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GB2012757A - Separation of Ethylamines - Google Patents

Separation of Ethylamines

Info

Publication number
GB2012757A
GB2012757A GB79944A GB7900944A GB2012757A GB 2012757 A GB2012757 A GB 2012757A GB 79944 A GB79944 A GB 79944A GB 7900944 A GB7900944 A GB 7900944A GB 2012757 A GB2012757 A GB 2012757A
Authority
GB
United Kingdom
Prior art keywords
water
ethylamines
diethylamine
mixture
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB79944A
Other versions
GB2012757B (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Priority to GB79944A priority Critical patent/GB2012757B/en
Publication of GB2012757A publication Critical patent/GB2012757A/en
Application granted granted Critical
Publication of GB2012757B publication Critical patent/GB2012757B/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/10Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/86Separation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Separation of mixtures of ethylamines is carried out by extracting a mixture comprising diethylamine, triethylamine, ethanol, water and optionally monoethylamine with water and a water-immiscible solvent, for example an alkane or aromatic hydrocarbon under such conditions that the ethanol and any monoethylamine are extracted into the water layer, the triethylamine into the water-immiscible layer, while the diethylamine is partitioned between the two layers, the diethylamine passing into either of the two layers when it forms a substantial component (greater than about 12%) of the ethylamine mixture but passing largely into the water layer when it forms a less significant part (up to about 11%) of the ethylamines mixture. <IMAGE>
GB79944A 1978-01-24 1979-01-10 Amine separation process Expired GB2012757B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB79944A GB2012757B (en) 1978-01-24 1979-01-10 Amine separation process

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB279378 1978-01-24
GB79944A GB2012757B (en) 1978-01-24 1979-01-10 Amine separation process

Publications (2)

Publication Number Publication Date
GB2012757A true GB2012757A (en) 1979-08-01
GB2012757B GB2012757B (en) 1982-08-18

Family

ID=26237732

Family Applications (1)

Application Number Title Priority Date Filing Date
GB79944A Expired GB2012757B (en) 1978-01-24 1979-01-10 Amine separation process

Country Status (1)

Country Link
GB (1) GB2012757B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0034400A2 (en) * 1980-02-08 1981-08-26 Imperial Chemical Industries Plc Amine separation process
US6821396B2 (en) 2001-10-30 2004-11-23 Basf Aktiengesellscahft Process for fractionating water-containing crude amine mixtures from amine synthesis
CN109053465A (en) * 2018-10-13 2018-12-21 宁波工程学院 A kind of ethamine clean-production system
CN109251147A (en) * 2018-10-22 2019-01-22 宁波工程学院 The ethamine production system of boiler fly ash removal of impurities is provided in a kind of utilization for oneself

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0034400A2 (en) * 1980-02-08 1981-08-26 Imperial Chemical Industries Plc Amine separation process
EP0034400A3 (en) * 1980-02-08 1982-01-13 Imperial Chemical Industries Plc Amine separation process
US6821396B2 (en) 2001-10-30 2004-11-23 Basf Aktiengesellscahft Process for fractionating water-containing crude amine mixtures from amine synthesis
CN109053465A (en) * 2018-10-13 2018-12-21 宁波工程学院 A kind of ethamine clean-production system
CN109251147A (en) * 2018-10-22 2019-01-22 宁波工程学院 The ethamine production system of boiler fly ash removal of impurities is provided in a kind of utilization for oneself

Also Published As

Publication number Publication date
GB2012757B (en) 1982-08-18

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Legal Events

Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee