GB1354565A - Process for the purification of adiponitrile - Google Patents
Process for the purification of adiponitrileInfo
- Publication number
- GB1354565A GB1354565A GB2948071A GB2948071A GB1354565A GB 1354565 A GB1354565 A GB 1354565A GB 2948071 A GB2948071 A GB 2948071A GB 2948071 A GB2948071 A GB 2948071A GB 1354565 A GB1354565 A GB 1354565A
- Authority
- GB
- United Kingdom
- Prior art keywords
- adiponitrile
- purification
- june
- weight
- iminocyanocyclopentane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1354565 Purification of adiponitrile RHONEPOULENC SA 23 June 1971 [24 June 1970] 29480/71 Heading C2C Adiponitrile is purified by contacting at a temperature of up to 50‹ C. inclusive with 0À1 to 5 times its weight of an aqueous solution containing 0À1 to 3% by weight of an inorganic or organic acid whose acidity constant pKa is not more than 5, and the adiponitrile is then separated from the aqueous layer by decantation and subsequently subjected to a fractional distillation. The acid may be, e.g. hydrochloric, sulphuric, nitric, orthophosphoric, acetic, benzoic or methane sulphonic and the impurity removed is typically iminocyanocyclopentane.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7023410A FR2094542A5 (en) | 1970-06-24 | 1970-06-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1354565A true GB1354565A (en) | 1974-06-05 |
Family
ID=9057732
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2948071A Expired GB1354565A (en) | 1970-06-24 | 1971-06-23 | Process for the purification of adiponitrile |
Country Status (8)
Country | Link |
---|---|
BE (1) | BE768943A (en) |
CS (1) | CS193463B2 (en) |
DE (1) | DE2131448A1 (en) |
FR (1) | FR2094542A5 (en) |
GB (1) | GB1354565A (en) |
LU (1) | LU63399A1 (en) |
NL (1) | NL7108281A (en) |
SU (1) | SU364161A3 (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6207851B1 (en) | 1996-09-10 | 2001-03-27 | Basf Aktiengesellschaft | Process for simultaneously preparing 6-aminocapronitrile and hexamethylene diamine |
CN112430196A (en) * | 2020-09-29 | 2021-03-02 | 瑞典国际化工技术有限公司 | Method and device for refining adiponitrile |
CN115215750A (en) * | 2022-07-26 | 2022-10-21 | 万华化学集团股份有限公司 | Preparation method of hexamethylene diamine |
-
1970
- 1970-06-24 FR FR7023410A patent/FR2094542A5/fr not_active Expired
-
1971
- 1971-05-12 SU SU1649987A patent/SU364161A3/ru active
- 1971-06-16 NL NL7108281A patent/NL7108281A/xx unknown
- 1971-06-22 LU LU63399D patent/LU63399A1/xx unknown
- 1971-06-22 CS CS461771A patent/CS193463B2/en unknown
- 1971-06-23 BE BE768943A patent/BE768943A/en unknown
- 1971-06-23 GB GB2948071A patent/GB1354565A/en not_active Expired
- 1971-06-24 DE DE19712131448 patent/DE2131448A1/en active Pending
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6207851B1 (en) | 1996-09-10 | 2001-03-27 | Basf Aktiengesellschaft | Process for simultaneously preparing 6-aminocapronitrile and hexamethylene diamine |
CN112430196A (en) * | 2020-09-29 | 2021-03-02 | 瑞典国际化工技术有限公司 | Method and device for refining adiponitrile |
CN115215750A (en) * | 2022-07-26 | 2022-10-21 | 万华化学集团股份有限公司 | Preparation method of hexamethylene diamine |
Also Published As
Publication number | Publication date |
---|---|
NL7108281A (en) | 1971-12-28 |
SU364161A3 (en) | 1972-12-25 |
LU63399A1 (en) | 1972-03-22 |
DE2131448A1 (en) | 1971-12-30 |
FR2094542A5 (en) | 1972-02-04 |
BE768943A (en) | 1971-12-23 |
CS193463B2 (en) | 1979-10-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |