JP2018517587A - 光学効果層を生成するための方法 - Google Patents
光学効果層を生成するための方法 Download PDFInfo
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- JP2018517587A JP2018517587A JP2017561710A JP2017561710A JP2018517587A JP 2018517587 A JP2018517587 A JP 2018517587A JP 2017561710 A JP2017561710 A JP 2017561710A JP 2017561710 A JP2017561710 A JP 2017561710A JP 2018517587 A JP2018517587 A JP 2018517587A
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Abstract
Description
[001]本発明は、有価文書及び有価商品の偽造及び違法複製からの保護の分野に関する。特に、本発明は、磁気的に配向した磁性又は磁化可能な顔料粒子を含む光学効果層(OEL)を生成するための方法に関する。
[002]磁性又は磁化可能な粒子又は顔料、特に磁性を有する光学的に可変の顔料を含有するインク、組成物又は層を、例えばセキュリティ文書の分野におけるセキュリティ要素の生成に使用することは、当技術分野において公知である。配向した磁性又は磁化可能な粒子を含むコーティング又は層は、例えば、米国特許第2,570,856号;米国特許第3,676,273号;米国特許第3,791,864号;米国特許第5,630,877号及び米国特許第5,364,689号において開示されている。特に魅力的な光学効果をもたらす、セキュリティ文書の保護に有用な配向した磁性色変化顔料粒子を含むコーティング又は層は、国際公開第2002/090002A2号及び国際公開第2005/002866A1号において開示されている。
[012]したがって、本発明の目的は、上述のような先行技術の欠陥を克服することである。
a)コーティング層を形成するために、フォトマスクを備える基板上に、1種又は複数種の光開始剤及び複数の磁性又は磁化可能な顔料粒子を含む放射線硬化性コーティング組成物を塗布するステップであり、上記コーティング層は、第1の状態にあり、上記コーティング層は、フォトマスクに少なくとも部分的に面している、ステップと;
b)
b1)コーティング層を保持する1つ又は複数の第1の基板エリアを、基板を通して硬質化させるステップであり、上記硬質化は、磁性又は磁化可能な顔料粒子をその位置及び配向で固定又は定着させるために、UV−Vis照射源での照射により第2の状態まで行われる、ステップと;
c)
c1)基板のフォトマスクの存在のために第1の状態にある、コーティング層を保持する少なくとも1つ又は複数の第2の基板エリアを、磁場生成デバイスの磁場に曝露し、それによって、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターンに従うように、複数の磁性又は磁化可能な顔料粒子を配向させるステップと;
c2)磁性又は磁化可能な顔料粒子をその採用された位置及び配向で固定又は定着させるために、UV−Vis照射源での照射により、コーティング層を保持する少なくとも1つ又は複数の第2の基板エリアを、第2の状態まで、同時に、部分的に同時に又は後続して硬質化させるステップと
を含む。
コーティング層のマスキングされたエリアの磁性又は磁化可能な顔料粒子は、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターンに従うように配向され;
コーティング層のマスキングされていないエリアの磁性又は磁化可能な顔料粒子は、ランダム配向に従うか、又はマスキングされていないエリアの磁性若しくは磁化可能な顔料粒子と異なる配向パターンに従うように配向され、人間の目により判定可能であるような視覚的に異なる光学的印象をもたらす。
[023]一実施形態において、フォトマスクは、UV吸収フォトマスク組成物で作製される。
定義
[0024]以下の定義は、説明において議論され、特許請求の範囲において列挙された用語の意味を解釈するために使用されるものである。
[037]本発明は、フォトマスクを備える基板上に光学効果層(OEL)を生成するための方法を提供し、OELは、単一の硬質化層で作製された少なくとも2つのエリア、好ましくは少なくとも2つの隣接するエリアで作製されたモチーフを備え、少なくとも2つのエリアは、異なる磁性又は磁化可能な顔料粒子の配向パターンを有する。少なくとも2つのエリアのうちの1つのエリアは、第1の磁性又は磁化可能な顔料粒子の配向パターンに従うように配向した、複数の磁性又は磁化可能な顔料粒子を含み、上記配向パターンは、ランダム配向パターン、又はランダム配向パターンを除く任意の配向パターン、好ましくは、複数の磁性又は磁化可能な顔料粒子が、OELを保持する側から視認した場合に凹状の湾曲に従うように配向した配向パターンであってもよく;少なくとも2つのエリアの別のエリアは、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターン、好ましくは、複数の磁性又は磁化可能な顔料粒子が、OELを保持する側から視認した場合に凸状の湾曲に従うように配向した配向パターンに従うように配向した、複数の磁性又は磁化可能な顔料を含み、少なくとも2つのエリアの磁性又は磁化可能な顔料粒子の配向パターンは、肉眼で区別可能である。
