GB856087A - Spectrometric cell structure - Google Patents
Spectrometric cell structureInfo
- Publication number
- GB856087A GB856087A GB17765/59A GB1776559A GB856087A GB 856087 A GB856087 A GB 856087A GB 17765/59 A GB17765/59 A GB 17765/59A GB 1776559 A GB1776559 A GB 1776559A GB 856087 A GB856087 A GB 856087A
- Authority
- GB
- United Kingdom
- Prior art keywords
- cell
- cavity
- rock salt
- infra
- drilled
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
- G01N2021/0346—Capillary cells; Microcells
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
856,087. Spectrometer cells. NATIONAL RESEARCH COUNCIL. May 25, 1959 [June 3, 1958], No. 17765/59. Class 97(1) A cell for containing samples of liquid for infra-red spectroscopic analysis is made as a unitary body from a single piece of material. For preference, rock salt is used, but other materials which are transparent to infra-red radiation may also be used; for example, the halides of the alkali-metals, silver, barium calcium and lead, and also arsenic-trisulphide. If the cell is made from rock salt, a single crystal must be used of sufficient size to allow the cell to have dimensions of the order of 2cm x lcm x 0.5cm. The cell cavity is formed by ultrasonic impact drilling and is normally rectangular in shape with planar parallel faces as shown in Fig. 1. The uppermost portion of the cavity is first drilled by conventional means to form a circular aperture for a stopper. If it is desirable to have a small opening in order to minimize evaporation, this is drilled in a separate piece of rock salt which is then bonded to the top of the cell by moistening with aqueous sodium chloride and clamping under pressure at a temperature of 110‹C for 12 hours. To obtain a very thin cavity without deformation of the grinding tool, the tool is reinforced with cylindrical bars on both sideedges. The resulting cavity will then have a dumb-bell shaped cross-section as in Fig. 8 in the central parallel-sided portion of which the test liquid is held by capillary action without the cylindrical portions having to be filled.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA856087X | 1958-06-03 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB856087A true GB856087A (en) | 1960-12-14 |
Family
ID=4172705
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB17765/59A Expired GB856087A (en) | 1958-06-03 | 1959-05-25 | Spectrometric cell structure |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB856087A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL7610712A (en) * | 1975-09-29 | 1977-03-31 | Jan Evert Lilja En Sven Erik L | CUVET FOR SAMPLING. |
-
1959
- 1959-05-25 GB GB17765/59A patent/GB856087A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL7610712A (en) * | 1975-09-29 | 1977-03-31 | Jan Evert Lilja En Sven Erik L | CUVET FOR SAMPLING. |
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