ3との間に設けられたシール部4にて前記ピン1と前記ボックス2とが半径方向に金属接触して流体をシールする構造とされた鋼管用ねじ継手の前記ピン1又は前記ボックス2にリン酸塩系の皮膜処理を施す点は従来と同様である。   In the present invention, as shown in FIG. 1 and FIG. 2, a male pin 1 and a female box 2 of male and female males and females having corresponding male and female taper screws 3 are formed. The pin 1 and the box 2 are in axial contact with each other at a shoulder portion 5 provided on both the male and female when the threaded joint is tightened, and is provided between the shoulder portion 5 and the taper screw 3. The pin 1 and the box 2 of the threaded joint for steel pipes are structured such that the pin 1 and the box 2 are in metal contact with each other in the radial direction at the seal portion 4 to seal the fluid. The point of applying is the same as in the prior art.

然しながら、本発明では、前記皮膜処理をする前に、該皮膜処理をされる側である前記ピン1側又は前記ボックス2側のシール部4に、例えば図4にボックス2側に施す場合を示す様に、切削により管軸方向の平均表面粗さRaを1.0μm以上5.0μm以下とする周方向の溝8を付与し、その後前記皮膜処理を行う点で従来とは異なる。
前記切削には図4の様にポイントカットツール10を用い、該ポイントカットツール10の先端形状、管半径方向切削量及び管軸方向送りを制御することにより、前記周方向の溝8を付与すると、シール形状加工と同時に表面粗さ作り込みが可能となるため効率的である。
However, in the present invention, before the coating treatment, the case where the coating treatment is applied to the seal portion 4 on the pin 1 side or the box 2 side, for example, on the box 2 side is shown. Similarly, the circumferential groove 8 having an average surface roughness Ra in the tube axis direction of 1.0 μm or more and 5.0 μm or less is provided by cutting, and then the coating treatment is performed.
When the point cut tool 10 is used for the cutting as shown in FIG. 4 and the tip shape of the point cut tool 10, the amount of cutting in the radial direction of the pipe and the feed in the pipe axis direction are controlled, the circumferential groove 8 is provided. Since the surface roughness can be made simultaneously with the sealing shape processing, it is efficient.

この様に切削加工によって周方向の溝8を形成することにより、図4の様に、管軸方向に周期的な凹凸が形成され、切削痕である溝8の溝縁8Aが前記凹凸の凸部を形成し、該溝縁8Aは、その後のリン酸塩系皮膜形成を経てからのねじ継手締付時に、シール接触長Ls部位両端に亘る周面を螺旋状に周回する非常に長い線接触状態を成すから、図5の様なリークパス21は極めて形成され難くなる。   By forming the circumferential grooves 8 in this way by cutting, periodic irregularities are formed in the tube axis direction as shown in FIG. 4, and the groove edges 8A of the grooves 8 that are the cutting traces are irregularities of the irregularities. The groove edge 8A has a very long line contact that spirally circulates around the circumferential surface over both ends of the seal contact length Ls part when the threaded joint is tightened after subsequent formation of the phosphate film. Therefore, the leak path 21 as shown in FIG. 5 is extremely difficult to form.

切削による周方向の溝加工で付与するRaが1.0μm未満であると、前記モード2の厚みが不十分となり十分な耐ゴーリング性が得られない。一方、Raが5.0μm超であると、線接触領域の面積が不足して接触面圧が過大となり摩耗が促進されるため、耐ゴーリング性とシール性が低下する。よって、Raは1.0〜5.0μmとする。
尚、前記切削後の被加工面に更に、前記溝の凹凸を潰さない程度の小さな凹凸をショットブラストにて付与すると、耐ゴーリング性が更に向上するので好ましい。
If the Ra applied by circumferential groove processing by cutting is less than 1.0 μm, the thickness of the mode 2 becomes insufficient and sufficient galling resistance cannot be obtained. On the other hand, when Ra is more than 5.0 μm, the area of the line contact region is insufficient, the contact surface pressure becomes excessive, and wear is promoted, so that the galling resistance and the sealing performance are deteriorated. Therefore, Ra is set to 1.0 to 5.0 μm.
In addition, it is preferable to provide shot-blasting with small unevenness that does not crush the unevenness of the groove on the surface to be processed after the cutting, because galling resistance is further improved.

