JP5813548B2 - さび止め油組成物 - Google Patents
さび止め油組成物 Download PDFInfo
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- JP5813548B2 JP5813548B2 JP2012067772A JP2012067772A JP5813548B2 JP 5813548 B2 JP5813548 B2 JP 5813548B2 JP 2012067772 A JP2012067772 A JP 2012067772A JP 2012067772 A JP2012067772 A JP 2012067772A JP 5813548 B2 JP5813548 B2 JP 5813548B2
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- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 title claims description 139
- 239000000203 mixture Substances 0.000 title claims description 96
- 230000002265 prevention Effects 0.000 title claims description 72
- -1 Fatty acid amine salts Chemical class 0.000 claims description 249
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- 150000001412 amines Chemical class 0.000 claims description 97
- 150000002148 esters Chemical class 0.000 claims description 46
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 41
- 239000000194 fatty acid Substances 0.000 claims description 41
- 229930195729 fatty acid Natural products 0.000 claims description 41
- 239000002480 mineral oil Substances 0.000 claims description 38
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- 230000003449 preventive effect Effects 0.000 claims description 36
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 35
- 239000001993 wax Substances 0.000 claims description 26
- 150000003839 salts Chemical class 0.000 claims description 23
- 238000012360 testing method Methods 0.000 claims description 19
- 150000001735 carboxylic acids Chemical class 0.000 claims description 16
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 230000007935 neutral effect Effects 0.000 claims description 14
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- 239000007921 spray Substances 0.000 claims description 10
- 125000003118 aryl group Chemical group 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 6
- 150000001639 boron compounds Chemical class 0.000 claims description 5
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- 241000255925 Diptera Species 0.000 claims description 2
- 150000001734 carboxylic acid salts Chemical class 0.000 claims description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 86
- 125000000217 alkyl group Chemical group 0.000 description 79
- 125000004432 carbon atom Chemical group C* 0.000 description 68
- 239000002199 base oil Substances 0.000 description 45
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 45
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- 230000036961 partial effect Effects 0.000 description 32
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- 229910052784 alkaline earth metal Inorganic materials 0.000 description 27
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- 125000003342 alkenyl group Chemical group 0.000 description 25
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- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 24
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- 239000002585 base Substances 0.000 description 17
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical class C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 description 17
- 150000001342 alkaline earth metals Chemical class 0.000 description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 16
