GB2012757A - Separation of Ethylamines - Google Patents
Separation of EthylaminesInfo
- Publication number
- GB2012757A GB2012757A GB79944A GB7900944A GB2012757A GB 2012757 A GB2012757 A GB 2012757A GB 79944 A GB79944 A GB 79944A GB 7900944 A GB7900944 A GB 7900944A GB 2012757 A GB2012757 A GB 2012757A
- Authority
- GB
- United Kingdom
- Prior art keywords
- water
- ethylamines
- diethylamine
- mixture
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/10—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/86—Separation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Separation of mixtures of ethylamines is carried out by extracting a mixture comprising diethylamine, triethylamine, ethanol, water and optionally monoethylamine with water and a water-immiscible solvent, for example an alkane or aromatic hydrocarbon under such conditions that the ethanol and any monoethylamine are extracted into the water layer, the triethylamine into the water-immiscible layer, while the diethylamine is partitioned between the two layers, the diethylamine passing into either of the two layers when it forms a substantial component (greater than about 12%) of the ethylamine mixture but passing largely into the water layer when it forms a less significant part (up to about 11%) of the ethylamines mixture. <IMAGE>
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB79944A GB2012757B (en) | 1978-01-24 | 1979-01-10 | Amine separation process |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB279378 | 1978-01-24 | ||
GB79944A GB2012757B (en) | 1978-01-24 | 1979-01-10 | Amine separation process |
Publications (2)
Publication Number | Publication Date |
---|---|
GB2012757A true GB2012757A (en) | 1979-08-01 |
GB2012757B GB2012757B (en) | 1982-08-18 |
Family
ID=26237732
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB79944A Expired GB2012757B (en) | 1978-01-24 | 1979-01-10 | Amine separation process |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB2012757B (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0034400A2 (en) * | 1980-02-08 | 1981-08-26 | Imperial Chemical Industries Plc | Amine separation process |
US6821396B2 (en) | 2001-10-30 | 2004-11-23 | Basf Aktiengesellscahft | Process for fractionating water-containing crude amine mixtures from amine synthesis |
CN109053465A (en) * | 2018-10-13 | 2018-12-21 | 宁波工程学院 | A kind of ethamine clean-production system |
CN109251147A (en) * | 2018-10-22 | 2019-01-22 | 宁波工程学院 | The ethamine production system of boiler fly ash removal of impurities is provided in a kind of utilization for oneself |
-
1979
- 1979-01-10 GB GB79944A patent/GB2012757B/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0034400A2 (en) * | 1980-02-08 | 1981-08-26 | Imperial Chemical Industries Plc | Amine separation process |
EP0034400A3 (en) * | 1980-02-08 | 1982-01-13 | Imperial Chemical Industries Plc | Amine separation process |
US6821396B2 (en) | 2001-10-30 | 2004-11-23 | Basf Aktiengesellscahft | Process for fractionating water-containing crude amine mixtures from amine synthesis |
CN109053465A (en) * | 2018-10-13 | 2018-12-21 | 宁波工程学院 | A kind of ethamine clean-production system |
CN109251147A (en) * | 2018-10-22 | 2019-01-22 | 宁波工程学院 | The ethamine production system of boiler fly ash removal of impurities is provided in a kind of utilization for oneself |
Also Published As
Publication number | Publication date |
---|---|
GB2012757B (en) | 1982-08-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PCNP | Patent ceased through non-payment of renewal fee |