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GB887360A - Process for making derivatives of hydroxymethyl furfural - Google Patents

Process for making derivatives of hydroxymethyl furfural

Info

Publication number
GB887360A
GB887360A GB27494/58A GB2749458A GB887360A GB 887360 A GB887360 A GB 887360A GB 27494/58 A GB27494/58 A GB 27494/58A GB 2749458 A GB2749458 A GB 2749458A GB 887360 A GB887360 A GB 887360A
Authority
GB
United Kingdom
Prior art keywords
hydroxymethyl furfural
alkanol
carbon atoms
making derivatives
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB27494/58A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merck and Co Inc
Original Assignee
Merck and Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merck and Co Inc filed Critical Merck and Co Inc
Publication of GB887360A publication Critical patent/GB887360A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Compounds having the formula <FORM:0887360/IV (b)/1> in which R is an alkyl radical having from 1 to 8 carbon atoms or the radical <FORM:0887360/IV (b)/2> are made by heating 5-hydroxymethyl furfural alone or with an alkanol having 1-8 carbon atoms in the molecule in the presence of an acid catalyst, the effect of the water formed being controlled either by continuously removing it or by using a large excess of alkanol. Suitable catalysts are, for example, p-toluene sulphonic acid, sulphuric acid, a sulphonated ion-exchange resin, hydrogen chloride or zinc chloride.
GB27494/58A 1957-09-04 1958-08-27 Process for making derivatives of hydroxymethyl furfural Expired GB887360A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US887360XA 1957-09-04 1957-09-04

Publications (1)

Publication Number Publication Date
GB887360A true GB887360A (en) 1962-01-17

Family

ID=22213140

Family Applications (1)

Application Number Title Priority Date Filing Date
GB27494/58A Expired GB887360A (en) 1957-09-04 1958-08-27 Process for making derivatives of hydroxymethyl furfural

Country Status (1)

Country Link
GB (1) GB887360A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7317116B2 (en) 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
US7432382B2 (en) 2004-12-10 2008-10-07 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
WO2009030507A2 (en) 2007-09-07 2009-03-12 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars and higher alcohols

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7317116B2 (en) 2004-12-10 2008-01-08 Archer-Daniels-Midland-Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
US7432382B2 (en) 2004-12-10 2008-10-07 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
US7579490B2 (en) 2004-12-10 2009-08-25 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
US7579489B2 (en) 2004-12-10 2009-08-25 Archer-Daniels-Midland Company Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives
US8058458B2 (en) 2004-12-10 2011-11-15 Archer Daniels Midland Company Processes for the preparation and purification of hydroxymethylfuraldehyde derivatives
WO2009030507A2 (en) 2007-09-07 2009-03-12 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars and higher alcohols
WO2009030507A3 (en) * 2007-09-07 2009-05-28 Furanix Technologies Bv Hydroxymethylfurfural ethers from sugars and higher alcohols
US20100218415A1 (en) * 2007-09-07 2010-09-02 Furanix Technologies B.V. Hydroxymethylfurfural ethers from sugars and higher alcohols

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