又、シール性の更なる向上の観点から、前記切削加工では、ポイントカットツール10の1回転当たりの管軸方向送りをLs/10以下にするのが好ましい。
又、本発明の皮膜形成方法の適用による効果の顕現性の点から、対象とされるねじ継手は、図1、図2に示した形態の特殊ねじ継手(プレミアムジョイント)において、シール部4のピン側を、ピンのシール半径Rが1.0inch以上の、円弧形状とされ、ボックス側を、ボックスのシールテーパ角θが3.0〜10.0度の、直線形状とされた特殊ねじ継手である事が好ましい。
Further, from the viewpoint of further improving the sealing performance, in the cutting process, it is preferable that the feed in the tube axis direction per rotation of the point cut tool 10 is Ls / 10 or less.
Moreover, from the point of the obviousness of the effect by application of the film forming method of the present invention, the target threaded joint is a special threaded joint (premium joint) of the form shown in FIGS. A special threaded joint with a pin side that has a circular arc shape with a pin seal radius R of 1.0 inch or more, and a box side that has a linear shape with a seal taper angle θ of the box of 3.0 to 10.0 degrees. It is preferable that

外径9-5/8inch×肉厚0.545inchの炭素鋼P110(ISO11960にて規定)の継目無管材に複数の実験水準で図1、図2の形態の特殊ねじ加工を施したピン及びそれに対応するボックスを用いてISO13679に記載のMake&Break(略してM&B)テストを実施し耐ゴーリング性の評価を行った。各水準とも、ボックスのシール部を対象として、ポイントカットツールで螺旋状に切削して周方向の溝を形成し、或いは更にショットブラストを施して、表面粗さを付与した後、リン酸Mn処理を施してリン酸Mn皮膜を形成した。実験条件及び実験結果を表1に示す。表1より、リン酸Mn処理前のボックスのRaを1.0μm以上とする事により、M&B4回合格が達成され、優れた耐ゴーリング性を示すことが示された。   Pins with special screw machining in the form of Fig. 1 and Fig. 2 on the seamless pipe material of carbon steel P110 (specified in ISO11960) of outer diameter 9-5 / 8inch x wall thickness 0.545inch at multiple experimental levels A make & break (abbreviated as M & B) test described in ISO 13679 was performed using the corresponding box to evaluate galling resistance. For each level, for the seal part of the box, cut it in a spiral shape with a point cut tool to form a circumferential groove, or apply shot blasting to give surface roughness, and then treat with Mn phosphate To form a Mn phosphate coating. Table 1 shows experimental conditions and experimental results. From Table 1, it was shown that by passing Ra of the box before the treatment with Mn phosphate to 1.0 μm or more, M & B was passed 4 times and excellent galling resistance was exhibited.

次に、ISO13679に記載のシリーズAテストを実施しシール性の評価を行った。その結果を表1に示す。表1より、耐ゴーリング性向上の為にショットブラストにてRaを高くした条件ではリークが発生した。一方で、切削にてRaを高くした条件でも、リン酸Mn処理前のボックスのRaを高くし過ぎた場合はリークが発生した。これに対して本発明例は優れたシール性を有することが明らかとなった。特に、シール部の接触長Lsに対するポイントカットツールの送り量の割合を1/10以下とするとともに、ピンのシール半径Rを1.0inch以上とすることにより、シリーズAテストにおいてより厳しい条件となる高圧縮率条件下でもシール性が確保できることが示された。   Next, the series A test described in ISO 13679 was performed to evaluate the sealing performance. The results are shown in Table 1. From Table 1, leakage occurred under the condition that Ra was increased by shot blasting to improve galling resistance. On the other hand, even when Ra was increased by cutting, leakage occurred when Ra of the box before the Mn phosphate treatment was excessively increased. On the other hand, it became clear that the examples of the present invention have excellent sealing properties. In particular, the ratio of the feed amount of the point cut tool to the contact length Ls of the seal portion is set to 1/10 or less, and the seal radius R of the pin is set to 1.0 inch or more. It was shown that sealability can be secured even under high compressibility conditions.

Figure 0005910284
Figure 0005910284

1 ピン
2 ボックス
3 テーパねじ
4 シール部
5 ショルダ部
6 管軸
7 管軸方向
8 周方向の溝
8A 溝縁
9 非ねじ部
10 ポイントカットツール
20 点状凸部
21 リークパス
Ls:シール部の接触長
θ:シールテーパ角
R:ピンのシール半径
SP:シールポイント
1 pin 2 box 3 taper screw 4 seal part 5 shoulder part 6 tube axis 7 pipe axis direction 8 circumferential groove 8A groove edge 9 non-threaded part 10 point cut tool 20 point-like convex part 21 leak path
Ls: Seal contact length θ: Seal taper angle R: Pin seal radius
SP: Seal point

Claims (5)

