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GB1373230A - Process for producing terephthalic acid - Google Patents

Process for producing terephthalic acid

Info

Publication number
GB1373230A
GB1373230A GB5991871A GB5991871A GB1373230A GB 1373230 A GB1373230 A GB 1373230A GB 5991871 A GB5991871 A GB 5991871A GB 5991871 A GB5991871 A GB 5991871A GB 1373230 A GB1373230 A GB 1373230A
Authority
GB
United Kingdom
Prior art keywords
terephthalic acid
acetic acid
vapour
flashing
recycled
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5991871A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Petrochemical Industries Ltd
Original Assignee
Mitsui Petrochemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Petrochemical Industries Ltd filed Critical Mitsui Petrochemical Industries Ltd
Priority to GB5991871A priority Critical patent/GB1373230A/en
Publication of GB1373230A publication Critical patent/GB1373230A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1373230 Terephthalic acid MITSUI PETROCHEMICAL INDUSTRIES Ltd 23 Dec 1971 59918/71 Heading C2C In an otherwise known process for the production of terephthalic acid in which p-xylene is oxidized in the liquid phase in the presence of acetic acid with either molecular oxygen or a gas containing molecular oxygen and in the presence of a cobalt containing catalyst the improvement wherein the vapour effluent from the reactor, which contains a non-condensable gas, steam and acetic acid vapour, is fractionally distilled to recover acetic acid which is recycled to the reactor and terephthalic acid is crystallized and removed from the liquid reaction product the resultant mother liquor being recycled, without distillation, to the reaction. Crystallization of terephthalic acid may be achieved by cooling or by flashing the hot reaction product. The vapour obtained by flashing is an acetic acid solution which may be used to wash the crystalline product prior to drying.
GB5991871A 1971-12-23 1971-12-23 Process for producing terephthalic acid Expired GB1373230A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB5991871A GB1373230A (en) 1971-12-23 1971-12-23 Process for producing terephthalic acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB5991871A GB1373230A (en) 1971-12-23 1971-12-23 Process for producing terephthalic acid

Publications (1)

Publication Number Publication Date
GB1373230A true GB1373230A (en) 1974-11-06

Family

ID=10484650

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5991871A Expired GB1373230A (en) 1971-12-23 1971-12-23 Process for producing terephthalic acid

Country Status (1)

Country Link
GB (1) GB1373230A (en)

Cited By (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1992009551A1 (en) * 1990-11-29 1992-06-11 Eastman Kodak Company Continuous production of aromatic carboxylic acids
EP0498591A2 (en) * 1991-02-05 1992-08-12 Imperial Chemical Industries Plc Process for the production of terephthalic acid
US5463113A (en) * 1993-03-30 1995-10-31 Mitsui Petrochemicalindustries, Ltd. Process and apparatus for producing terephthalic acid
WO1999031038A1 (en) * 1997-12-15 1999-06-24 Shell Internationale Research Maatschappij B.V. Method to produce aromatic carboxylic acids
US6143925A (en) * 1998-06-05 2000-11-07 Mitsui Chemicals, Inc. Process for producing aromatic carboxylic acid
WO2002098833A1 (en) * 2001-06-04 2002-12-12 Eastman Chemical Company Process for production of aromatic carboxylic acids with improved water removal technique
US7005011B2 (en) * 2001-10-05 2006-02-28 Bp Corporation North America Inc. Method of removing iron oxide deposits from the surface of titanium components
WO2006028769A2 (en) * 2004-09-02 2006-03-16 Eastman Chemical Company Optimized liquid-phase oxidation of p-xylene
US7213540B2 (en) 2004-02-05 2007-05-08 Eastman Chemical Company Steam recompression in carboxylic acid processes
US7326808B2 (en) 2006-03-01 2008-02-05 Eastman Chemical Company Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system
US7393973B2 (en) 2006-03-01 2008-07-01 Eastman Chemical Company Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion
US7501537B2 (en) 2006-03-01 2009-03-10 Eastman Chemical Company Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange
US7659427B2 (en) 2004-09-02 2010-02-09 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7772424B2 (en) 2006-03-01 2010-08-10 Eastman Chemical Company Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion
US7816556B2 (en) 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7829037B2 (en) 2006-03-01 2010-11-09 Eastman Chemical Company Oxidation system with sidedraw secondary reactor
US7884232B2 (en) 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7902396B2 (en) 2004-09-02 2011-03-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7901636B2 (en) 2004-09-02 2011-03-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7910071B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7935844B2 (en) 2005-03-21 2011-05-03 Bp Corporation North America Inc. Recovery of energy during the production of aromatic carboxylic acids
US7960581B2 (en) 2004-09-02 2011-06-14 Grupo Petrotemex, S.A. De C.V. Optimized liquid-phase oxidation
US7977505B2 (en) 2004-09-02 2011-07-12 Eastman Chemical Company Optimized liquid-phase oxidation
US8114356B2 (en) 2004-09-02 2012-02-14 Grupo Pretrotemex, S.A. de C.V. Optimized liquid-phase oxidation
US8470257B2 (en) 2004-09-02 2013-06-25 Grupo Petrotemex, S.A. De C.V. Optimized liquid-phase oxidation
WO2015094911A1 (en) 2013-12-18 2015-06-25 Bp Corporation North America Inc. Improved process and apparatus for manufacturing aromatic carboxylic acids

Cited By (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1992009551A1 (en) * 1990-11-29 1992-06-11 Eastman Kodak Company Continuous production of aromatic carboxylic acids
EP0498591A2 (en) * 1991-02-05 1992-08-12 Imperial Chemical Industries Plc Process for the production of terephthalic acid
EP0498591A3 (en) * 1991-02-05 1993-01-27 Imperial Chemical Industries Plc Process for the production of terephthalic acid
US5304676A (en) * 1991-02-05 1994-04-19 Imperial Chemical Industries Plc Process for the production of terephthalic acid
USRE36008E (en) * 1991-02-05 1998-12-22 E. I. Du Pont De Nemours And Company Process for the production of terephthalic acid
US5463113A (en) * 1993-03-30 1995-10-31 Mitsui Petrochemicalindustries, Ltd. Process and apparatus for producing terephthalic acid
WO1999031038A1 (en) * 1997-12-15 1999-06-24 Shell Internationale Research Maatschappij B.V. Method to produce aromatic carboxylic acids
US6143925A (en) * 1998-06-05 2000-11-07 Mitsui Chemicals, Inc. Process for producing aromatic carboxylic acid
WO2002098833A1 (en) * 2001-06-04 2002-12-12 Eastman Chemical Company Process for production of aromatic carboxylic acids with improved water removal technique
US6504051B1 (en) 2001-06-04 2003-01-07 Eastman Chemical Company Process for production of aromatic carboxylic acids with improved water removal technique
US7005011B2 (en) * 2001-10-05 2006-02-28 Bp Corporation North America Inc. Method of removing iron oxide deposits from the surface of titanium components
US7213540B2 (en) 2004-02-05 2007-05-08 Eastman Chemical Company Steam recompression in carboxylic acid processes
US8470257B2 (en) 2004-09-02 2013-06-25 Grupo Petrotemex, S.A. De C.V. Optimized liquid-phase oxidation
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7910071B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
CN101056838B (en) * 2004-09-02 2012-08-08 奇派特石化有限公司 Optimized liquid-phase oxidation
US8178054B2 (en) 2004-09-02 2012-05-15 Grupo Petrotemex, S. A. DE C. V. Optimized liquid-phase oxidation
US7659427B2 (en) 2004-09-02 2010-02-09 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
WO2006028769A3 (en) * 2004-09-02 2006-05-04 Eastman Chem Co Optimized liquid-phase oxidation of p-xylene
WO2006028769A2 (en) * 2004-09-02 2006-03-16 Eastman Chemical Company Optimized liquid-phase oxidation of p-xylene
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US8114356B2 (en) 2004-09-02 2012-02-14 Grupo Pretrotemex, S.A. de C.V. Optimized liquid-phase oxidation
US7977505B2 (en) 2004-09-02 2011-07-12 Eastman Chemical Company Optimized liquid-phase oxidation
US7960581B2 (en) 2004-09-02 2011-06-14 Grupo Petrotemex, S.A. De C.V. Optimized liquid-phase oxidation
US7910769B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7902396B2 (en) 2004-09-02 2011-03-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7901636B2 (en) 2004-09-02 2011-03-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US8501986B2 (en) 2004-11-29 2013-08-06 Grupo Petrotemex, S.A. De C.V. Optimized liquid-phase oxidation
US7935844B2 (en) 2005-03-21 2011-05-03 Bp Corporation North America Inc. Recovery of energy during the production of aromatic carboxylic acids
US7935845B2 (en) 2005-03-21 2011-05-03 Bp Corporation North America Inc. Process and apparatus for manufacturing aromatic carboxylic acids including pure forms thereof
US8779185B2 (en) 2005-03-21 2014-07-15 Bp Corporation North America Inc. Process and apparatus for manufacturing pure forms of aromatic carboxylic acids
US8173834B2 (en) 2005-03-21 2012-05-08 Bp Corporation North America Inc. Process and apparatus for manufacturing pure forms of aromatic carboxylic acids
US7884232B2 (en) 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US8153840B2 (en) 2006-03-01 2012-04-10 Grupo Petrotemex, S.A. De C.V. Oxidation system with sidedraw secondary reactor
US7772424B2 (en) 2006-03-01 2010-08-10 Eastman Chemical Company Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion
US7501537B2 (en) 2006-03-01 2009-03-10 Eastman Chemical Company Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange
US7393973B2 (en) 2006-03-01 2008-07-01 Eastman Chemical Company Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion
US7326808B2 (en) 2006-03-01 2008-02-05 Eastman Chemical Company Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system
US7816556B2 (en) 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7829037B2 (en) 2006-03-01 2010-11-09 Eastman Chemical Company Oxidation system with sidedraw secondary reactor
WO2015094911A1 (en) 2013-12-18 2015-06-25 Bp Corporation North America Inc. Improved process and apparatus for manufacturing aromatic carboxylic acids

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Legal Events

Date Code Title Description
PS Patent sealed
PE20 Patent expired after termination of 20 years