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IE812785L - Removal of urea, ammonia and carbon dioxide from aqueous¹solutions - Google Patents

Removal of urea, ammonia and carbon dioxide from aqueous¹solutions

Info

Publication number
IE812785L
IE812785L IE812785A IE278581A IE812785L IE 812785 L IE812785 L IE 812785L IE 812785 A IE812785 A IE 812785A IE 278581 A IE278581 A IE 278581A IE 812785 L IE812785 L IE 812785L
Authority
IE
Ireland
Prior art keywords
urea
ammonia
carbon dioxide
removal
bar
Prior art date
Application number
IE812785A
Other versions
IE53218B1 (en
Original Assignee
Unie Van Kunstmestfab Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unie Van Kunstmestfab Bv filed Critical Unie Van Kunstmestfab Bv
Publication of IE812785L publication Critical patent/IE812785L/en
Publication of IE53218B1 publication Critical patent/IE53218B1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/26—Fractionating columns in which vapour and liquid flow past each other, or in which the fluid is sprayed into the vapour, or in which a two-phase mixture is passed in one direction
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C02F1/586—Treatment of water, waste water, or sewage by removing specified dissolved compounds by removing ammoniacal nitrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/025—Thermal hydrolysis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048—Purification of waste water by evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Engineering & Computer Science (AREA)
  • Hydrology & Water Resources (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

Removal of urea, ammonia and carbon dioxide from diluted aqueous solutions, for instance urea process effluent, the solution being led into the top of a reaction column under a pressure of 10-30 bar, in which it flows down in counter-current to a flow of gas, for instance steam. The temperature in the top of the reaction column is 170-220 DEG C; at the bottom, it is 180-230 DEG C. Next, at a pressure of 1-5 bar, ammonia and carbon dioxide are removed from the urea-free bottom solution. The remaining solution contains less than 10 ppm urea and less than 10 ppm ammonia. [EP0053410A1]
IE2785/81A 1980-11-28 1981-11-27 Process for the removal of urea,ammonia and carbon dioxide from dilute aqueous solutions IE53218B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL8006477A NL8006477A (en) 1980-11-28 1980-11-28 METHOD FOR REMOVING UREA, AMMONIA AND CARBON DIOXIDE FROM DILUTED AQUEOUS SOLUTION.

Publications (2)

Publication Number Publication Date
IE812785L true IE812785L (en) 1982-05-28
IE53218B1 IE53218B1 (en) 1988-09-14

Family

ID=19836250

Family Applications (1)

Application Number Title Priority Date Filing Date
IE2785/81A IE53218B1 (en) 1980-11-28 1981-11-27 Process for the removal of urea,ammonia and carbon dioxide from dilute aqueous solutions

Country Status (33)