- 150000001340 alkali metals Chemical class 0.000 description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 14
- 150000001298 alcohols Chemical class 0.000 description 14
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- 239000003112 inhibitor Substances 0.000 description 12
- 229940039717 lanolin Drugs 0.000 description 12
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- 235000019271 petrolatum Nutrition 0.000 description 12
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 12
- 235000019809 paraffin wax Nutrition 0.000 description 11
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 11
- 239000002994 raw material Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 10
- 229910052788 barium Inorganic materials 0.000 description 9
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 9
- 239000011575 calcium Substances 0.000 description 9
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 9
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- 229910052791 calcium Inorganic materials 0.000 description 8
- 239000000460 chlorine Substances 0.000 description 8
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- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 108010077895 Sarcosine Proteins 0.000 description 7
- 229940043230 sarcosine Drugs 0.000 description 7
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 6
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 6
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 6
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 6
- WWZKQHOCKIZLMA-UHFFFAOYSA-N Caprylic acid Natural products CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 239000005642 Oleic acid Substances 0.000 description 6
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 6
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- 125000002947 alkylene group Chemical group 0.000 description 6
- 150000001721 carbon Chemical group 0.000 description 6
- 239000000539 dimer Substances 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 239000003925 fat Substances 0.000 description 6
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 6
- 239000011630 iodine Substances 0.000 description 6
- 229910052740 iodine Inorganic materials 0.000 description 6
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 6
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 6
- 239000003208 petroleum Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 235000011044 succinic acid Nutrition 0.000 description 6
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 6
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 5
- 150000003973 alkyl amines Chemical class 0.000 description 5
- 125000002843 carboxylic acid group Chemical group 0.000 description 5
- 239000000470 constituent Substances 0.000 description 5
- 230000007062 hydrolysis Effects 0.000 description 5
- 238000006460 hydrolysis reaction Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 5
- 239000011591 potassium Substances 0.000 description 5
- 229910052700 potassium Inorganic materials 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- 239000001384 succinic acid Substances 0.000 description 5
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 5
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 4
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 4
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 4