相対応する雌雄のテーパねじを有してねじ継手を成す雌雄のうちの雄側であるピンと雌側であるボックスとを備え、ねじ継手締付時に、雌雄双方に設けられたショルダ部にて前記ピンと前記ボックスとが軸方向に当接し、且つ前記ショルダ部と前記テーパねじとの間に設けられたシール部にて前記ピンと前記ボックスとが半径方向に金属接触して流体をシールする構造とされた鋼管用ねじ継手の前記ピン又は前記ボックスにリン酸塩系の最表層皮膜処理を施す鋼管用ねじ継手の皮膜形成方法であって、前記最表層皮膜処理をする前に、該最表層皮膜処理をされる側である前記ピン側又は前記ボックス側のシール部に、切削により管軸方向の平均表面粗さRaを1.0μm以上5.0μm以下とする周方向の溝を付与し、或いは更に前記溝の凹凸を潰さない程度の小さな凹凸をショットブラストにて付与し、その後前記最表層皮膜処理を行うことを特徴とする、シール性を確保しつつ耐摩耗性・耐ゴーリング性を改善した、鋼管用ねじ継手の皮膜形成方法。
A male and female pin having male and female taper screws having corresponding tapers and a box on the female side are provided, and at the time of tightening the screw joint, The pin and the box are in contact with each other in the axial direction, and the pin and the box are in metal contact in the radial direction to seal the fluid at a seal portion provided between the shoulder portion and the taper screw. and the pin or the box tubular threaded joint comprising a film-forming method for a threaded joint for steel pipes subjected to the outermost layer coating treatment of phosphate-based, said before the outermost layer film treatment, the outermost layer film treatment A circumferential groove that gives an average surface roughness Ra in the tube axis direction of 1.0 μm or more to 5.0 μm or less by cutting is given to the seal portion on the pin side or the box side, which is the side to be processed, or further Unevenness of the groove Grant by small irregularities shot blasting as not crushed, then the and performs outermost layer film treatment, and improved wear resistance, galling resistance while securing sealing performance, tubular threaded joint Film forming method.
前記切削にはポイントカットツールを用い、該ポイントカットツールの先端形状、管半径方向切削量及び管軸方向送りを制御することにより、前記周方向の溝を付与することを特徴とする請求項1に記載の鋼管用ねじ継手の皮膜形成方法。   The point cutting tool is used for the cutting, and the circumferential groove is provided by controlling a tip shape of the point cutting tool, a pipe radial direction cutting amount, and a pipe axial direction feed. The film formation method of the threaded joint for steel pipes as described in any one of. 前記金属接触をさせる領域の管軸方向長さであるシール接触長Lsに対し、前記ポイントカットツールの1回転当たりの管軸方向送りをLs/10以下とすることを特徴とする請求項2に記載の鋼管用ねじ継手の皮膜形成方法。   The tube axis direction feed per one rotation of the point cut tool is set to Ls / 10 or less with respect to a seal contact length Ls which is a length in the tube axis direction of the region in which the metal is contacted. The film formation method of the threaded joint for steel pipes of description. 相対応してねじ継手を成す雌雄のうちの雄側のテーパねじを有するピンと雌側のテーパねじを有するボックスとを備え、ねじ継手締付時に、雌雄双方に設けられたショルダ部にて前記ピンと前記ボックスとが軸方向に当接し、且つ雌雄双方に設けられたショルダ部とテーパねじ部との間の非ねじ部内のシール部にて前記ピンと前記ボックスとが半径方向に金属接触して流体をシールする構造とされた鋼管用ねじ継手製品であって、請求項1〜3の何れかに記載の鋼管用ねじ継手の皮膜形成方法によりリン酸塩系皮膜を形成されてなり、前記リン酸塩系皮膜とその下地材である母材との界面の管軸方向の平均表面粗さRaが1.0〜5.0μmであることを特徴とする鋼管用ねじ継手製品。   A pin having a male side taper screw and a box having a female side taper screw of a male and female that form a screw joint correspondingly, and a box provided with both male and female when tightening the screw joint, The box and the box are in contact with each other in the axial direction, and the pin and the box are in metal contact with each other in the radial direction at the seal portion in the non-threaded portion between the shoulder portion and the taper screw portion provided on both the male and female. A threaded joint product for steel pipes having a structure to be sealed, wherein a phosphate-based film is formed by the film forming method for a threaded joint for steel pipes according to any one of claims 1 to 3, and the phosphate A threaded joint product for steel pipes, characterized in that the average surface roughness Ra in the pipe axis direction at the interface between the base film and the base material which is the base material is 1.0 to 5.0 μm. 前記ピン外面内のシール部は管軸方向断面内でピンのシール半径Rが1.0inch以上の円弧形状であり、前記ボックス内面内のシール部は管軸方向断面内でボックスのシールテーパ角θが3.0〜10.0度の直線形状であることを特徴とする請求項4に記載の鋼管用ねじ継手製品。   The seal portion in the outer surface of the pin has an arc shape with a pin seal radius R of 1.0 inch or more in the cross section in the tube axis direction, and the seal portion in the inner surface of the box has a seal taper angle θ of the box in the cross section in the tube axis direction. 5 is a linear shape of 3.0 to 10.0 degrees, the threaded joint product for steel pipes according to claim 4.
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