Country Link
US (1) US4456535A (en)
EP (1) EP0053410B1 (en)
JP (1) JPS57118011A (en)
KR (2) KR860000189B1 (en)
AU (1) AU547371B2 (en)
BR (1) BR8107728A (en)
CA (1) CA1201726A (en)
CS (1) CS227021B2 (en)
CU (1) CU21419A (en)
DE (1) DE3171612D1 (en)
ES (1) ES8301841A1 (en)
FI (1) FI74947C (en)
GR (1) GR75396B (en)
HU (1) HU188717B (en)
IE (1) IE53218B1 (en)
IL (1) IL64392A (en)
IN (1) IN156310B (en)
MA (1) MA19335A1 (en)
MY (1) MY8600489A (en)
NL (1) NL8006477A (en)
NO (1) NO154749C (en)
NZ (1) NZ199085A (en)
OA (1) OA06958A (en)
PH (1) PH19196A (en)
PL (1) PL134841B1 (en)
PT (1) PT74046B (en)
RO (1) RO83971B (en)
SG (1) SG100285G (en)
SU (1) SU1378781A3 (en)
TR (1) TR21827A (en)
YU (1) YU41999B (en)
ZA (1) ZA818269B (en)
ZW (1) ZW28781A1 (en)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4522727A (en) * 1984-10-22 1985-06-11 Atec Inc. Process for continuous removal of ammoniacal nitrogen from aqueous streams
AT388157B (en) * 1987-07-16 1989-05-10 Vogelbusch Gmbh METHOD FOR TREATING AMMONIA AND / OR OTHER ODOR-ACTIVE SUBSTANCES AND ORGANICALLY BURNED SOLIDS CONTAINING SOLIDS
NL8702530A (en) * 1987-10-23 1989-05-16 Stamicarbon PROCESS FOR THE PREPARATION OF UREA AND WATER FROM AMMONIA AND CARBON DIOXIDE.
IT1232670B (en) * 1989-09-15 1992-03-02 Snam Progetti PROCEDURE FOR PURIFICATION OF WASTEWATER PRODUCED BY UREA PRODUCTION PLANTS.
RU2056408C1 (en) * 1991-10-23 1996-03-20 Уриа Казале С.А. Method of urea hydrolysis containing in spent water from plants of urea synthesis and column apparatus for its realization
US5525237A (en) * 1993-12-23 1996-06-11 United Technologies Corporation Process for removing free and dissolved CO2 from aqueous solutions
US5518626A (en) * 1993-12-23 1996-05-21 United Technologies Corporation Process employing thermally sterilizable aqueous polishing agents
US5597454A (en) * 1995-04-06 1997-01-28 Lee; Jing M. Process for producing urea
KR100398799B1 (en) * 2001-04-04 2003-09-19 한화석유화학 주식회사 Process for treating a waste water containing a nitrous organic components
US6761868B2 (en) * 2001-05-16 2004-07-13 The Chemithon Corporation Process for quantitatively converting urea to ammonia on demand
US6755029B2 (en) 2002-01-08 2004-06-29 Marvin Ralph Bertrand, Jr. Ammonia separator and neutralizer
US20040177644A1 (en) * 2002-01-08 2004-09-16 Masterson James A. Method and apparatus for separating and neutralizing ammonia
US7272953B2 (en) * 2002-01-08 2007-09-25 Masterson James A Method and apparatus for separating and neutralizing ammonia
US6887449B2 (en) * 2002-11-21 2005-05-03 The Chemithon Corporation Method of quantitatively producing ammonia from urea
CN100400430C (en) * 2006-05-18 2008-07-09 刘国胜 Energy saving, purifying and recovering process for urea process condensate
EP2386346A1 (en) 2010-05-11 2011-11-16 Stamicarbon B.V. Process for the reduction of ammonia emissions in a urea manufacturing process
JP6634342B2 (en) * 2016-05-24 2020-01-22 東洋エンジニアリング株式会社 Method and apparatus for treating urea aqueous solution
WO2019030196A1 (en) * 2017-08-11 2019-02-14 Akzo Nobel Chemicals International B.V. Process for converting cyclic alkylene ureas into their corresponding alkylene amines
DE102019208859A1 (en) * 2019-06-18 2020-12-24 Skw Stickstoffwerke Piesteritz Gmbh Process for the continuous production of pure urea solutions by utilizing process water
CN111137906A (en) * 2020-03-13 2020-05-12 安徽六国化工股份有限公司 Device and method for treating urea dilute urine solution
CN112744945A (en) * 2020-11-30 2021-05-04 安徽金禾实业股份有限公司 Method and device for oxidizing and alkaline hydrolyzing sucralose rectification wastewater

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE146751C (en) *
DE146752C (en) *
US3390058A (en) * 1964-06-08 1968-06-25 Toyo Koatsu Ind Inc Plural stage pressure distillation of urea synthesis effluent with liquified gas addition
ES318356A1 (en) * 1964-10-16 1966-05-16 Toyo Koatsu Ind Incorporated Method of depuration of an effluent in the obtaining of synthetic urea. (Machine-translation by Google Translate, not legally binding)
US4341640A (en) * 1976-09-27 1982-07-27 Standard Oil Company Urea hydrolysis
JPS5826909B2 (en) * 1979-09-14 1983-06-06 東洋エンジニアリング株式会社 Method for concentrating urea aqueous solution

Also Published As

Publication number Publication date
ZA818269B (en) 1983-06-29
DE3171612D1 (en) 1985-09-05
MY8600489A (en) 1986-12-31
NL8006477A (en) 1982-06-16
AU547371B2 (en) 1985-10-17
IL64392A0 (en) 1982-02-28
PL234005A1 (en) 1982-06-21
BR8107728A (en) 1982-08-31
FI74947B (en) 1987-12-31
NO154749B (en) 1986-09-08
KR830007109A (en) 1983-10-14
YU274181A (en) 1983-02-28
GR75396B (en) 1984-07-13
IN156310B (en) 1985-06-22
SG100285G (en) 1986-07-18
EP0053410B1 (en) 1985-07-31
CU21419A (en) 1983-12-21
US4456535A (en) 1984-06-26
SU1378781A3 (en) 1988-02-28
IL64392A (en) 1984-10-31
MA19335A1 (en) 1982-07-01
IE53218B1 (en) 1988-09-14
ES507512A0 (en) 1983-01-01
FI74947C (en) 1988-04-11
ES8301841A1 (en) 1983-01-01
NZ199085A (en) 1985-08-30
HU188717B (en) 1986-05-28
EP0053410A1 (en) 1982-06-09
PH19196A (en) 1986-01-28
RO83971B (en) 1984-08-30
KR860000189B1 (en) 1986-03-03
CS227021B2 (en) 1984-04-16
ZW28781A1 (en) 1982-02-24
NO154749C (en) 1986-12-17
FI813811L (en) 1982-05-29
TR21827A (en) 1985-08-15
AU7794181A (en) 1982-06-03
PL134841B1 (en) 1985-09-30
NO814070L (en) 1982-06-01
CA1201726A (en) 1986-03-11
PT74046A (en) 1981-12-01
YU41999B (en) 1988-04-30
JPS57118011A (en) 1982-07-22
RO83971A (en) 1984-06-21
OA06958A (en) 1983-07-31
PT74046B (en) 1983-04-26

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