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 4
- 241000223259 Trichoderma Species 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 235000015278 beef Nutrition 0.000 description 4
- 150000007942 carboxylates Chemical class 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 125000000753 cycloalkyl group Chemical group 0.000 description 4
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 4
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 description 4
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 4
- CKDDRHZIAZRDBW-UHFFFAOYSA-N henicosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCC(O)=O CKDDRHZIAZRDBW-UHFFFAOYSA-N 0.000 description 4
- KEMQGTRYUADPNZ-UHFFFAOYSA-N heptadecanoic acid Chemical compound CCCCCCCCCCCCCCCCC(O)=O KEMQGTRYUADPNZ-UHFFFAOYSA-N 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 229910052749 magnesium Inorganic materials 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 4
- ISYWECDDZWTKFF-UHFFFAOYSA-N nonadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCCC(O)=O ISYWECDDZWTKFF-UHFFFAOYSA-N 0.000 description 4
- FBUKVWPVBMHYJY-UHFFFAOYSA-N nonanoic acid Chemical compound CCCCCCCCC(O)=O FBUKVWPVBMHYJY-UHFFFAOYSA-N 0.000 description 4
- DPBLXKKOBLCELK-UHFFFAOYSA-N pentan-1-amine Chemical compound CCCCCN DPBLXKKOBLCELK-UHFFFAOYSA-N 0.000 description 4
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- WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 description 4
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- XEZVDURJDFGERA-UHFFFAOYSA-N tricosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCC(O)=O XEZVDURJDFGERA-UHFFFAOYSA-N 0.000 description 4
- SZHOJFHSIKHZHA-UHFFFAOYSA-N tridecanoic acid Chemical compound CCCCCCCCCCCCC(O)=O SZHOJFHSIKHZHA-UHFFFAOYSA-N 0.000 description 4
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- NJVZWCOTNSEBGI-UHFFFAOYSA-N 2-(sulfonylamino)ethanamine Chemical compound NCCN=S(=O)=O NJVZWCOTNSEBGI-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
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- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
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- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 description 3
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical class OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 3
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- 238000006243 chemical reaction Methods 0.000 description 3
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- 125000003493 decenyl group Chemical group [H]C([*])=C([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
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- 229910001385 heavy metal Inorganic materials 0.000 description 3
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- 125000006038 hexenyl group Chemical group 0.000 description 3
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 239000011133 lead Substances 0.000 description 3
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 125000001624 naphthyl group Chemical group 0.000 description 3
- 125000005187 nonenyl group Chemical group C(=CCCCCCCC)* 0.000 description 3
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 125000004365 octenyl group Chemical group C(=CCCCCCC)* 0.000 description 3
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