TSM(λ)=TS(λ)TM(λ)
式中、TS(λ)は、波長λにおける基板の透過率であり、TM(λ)は、波長λにおけるフォトマスクの透過率である。
[0163]図6A〜B、7A〜C及び8A〜Bに示されるプロセスにより、基板(Papierfabrik Louisenthal製信託標準紙BNP 90g/m2)上にOELを生成した。
(*)JDS−Uniphase、Santa Rosa、CAから得られた、約9.3μmの直径d50及び約1μmの厚さのフレーク形状を有する金色から緑色の光学的に可変の磁性顔料粒子。
[0167]「50」の印の形状(図6C)の、1.1重量%のCブラック(Orion製カーボンスペシャルブラック(Carbon Special Black)4A)を含有する溶媒ベースシルクスクリーン組成物(表3を参照されたい)で作製されたフォトマスク(680)を備える基板を使用した。T90シルクスクリーンにより、フォトマスクを塗布した(約25g/m2の湿潤堆積物に対応する)。
[0173]長方形の形状(図7A〜D)の、1.1%のCブラック(Orion製カーボンスペシャルブラック4A)を含有する溶媒ベースシルクスクリーン組成物(表3を参照されたい)で作製されたフォトマスク(780)を備える基板を使用した。T90シルクスクリーンにより、フォトマスクを塗布した(約25g/m2の湿潤堆積物に対応する)。
[0178]長方形(2.5×3.5cm)の形状(図8A〜C)の、25重量%のCブラック(Orion製カーボンスペシャルブラック4A)を含有するオフセット組成物(表2を参照されたい)で作製されたフォトマスク(880)を備える基板を使用した。フォトマスクを、Prufbau製印刷可能性テスターでベタ印刷(約20cm×4cm)として印刷した(オフセット組成物の量は2g/m2であった)。
[0184]75部のオフセットビヒクルV1(表2)及び25部のCブラック(Orion製カーボンスペシャルブラック4A)を室温で混合することにより、E3のオフセット組成物を調製した。結果的なペーストを、SDY300三本ロールミルで3回(1回目は6バールの圧力、2回目及び3回目は12バールの圧力)粉砕した。
Claims (15)
- フォトマスクを備える基板上に光学効果層(OEL)を生成するための方法であって、前記OELは、単一の硬質化層で作製された少なくとも2つのエリア、好ましくは少なくとも2つの隣接するエリアで作製されたモチーフを備え、前記方法は、
a)コーティング層を形成するために、前記フォトマスクを備える前記基板上に、1種又は複数種の光開始剤及び複数の磁性又は磁化可能な顔料粒子を含む放射線硬化性コーティング組成物を塗布するステップであり、前記コーティング層は、第1の状態にあり、前記コーティング層は、前記フォトマスクに少なくとも部分的に面している、ステップと;
b)
b1)前記コーティング層を保持する1つ又は複数の第1の基板エリアを、前記基板を通して硬質化させるステップであり、前記硬質化は、前記磁性又は磁化可能な顔料粒子をその位置及び配向で固定又は定着させるために、UV−Vis照射源での照射により第2の状態まで行われる、ステップと;
c)
c1)前記基板の前記フォトマスクの存在のために第1の状態にある、前記コーティング層を保持する少なくとも1つ又は複数の第2の基板エリアを、磁場生成デバイスの磁場に曝露し、それによって、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターンに従うように、前記複数の磁性又は磁化可能な顔料粒子を配向させるステップと;
c2)前記磁性又は磁化可能な顔料粒子をその採用された位置及び配向で固定又は定着させるために、UV−Vis照射源での照射により、前記コーティング層を保持する少なくとも前記1つ又は複数の第2の基板エリアを、第2の状態まで、同時に、部分的に同時に又は後続して硬質化させるステップとを含み、
前記フォトマスクは、1.0以上、好ましくは1.1以上、より好ましくは1.2以上の光学密度DMを有する、方法。 - 前記ステップb)が、
b0)前記コーティング層を保持する1つ又は複数の第1の基板エリアを、第1の磁場生成デバイスの磁場に曝露し、それによって、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターンである、磁性又は磁化可能な顔料粒子の配向パターンに従うように、前記複数の磁性又は磁化可能な顔料粒子を配向させるステップと、
b1)前記コーティング層を前記基板を通して同時に、又は部分的に同時に又は後続して硬質化させるステップであり、前記硬質化は、前記磁性又は磁化可能な顔料粒子をその採用された位置及び配向で固定又は定着させるために、UV−Vis照射源での照射により第2の状態まで行われる、ステップと
を含み、ステップb0)の前記配向パターンは、ステップc1)の前記配向パターンとは異なる、請求項1に記載の方法。 - 前記第1の磁場生成デバイスが、前記基板の前記コーティング層を保持する側に位置する、請求項2に記載の方法。
- 前記第1の磁場生成デバイスが、前記コーティング層を保持する側から視認した場合に凹状湾曲に従うように、前記複数の磁性又は磁化可能な顔料粒子を配向させる、請求項3に記載の方法。
- ステップb1)が、ステップb0)と、部分的に同時に、又は同時に行われる、請求項2〜4のいずれか一項に記載の方法。
- 前記ステップc1)が、第2の磁場生成デバイスを用いて行われ、それによって、前記コーティング層を保持する側から視認した場合に凸状湾曲に従うように、前記複数の磁性又は磁化可能な顔料粒子を配向させる、請求項1〜5のいずれか一項に記載の方法。