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- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 3
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- BITHHVVYSMSWAG-KTKRTIGZSA-N (11Z)-icos-11-enoic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCCC(O)=O BITHHVVYSMSWAG-KTKRTIGZSA-N 0.000 description 2
- GEHPRJRWZDWFBJ-FOCLMDBBSA-N (2E)-2-heptadecenoic acid Chemical compound CCCCCCCCCCCCCC\C=C\C(O)=O GEHPRJRWZDWFBJ-FOCLMDBBSA-N 0.000 description 2
- NIONDZDPPYHYKY-SNAWJCMRSA-N (2E)-hexenoic acid Chemical compound CCC\C=C\C(O)=O NIONDZDPPYHYKY-SNAWJCMRSA-N 0.000 description 2
- ULNRTPCFRBIMKL-GHVJWSGMSA-N (e)-2-tetracosenoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCC\C=C\C(O)=O ULNRTPCFRBIMKL-GHVJWSGMSA-N 0.000 description 2
- ATNNLHXCRAAGJS-QZQOTICOSA-N (e)-docos-2-enoic acid Chemical compound CCCCCCCCCCCCCCCCCCC\C=C\C(O)=O ATNNLHXCRAAGJS-QZQOTICOSA-N 0.000 description 2
- OTJFQRMIRKXXRS-UHFFFAOYSA-N (hydroxymethylamino)methanol Chemical compound OCNCO OTJFQRMIRKXXRS-UHFFFAOYSA-N 0.000 description 2
- ARXKVVRQIIOZGF-UHFFFAOYSA-N 1,2,4-butanetriol Chemical compound OCCC(O)CO ARXKVVRQIIOZGF-UHFFFAOYSA-N 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- KQIXMZWXFFHRAQ-UHFFFAOYSA-N 1-(2-hydroxybutylamino)butan-2-ol Chemical compound CCC(O)CNCC(O)CC KQIXMZWXFFHRAQ-UHFFFAOYSA-N 0.000 description 2
- FJLUATLTXUNBOT-UHFFFAOYSA-N 1-Hexadecylamine Chemical compound CCCCCCCCCCCCCCCCN FJLUATLTXUNBOT-UHFFFAOYSA-N 0.000 description 2
- BFIAIMMAHAIVFT-UHFFFAOYSA-N 1-[bis(2-hydroxybutyl)amino]butan-2-ol Chemical compound CCC(O)CN(CC(O)CC)CC(O)CC BFIAIMMAHAIVFT-UHFFFAOYSA-N 0.000 description 2
- KODLUXHSIZOKTG-UHFFFAOYSA-N 1-aminobutan-2-ol Chemical compound CCC(O)CN KODLUXHSIZOKTG-UHFFFAOYSA-N 0.000 description 2
- JPZYXGPCHFZBHO-UHFFFAOYSA-N 1-aminopentadecane Chemical compound CCCCCCCCCCCCCCCN JPZYXGPCHFZBHO-UHFFFAOYSA-N 0.000 description 2
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- YIYBQIKDCADOSF-ONEGZZNKSA-N trans-pent-2-enoic acid Chemical compound CC\C=C\C(O)=O YIYBQIKDCADOSF-ONEGZZNKSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 description 1
- 125000002469 tricosyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- YFTHZRPMJXBUME-UHFFFAOYSA-N tripropylamine Chemical compound CCCN(CCC)CCC YFTHZRPMJXBUME-UHFFFAOYSA-N 0.000 description 1
- ZMKXDWIJLNQLPW-UHFFFAOYSA-N undec-1-en-1-amine Chemical compound CCCCCCCCCC=CN ZMKXDWIJLNQLPW-UHFFFAOYSA-N 0.000 description 1
- QFKMMXYLAPZKIB-UHFFFAOYSA-N undecan-1-amine Chemical compound CCCCCCCCCCCN QFKMMXYLAPZKIB-UHFFFAOYSA-N 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
Classifications
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- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
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- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
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- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/02—Petroleum fractions
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/26—Carboxylic acids; Salts thereof
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/26—Carboxylic acids; Salts thereof
- C10M129/28—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M129/38—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 8 or more carbon atoms
- C10M129/40—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 8 or more carbon atoms monocarboxylic
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
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- C10M129/68—Esters
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- C10M133/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen
- C10M133/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen having a carbon chain of less than 30 atoms
- C10M133/04—Amines, e.g. polyalkylene polyamines; Quaternary amines
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- C10M133/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen
- C10M133/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen having a carbon chain of less than 30 atoms
- C10M133/16—Amides; Imides
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- C10M135/08—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium containing a sulfur-to-oxygen bond
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- C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
- C10M159/02—Natural products
- C10M159/06—Waxes, e.g. ozocerite, ceresine, petrolatum, slack-wax
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- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
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- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
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- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
- C23F11/14—Nitrogen-containing compounds
- C23F11/141—Amines; Quaternary ammonium compounds
- C23F11/143—Salts of amines
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- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/12—Oxidised hydrocarbons, i.e. oxidised subsequent to macromolecular formation
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
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- C10M2207/287—Partial esters
- C10M2207/289—Partial esters containing free hydroxy groups
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Lubricants (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Description
40℃における動粘度が6mm2/s以下の鉱油である第1の鉱油と、
40℃における動粘度が250mm2/s以上の鉱油である第2の鉱油と、
脂肪酸アミン塩と、
エステルと、
ザルコシン型化合物、ノニオン系界面活性剤、スルホン酸塩、アミン、カルボン酸、カルボン酸塩、パラフィンワックス、酸化ワックス塩及びホウ素化合物からなる群から選ばれる1種以上のさび止め剤と、
を含有し、
前記脂肪酸アミン塩の含有量が、組成物全量基準で2質量%以上10質量%以下であり、
前記エステルの含有量が、組成物全量基準で4質量%以上20質量%以下である。
(A−1)40℃における動粘度が6mm2/s以下の鉱油(第1の鉱油)と、
(A−2)40℃における動粘度が250mm2/s以上の鉱油(第2の鉱油)と、
(B)脂肪酸アミン塩と、
(C)エステルと、
(D)ザルコシン型化合物、ノニオン系界面活性剤、スルホン酸塩、アミン、カルボン酸、脂肪酸アミン塩、カルボン酸塩、パラフィンワックス、酸化ワックス塩及びホウ素化合物からなる群から選ばれる1種以上のさび止め剤と、
を含有する。
を含む)等のN−アルケニルエチレンジアミン;N−アルキルジエチレントリアミン、N−アルケニルジエチレントリアミン、N−アルキルトリエチレンテトラミン、N−アルケニルトリエチレンテトラミン、N−アルキルテトラエチレンペンタミン、N−アルケニルテトラエチレンペンタミン、N−アルキルペンタエチレンヘキサミン、N−アルケニルペンタエチレンヘキサミン、N−アルキルプロピレンジアミン、N−アルケニルプロピレンジアミン、N−アルキルジプロピレントリアミン、N−アルケニルジプロピレントリアミン、N−アルキルトリプロピレンテトラミン、N−アルケニルトリプロピレンテトラミン、N−アルキルテトラプロピレンペンタミン、N−アルケニルテトラプロピレンペンタミン、N−アルキルペンタプロピレンヘキサミン、N−アルケニルペンタプロピレンヘキサミン、N−アルキルブチレンジアミン、N−アルケニルブチレンジアミン、N−アルキルジブチレントリアミン、N−アルケニルジブチレントリアミン、N−アルキルトリブチレンテトラミン、N−アルケニルトリブチレンテトラミン、N−アルキルテトラブチレンペンタミン、N−アルケニルテトラブチレンペンタミン、N−アルキルペンタブチレンヘキサミン、N−アルケニルペンタブチレンヘキサミン等のN−アルキルまたはN−アルケニルアルキレンポリアミン;等が挙げられる。また、このポリアミンには牛脂ポリアミン等に代表されるような、油脂から誘導されるポリアミンも含まれる。