- 前記磁性又は磁化可能な顔料粒子が、非球状の磁性又は磁化可能な顔料粒子、好ましくは扁長若しくは扁平楕円体状、小板状又は針状粒子、或いはそれらの2つ以上の混合物、より好ましくは小板状粒子である、請求項1〜6のいずれか一項に記載の方法。
- 前記複数の前記磁性又は磁化可能な顔料粒子の少なくとも一部が、磁性薄膜干渉顔料、磁性コレステリック液晶顔料、1種又は複数種の磁性材料を含む干渉コーティング顔料、及びそれらの混合物で構成される、請求項1〜7のいずれか一項に記載の方法。
- 前記フォトマスクが、バインダー及び1種又は複数種のUV吸収材料を含むUV吸収フォトマスク組成物で作製された、印刷UV吸収フォトマスクである、請求項1〜8のいずれか一項に記載の方法。
- 前記1種又は複数種のUV吸収材料が、染料、有機顔料、無機顔料、光学的に可変の顔料、充填剤、UV吸収剤、鉱物酸化物ナノ粒子、及びそれらの混合物からなる群から選択される、請求項9に記載の方法。
- UV−Vis照射源での照射により、前記コーティングを保持する少なくとも前記1つ又は複数の第2の基板エリアを硬質化させる前記ステップc2)が、少なくとも1つ又は複数の第2の基板エリアを前記第2の磁場生成デバイスの前記磁場に曝露する前記ステップc1)と同時に、又は部分的に同時に行われる、請求項1〜10のいずれか一項に記載の方法。
- 請求項1〜11のいずれか一項に記載の方法により調製される、光学効果層(OEL)。
- セキュリティ文書の偽造若しくは不正からの保護、又は装飾用途のための、請求項12に記載の光学効果層(OEL)の使用。
- 1つ又は複数の請求項12に記載の光学効果層(OEL)を備える、セキュリティ文書。
- フォトマスクを備える基板上に配置された光学効果層(OEL)であって、前記OELは、単一の硬質化層で作製された少なくとも2つのエリア、好ましくは少なくとも2つの隣接するエリアで作製されたモチーフを備え、前記OELは、コーティング層を形成するために放射線硬化により放射線硬化コーティング組成物中で固定又は定着された複数の磁性又は磁化可能な顔料粒子を含む前記コーティング組成物を含み、前記コーティング層は、少なくとも部分的に前記フォトマスクと重複して、そのマスキングされたエリア及びマスキングされていないエリアをもたらし;
前記コーティング層の前記マスキングされたエリアの前記磁性又は磁化可能な顔料粒子は、ランダム配向を除く任意の磁性又は磁化可能な顔料粒子の配向パターンに従うように配向され;
前記コーティング層の前記マスキングされていないエリアの前記磁性又は磁化可能な顔料粒子は、ランダム配向に従うか、又は前記マスキングされたエリアの前記磁性若しくは磁化可能な顔料粒子の配向パターンと異なる配向パターンに従うように配向され、人間の目により判定可能であるような視覚的に異なる光学的印象をもたらす、光学効果層(OEL)。
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US20130189454A1 (en) * | 2012-01-12 | 2013-07-25 | Vladimir P. Raksha | Article with curved patterns formed of aligned pigment flakes |
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JP2023506204A (ja) * | 2019-12-12 | 2023-02-15 | タレス ディアイエス フランス エスアーエス | 隠れフローティングイメージ |
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EP3304204A1 (en) | 2018-04-11 |
US10328739B2 (en) | 2019-06-25 |
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ES2726306T3 (es) | 2019-10-03 |
KR20180014687A (ko) | 2018-02-09 |
JP6716828B2 (ja) | 2020-07-01 |
CN107710075B (zh) | 2019-11-08 |
AU2016273191B2 (en) | 2020-02-06 |
CA2980858C (en) | 2023-09-26 |
AR104860A1 (es) | 2017-08-23 |
RU2017138115A (ru) | 2019-07-10 |
EP3304204B1 (en) | 2019-03-06 |
KR102589873B1 (ko) | 2023-10-17 |
US20180111406A1 (en) | 2018-04-26 |
RU2017138115A3 (ja) | 2019-07-31 |
CN107710075A (zh) | 2018-02-16 |
HK1244892A1 (zh) | 2018-08-17 |
RU2698428C2 (ru) | 2019-08-26 |
TW201703879A (zh) | 2017-02-01 |
AU2016273191A1 (en) | 2017-09-28 |
TR201907570T4 (tr) | 2019-06-21 |
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