上記アルカノールアミンとしては、具体的には例えば、モノメタノールアミン、ジメタノールアミン、トリメタノールアミン、モノエタノールアミン、ジエタノールアミン、トリエタノールアミン、モノ(n−プロパノール)アミン、ジ(n−プロパノール)アミン、トリ(n−プロパノール)アミン、モノイソプロパノールアミン、ジイソプロパノールアミン、トリイソプロパノールアミン、モノブタノールアミン(全ての異性体を含む)、ジブタノールアミン(全ての異性体を含む)、トリブタノールアミン(全ての異性体を含む)、モノペンタノールアミン(全ての異性体を含む)、ジペンタノールアミン(全ての異性体を含む)、トリペンタノールアミン(全ての異性体を含む)、モノヘキサノールアミン(全ての異性体を含む)、ジヘキサノールアミン(全ての異性体を含む)、モノヘプタノールアミン(全ての異性体を含む)、ジヘプタノールアミン(全ての異性体を含む)、モノオクタノールアミン(全ての異性体を含む)、モノノナノールアミン(全ての異性体を含む)、モノデカノールアミン(全ての異性体を含む)、モノウンデカノールアミン(全ての異性体を含む)、モノドデカノールアミン(全ての異性体を含む)、モノトリデカノールアミン(全ての異性体を含む)、モノテトラデカノールアミン(全ての異性体を含む)、モノペンタデカノールアミン(全ての異性体を含む)、モノヘキサデカノールアミン(全ての異性体を含む)、ジエチルモノエタノールアミン、ジエチルモノプロパノールアミン(全ての異性体を含む)、ジエチルモノブタノールアミン(全ての異性体を含む)、ジエチルモノペンタノールアミン(全ての異性体を含む)、ジプロピルモノエタノールアミン(全ての異性体を含む)、ジプロピルモノプロパノールアミン(全ての異性体を含む)、ジプロピルモノブタノールアミン(全ての異性体を含む)、ジプロピルモノペンタノールアミン(全ての異性体を含む)、ジブチルモノエタノールアミン(全ての異性体を含む)、ジブチルモノプロパノールアミン(全ての異性体を含む)、ジブチルモノブタノールアミン(全ての異性体を含む)、ジブチルモノペンタノールアミン(全ての異性体を含む)、モノエチルジエタノールアミン、モノエチルジプロパノールアミン(全ての異性体を含む)、モノエチルジブタノールアミン(全ての異性体を含む)、モノエチルジペンタノールアミン(全ての異性体を含む)、モノプロピルジエタノールアミン(全ての異性体を含む)、モノプロピルジプロパノールアミン(全ての異性体を含む)、モノプロピルジブタノールアミン(全ての異性体を含む)、モノプロピルジペンタノールアミン(全ての異性体を含む)、モノブチルジエタノールアミン(全ての異性体を含む)、モノブチルジプロパノールアミン(全ての異性体を含む)、モノブチルジブタノールアミン(全ての異性体を含む)、モノブチルジペンタノールアミン(全ての異性体を含む)等が挙げられる。上記したアミンの中でも、冷凍システムへの影響が少ないことから、モノアミンが好ましく、モノアミンの中でも特にアルキルアミン、アルキル基及びアルケニル基を有するモノアミン、アルキル基及びシクロアルキル基を有するモノアミン、シクロアルキルアミン並びにアルキルシクロアルキルアミンがより好ましい。また、耐ステイン性の点から、アミン分子中の合計炭素数が3以上のアミンが好ましく、合計炭素数が5以上のアミンがより好ましい。
(C−1)多価アルコールの部分エステルとは、多価アルコール中の水酸基の少なくとも1個以上がエステル化されておらず水酸基のままで残っているエステルであり、その原料である多価アルコールとしては任意のものが使用可能であるが、分子中の水酸基の数は好ましくは2〜10、より好ましくは3〜6であり、且つ炭素数が2〜20、より好ましくは3〜10である多価アルコールが好適に使用される。これらの多価アルコールの中でも、グリセリン、トリメチロールエタン、トリメチロールプロパン、ペンタエリスリトールおよびソルビタンからなる群より選ばれる少なくとも1種の多価アルコールを用いることが好ましく、ペンタエリスリトールを用いることがより好ましい。
式中、R1は水素原子、炭素数1〜38のアルキル基または炭素数2〜38のアルケニ
ル基を示す。またR2は、炭素数1〜38のアルキレン基または炭素数2〜38のアルケ
ニレン基を示す。
、プロピル基、ブチル基、ペンチル基、ヘキシル基、ヘプチル基、オクチル基、ノニル基、デシル基、ウンデシル基、ドデシル基、トリデシル基、テトラデシル基、ペンタデシル基、ヘキサデシル基、ヘプタデシル基、オクタデシル基、ノナデシル基、イコシル基、ヘンイコシル基、ドコシル基、トリコシル基、テトラコシル基、ペンタコシル基、ヘキサコシル基、ヘプタコシル基、オクタコシル基、ノナコシル基、トリアコンチル基、ヘントリアコンチル基、ドトリアコンチル基、トリトリアコンチル基、テトラトリアコンチル基、ペンタトリアコンチル基、ヘキサトリアコンチル基、ヘプタトリアコンチル基、オクタトリアコンチル基等のアルキル基;エテニル基(ビニル基)、プロペニル基(アリル基)、ブテニル基、ペンテニル基、ヘキセニル基、ヘプテニル基、オクテニル基、ノネニル基、デセニル基、ウンデセニル基、ドデセニル基、トリデセニル基、テトラデセニル基、ペンタデセニル基、ヘキサデセニル基、ヘプタデセニル基、オクタデセニル基、ノナデセニル基、イコセニル基、ヘンイコセニル基、ドコセニル基、トリコセニル基、テトラコセニル基、ペンタコセニル基、ヘキサコセニル基、ヘプタコセニル基、オクタコセニル基、ノナコセニル基、トリアコンテニル基、ヘントリアコンテニル基、ドトリアコンテニル基、トリトリアコンテニル基、テトラトリアコンテニル基、ペンタトリアコンテニル基、ヘキサトリアコンテニル基、ヘプタトリアコンテニル基、オクタトリアコンテニル基等のアルケニル基が挙げられ、これらの全ての異性体も挙げられる。
(i)多価アルコールとヒドロキシカルボン酸との、またはヒドロキシカルボン酸と水酸基を有さない飽和カルボン酸との混合物との部分エステルと、多価アルコールと水酸基を有さない不飽和カルボン酸との、または水酸基を有さない不飽和カルボン酸と水酸基を有さない飽和カルボン酸との混合物との部分エステルとを、両者の混合物におけるカルボン酸組成が上記条件を満たすように混合する方法。
(ii)得られる部分エステルのカルボン酸組成が上記条件を満たすように、水酸基を有するカルボン酸と水酸基を有さない不飽和カルボン酸とを混合し、あるいは水酸基を有さない飽和カルボン酸を更に混合し、当該カルボン酸混合物と多価アルコールとの部分エステル化反応を行う方法。
(iii)ヒドロキシカルボン酸と水酸基を有さない不飽和カルボン酸との混合物との、あるいはこれらのカルボン酸と水酸基を有さない飽和カルボン酸との混合物との部分エステルに、カルボン酸組成が上記条件を満たすように、多価アルコールとヒドロキシカルボン酸との、もしくはヒドロキシカルボン酸と水酸基を有さない飽和カルボン酸との混合物との部分エステル、または多価アルコールと水酸基を有さない不飽和カルボン酸との、もしくは水酸基を有さない不飽和カルボン酸と水酸基を有さない飽和カルボン酸との混合物との部分エステルを混合する方法。
R3−CO−NR4−(CH2)n−COOX (3)
(式中、R3は炭素数6〜30のアルキル基又は炭素数6〜30のアルケニル基、R4は炭素数1〜4のアルキル基、Xは水素原子、炭素数1〜30のアルキル基又は炭素数1〜30のアルケニル基、nは1〜4の整数を示す。)
[R3−CO−NR4−(CH2)n−COO]mY (4)
(式中、R3は炭素数6〜30のアルキル基又は炭素数6〜30のアルケニル基、R4は炭素数1〜4のアルキル基、Yはアルカリ金属又はアルカリ土類金属、nは1〜4の整数、mはYがアルカリ金属の場合は1、アルカリ土類金属の場合は2を示す。)
[R3−CO−NR4−(CH2)n−COO]m−Z−(OH)m' (5)
(式中、R3は炭素数6〜30のアルキル基又は炭素数6〜30のアルケニル基、R4は炭素数1〜4のアルキル基、Zは2価以上の多価アルコールの水酸基を除いた残基、mは1以上の整数、m’は0以上の整数、m+m’はZの価数、nは1〜4の整数を示す。)
点から、炭素数4以下のアルキル基であることが必要であり、炭素数3以下であることが好ましく、炭素数2以下であることがより好ましい。
スルホン酸塩を構成するアルカリ金属としては、ナトリウム、カリウム等が挙げられる。また、アルカリ土類金属としては、マグネシウム、カルシウム、バリウム等が挙げられる。中でも、アルカリ金属およびアルカリ土類金属としては、ナトリウム、カリウム、カルシウム及びバリウムが好ましく、カルシウムが特に好ましい。
ノビニルアミン、ジビニルアミン、トリビニルアミン、モノプロペニルアミン、ジプロペニルアミン、トリプロペニルアミン、モノブテニルアミン、ジブテニルアミン、トリブテニルアミン、モノペンテニルアミン、ジペンテニルアミン、トリペンテニルアミン、モノヘキセニルアミン、ジヘキセニルアミン、モノヘプテニルアミン、ジヘプテニルアミン、モノオクテニルアミン、ジオクテニルアミン、モノノネニルアミン、モノデセニルアミン、モノウンデセニルアミン、モノドデセニルアミン、モノトリデセニルアミン、モノテトラデセニルアミン、モノペンタデセニルアミン、モノヘキサデセニルアミン、モノヘプタデセニルアミン、モノオクタデセニルアミン、モノノナデセニルアミン、モノイコセニルアミン、モノヘンイコセニルアミン、モノドコセニルアミン、モノトリコセニルアミン等のアルケニルアミン;
ジメチル(ビニル)アミン、ジメチル(プロペニル)アミン、ジメチル(ブテニル)アミン、ジメチル(ペンテニル)アミン、ジメチル(ヘキセニル)アミン、ジメチル(ヘプテニル)アミン、ジメチル(オクテニル)アミン、ジメチル(ノネニル)アミン、ジメチル(デセニル)アミン、ジメチル(ウンデセニル)アミン、ジメチル(ドデセニル)アミン、ジメチル(トリデセニル)アミン、ジメチル(テトラデセニル)アミン、ジメチル(ペンタデセニル)アミン、ジメチル(ヘキサデセニル)アミン、ジメチル(ヘプタデセニル)アミン、ジメチル(オクタデセニル)アミン、ジメチル(ノナデセニル)アミン、ジメチル(イコセニル)アミン、ジメチル(ヘンイコセニル)アミン、ジメチル(トリコセニル)アミン等のアルキル基およびアルケニル基を有するモノアミン;
モノベンジルアミン、(1−フェネチル)アミン、(2−フェネチル)アミン(別名:モノフェネチルアミン)、ジベンジルアミン、ビス(1−フェネチル)アミン、ビス(2−フェネチル)アミン(別名:ジフェネチルアミン)等の芳香族置換アルキルアミン;モノシクロペンチルアミン、ジシクロペンチルアミン、トリシクロペンチルアミン、モノシクロヘキシルアミン、ジシクロヘキシルアミン、モノシクロヘプチルアミン、ジシクロヘプチルアミン等の炭素数5〜16のシクロアルキルアミン;ジメチル(シクロペンチル)アミン、ジメチル(シクロヘキシル)アミン、ジメチル(シクロヘプチル)アミン等のアルキル基およびシクロアルキル基を有するモノアミン;(メチルシクロペンチル)アミン、ビス(メチルシクロペンチル)アミン、(ジメチルシクロペンチル)アミン、ビス(ジメチルシクロペンチル)アミン、(エチルシクロペンチル)アミン、ビス(エチルシクロペンチル)アミン、(メチルエチルシクロペンチル)アミン、ビス(メチルエチルシクロペンチル)アミン、(ジエチルシクロペンチル)アミン、(メチルシクロヘキシル)アミン、ビス(メチルシクロヘキシル)アミン、(ジメチルシクロヘキシル)アミン、ビス(ジメチルシクロヘキシル)アミン、(エチルシクロヘキシル)アミン、ビス(エチルシクロヘキシル)アミン、(メチルエチルシクロヘキシル)アミン、(ジエチルシクロヘキシル)アミン、(メチルシクロヘプチル)アミン、ビス(メチルシクロヘプチル)アミン、(ジメチルシクロヘプチル)アミン、(エチルシクロヘプチル)アミン、(メチルエチルシクロヘプチル)アミン、(ジエチルシクロヘプチル)アミン等のアルキルシクロアルキルアミンが挙げられ、これらモノアミンの全ての置換異性体も挙げられる。ここでいうモノアミンには、油脂から誘導される牛脂アミン等のモノアミンも含まれる。
N−メチルエチレンジアミン、N−エチルエチレンジアミン、N−プロピルエチレンジアミン、N−ブチルエチレンジアミン、N−ペンチルエチレンジアミン、N−ヘキシルエチレンジアミン、N−ヘプチルエチレンジアミン、N−オクチルエチレンジアミン、N−ノニルエチレンジアミン、N−デシルエチレンジアミン、N−ウンデシル、N−ドデシルエチレンジアミン、N−トリデシルエチレンジアミン、N−テトラデシルエチレンジアミン、N−ペンタデシルエチレンジアミン、N−ヘキサデシルエチレンジアミン、N−ヘプタデシルエチレンジアミン、N−オクタデシルエチレンジアミン、N−ノナデシルエチレンジアミン、N−イコシルエチレンジアミン、N−ヘンイコシルエチレンジアミン、N−ドコシルエチレンジアミン、N−トリコシルエチレンジアミン等のN−アルキルエチレンジアミン;
N−ビニルエチレンジアミン、N−プロペニルエチレンジアミン、N−ブテニルエチレンジアミン、N−ペンテニルエチレンジアミン、N−ヘキセニルエチレンジアミン、N−ヘプテニルエチレンジアミン、N−オクテニルエチレンジアミン、N−ノネニルエチレンジアミン、N−デセニルエチレンジアミン、N−ウンデセニル、N−ドデセニルエチレンジアミン、N−トリデセニルエチレンジアミン、N−テトラデセニルエチレンジアミン、N−ペンタデセニルエチレンジアミン、N−ヘキサデセニルエチレンジアミン、N−ヘプタデセニルエチレンジアミン、N−オクタデセニルエチレンジアミン、N−ノナデセニルエチレンジアミン、N−イコセニルエチレンジアミン、N−ヘンイコセニルエチレンジアミン、N−ドコセニルエチレンジアミン、N−トリコセニルエチレンジアミン等のN−アルケニルエチレンジアミン;
N−アルキルジエチレントリアミン、N−アルケニルジエチレントリアミン、N−アルキルトリエチレンテトラミン、N−アルケニルトリエチレンテトラミン、N−アルキルテトラエチレンペンタミン、N−アルケニルテトラエチレンペンタミン、N−アルキルペンタエチレンヘキサミン、N−アルケニルペンタエチレンヘキサミン、N−アルキルプロピレンジアミン、N−アルケニルプロピレンジアミン、N−アルキルジプロピレントリアミン、N−アルケニルジプロピレントリアミン、N−アルキルトリプロピレンテトラミン、N−アルケニルトリプロピレンテトラミン、N−アルキルテトラプロピレンペンタミン、N−アルケニルテトラプロピレンペンタミン、N−アルキルペンタプロピレンヘキサミン、N−アルケニルペンタプロピレンヘキサミン、N−アルキルブチレンジアミン、N−アルケニルブチレンジアミン、N−アルキルジブチレントリアミン、N−アルケニルジブチレントリアミン、N−アルキルトリブチレンテトラミン、N−アルケニルトリブチレンテトラミン、N−アルキルテトラブチレンペンタミン、N−アルケニルテトラブチレンペンタミン、N−アルキルペンタブチレンヘキサミン、N−アルケニルペンタブチレンヘキサミン等のN−アルキルまたはN−アルケニルアルキレンポリアミンが挙げられ、これらポリアミンの全ての置換異性体も挙げられる。また、ここでいうポリアミンには油脂から誘導されるポリアミン(牛脂ポリアミン等)も含まれる。
アルカノールアミンとしては、例えば、モノメタノールアミン、ジメタノールアミン、トリメタノールアミン、モノエタノールアミン、ジエタノールアミン、トリエタノールアミン、モノ(n−プロパノール)アミン、ジ(n−プロパノール)アミン、トリ(n−プロパノール)アミン、モノイソプロパノールアミン、ジイソプロパノールアミン、トリイソプロパノールアミン、モノブタノールアミン、ジブタノールアミン、トリブタノールアミン、モノペンタノールアミン、ジペンタノールアミン、トリペンタノールアミン、モノヘキサノールアミン、ジヘキサノールアミン、モノヘプタノールアミン、ジヘプタノールアミン、モノオクタノールアミン、モノノナノールアミン、モノデカノールアミン、モノウンデカノールアミン、モノドデカノールアミン、モノトリデカノールアミン、モノテトラデカノールアミン、モノペンタデカノールアミン、モノヘキサデカノールアミン、ジエチルモノエタノールアミン、ジエチルモノプロパノールアミン、ジエチルモノブタノールアミン、ジエチルモノペンタノールアミン、ジプロピルモノエタノールアミン、ジプロピルモノプロパノールアミン、ジプロピルモノブタノールアミン、ジプロピルモノペンタノールアミン、ジブチルモノエタノールアミン、ジブチルモノプロパノールアミン、ジブチルモノブタノールアミン、ジブチルモノペンタノールアミン、モノエチルジエタノールアミン、モノエチルジプロパノールアミン、モノエチルジブタノールアミン、モノエチルジペンタノールアミン、モノプロピルジエタノールアミン、モノプロピルジプロパノールアミン、モノプロピルジブタノールアミン、モノプロピルジペンタノールアミン、モノブチルジエタノールアミン、モノブチルジプロパノールアミン、モノブチルジブタノールアミン、モノブチルジペンタノールアミン、モノシクロヘキシルモノエタノールアミン、モノシクロヘキシルジエタノールアミン、モノシクロヘキシルモノプロパノールアミン、モノシクロヘキシルジプロパノールアミンが挙げられ、これらアルカノールアミンの全ての置換異性体も挙げられる。
カルボン酸の含有量が前記下限値未満であると、その添加によるさび止め性向上効果が不十分となる恐れがある。また、カルボン酸の含有量は、組成物全量を基準として、好ましくは2質量%以下、より好ましくは1.5質量%以下、更に好ましくは1質量%以下である。カルボン酸の含有量が前記上限値を超えると、基油に対する溶解性が不十分となり、貯蔵安定性が低下する恐れがある。
なお、本発明における元素の含有量とは、以下の方法によって測定される値をいう。すなわち、バリウム、亜鉛および鉛の含有量とは、ASTM D 5185−95;塩素の含有量とは、英国石油協会規格「PROPOSED METHOD AK/81 Determination of chlorine Microcoulometry oxidative method」にそれぞれ準拠して測定される組成物全量を基準とした含有量(質量ppm)を意味する。上記測定方法における各元素の検出限界は通常1質量ppmである。
被処理体である金属製部材は特に制限されず、具体的には、自動車ボディや電気製品ボディとなる冷延鋼板、熱延鋼板、高張力鋼板、亜鉛めっき鋼板等の表面処理鋼板、ブリキ用原板、アルミニウム合金板、マグネシウム合金板等の金属製板材、更には転がり軸受、テーパー転がり軸受、ニードル軸受等の軸受部品、建築用鋼材、精密部品等が挙げられる。
このような金属製部材に対する従来のさび止め油としては、金属製部材の加工工程等の過程で用いられる中間さび止め油、出荷時のさび止めのために用いられる出荷さび止め油、プレス加工に供する前の異物除去または金属板製造メーカーにおいて出荷に先立つ異物除去のための洗浄工程で用いられる洗浄さび止め油などがあるが、本発明の洗浄兼さび止め油組成物はこれらすべての用途に使用することができる。
実施例1〜42及び比較例1〜15においては、それぞれ以下に示す成分を用いて、表1〜6に示す組成を有するさび止め油組成物を調製した。
(A)成分
A1:40℃における動粘度が0.9mm2/sの鉱油(芳香族分:0.1質量%以下)
A2:40℃における動粘度が1.6mm2/sの鉱油(芳香族分:0.1質量%以下)
A3:40℃における動粘度が1.9mm2/sの鉱油(芳香族分:4.8質量%)
A4:40℃における動粘度が8.4mm2/sの鉱油
A5:40℃における動粘度が23mm2/sの鉱油
A6:40℃における動粘度が68mm2/sの鉱油
A7:40℃における動粘度が195mm2/sの鉱油
A8:40℃における動粘度が461mm2/sの鉱油
A9:40℃における動粘度:586mm2/sの鉱油
(B)成分
B1:C8脂肪酸のC8アルキルアミン塩
B2:C8脂肪酸のC18アルキルアミン塩
B3:C18脂肪酸のC8アルキルアミン塩
B4:C18脂肪酸のC18アルキルアミン塩
(C)成分
C1:ペンタエリスリトールのラノリン脂肪酸部分エステル
C2:ソルビタンモノイソステアレート
C3:ソルビタンモノオレート
C4:トリメチロールプロパンモノオレート
(D)成分
D1:オレオイルザルコシン(N−Methyloleamidoacetic acid)
D2:エチレンジアミンスルホネート
D3:塩基性Caスルホネート(塩基価:95mgKOH/g)
D4:パラフィンワックス
JIS K2246「さび止め油」中性塩水噴霧試験に準拠して評価を実施した。なお、試験片の研磨はJIS K2246「さび止め油」水置換試験方法に準拠し、A,P100の研磨材で行った。試験を実施する前に、予め試験片を水平に保った状態で水道水に5分間浸漬しその後直ちに水平に保った状態でさび止め油に5秒間浸漬した後に、水平に保った状態で取り出し50℃、95%の恒温恒湿槽内で3時間静置した。その後、試験法に準拠して中性塩水噴霧試験を実施した。さびが発生するまでの時間(h)を測定して評価し、評価は所定の時間毎(16,24,36,48時間)に行った。評価はJIS法に基づき試験数3で実施した。得られた結果を表1〜6に示す。
なお、油剤の安定性が悪く分離が認められるようなものは十分に攪拌した状態で試験に供した。
本評価では水除去性能が不十分であると水に起因するさびが発生するため、油剤そのもののさび止め性能と併せ水除去性を評価することができる。
油剤1リットルにイオン交換水1リトルを加え、5Lビーカ内にて全体がけん濁する程度の強度にて10時間攪拌した(1日目)。その後静置し、翌日も同様の操作を実施した。これを10回繰り返した。1日目、3日目、5日目、10日目に攪拌終了後、油層を分別して試験油とし、JIS K2246の中性塩水噴霧試験を実施しさび止め性能の低下度合いを比較した。さび止め性の評価は24時間後の試験片の状態を観察して評価した。得られた結果を表1〜6に示す。
さび止め油組成物を調製後、45℃に調整した恒温槽中に240時間保持し、油剤の分離の有無を目視で評価した。分離しない場合を、「無」、分離した場合を「有」とした。得られた結果を表1〜6に示す。
JIS K2283に準拠して、さび止め油組成物の40℃における動粘度を測定した。得られた結果を表1〜6に示す。
Claims (4)
- 40℃における動粘度が6mm2/s以下の鉱油である第1の鉱油と、
40℃における動粘度が250mm2/s以上の鉱油である第2の鉱油と、
脂肪酸アミン塩と、
エステルと、
ザルコシン型化合物、ノニオン系界面活性剤、スルホン酸塩、アミン、カルボン酸、カルボン酸塩、パラフィンワックス、酸化ワックス塩及びホウ素化合物からなる群から選ばれる1種以上のさび止め剤と、
を含有し、
前記脂肪酸アミン塩の含有量が、組成物全量基準で2質量%以上10質量%以下であり、
前記エステルの含有量が、組成物全量基準で4質量%以上20質量%以下である、さび止め油組成物。 - 40℃における動粘度が10mm2/s以上120mm2/s以下の鉱油である第3の鉱油をさらに含有する、請求項1に記載のさび止め油組成物。
- 前記第1の鉱油の芳香族分含有量が、前記第1の鉱油の全量を基準として、3質量%以下である、請求項1又は2に記載のさび止め油組成物。
- JIS K 2246「さび止め油」で規定されている中性塩水噴霧試験において、さび発生度がA級(さび発生度が0%)を維持する時間が16時間以上である、請求項1〜3のいずれか一項に記載のさび止め油組成物。
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