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FR2419335A1 - PROCESS FOR DEPOSITING A COATING ON GLASS - Google Patents

PROCESS FOR DEPOSITING A COATING ON GLASS

Info

Publication number
FR2419335A1
FR2419335A1 FR7905492A FR7905492A FR2419335A1 FR 2419335 A1 FR2419335 A1 FR 2419335A1 FR 7905492 A FR7905492 A FR 7905492A FR 7905492 A FR7905492 A FR 7905492A FR 2419335 A1 FR2419335 A1 FR 2419335A1
Authority
FR
France
Prior art keywords
coating
mixture
reaction zone
gas mixture
substrate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7905492A
Other languages
French (fr)
Other versions
FR2419335B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US05/884,432 external-priority patent/US4206252A/en
Application filed by Individual filed Critical Individual
Publication of FR2419335A1 publication Critical patent/FR2419335A1/en
Application granted granted Critical
Publication of FR2419335B1 publication Critical patent/FR2419335B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
    • C03C17/3429—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials at least one of the coatings being a non-oxide coating
    • C03C17/3435—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials at least one of the coatings being a non-oxide coating comprising a nitride, oxynitride, boronitride or carbonitride
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/001—General methods for coating; Devices therefor
    • C03C17/002—General methods for coating; Devices therefor for flat glass, e.g. float glass
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C03C17/23—Oxides
    • C03C17/245—Oxides by deposition from the vapour phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
    • C03C17/3417—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials all coatings being oxide coatings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30—Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • C23C16/40—Oxides
    • C23C16/401—Oxides containing silicon
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/54—Apparatus specially adapted for continuous coating
    • C23C16/545—Apparatus specially adapted for continuous coating for coating elongated substrates
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/20—Materials for coating a single layer on glass
    • C03C2217/21—Oxides
    • C03C2217/211—SnO2
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/20—Materials for coating a single layer on glass
    • C03C2217/21—Oxides
    • C03C2217/229—Non-specific enumeration
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/10—Deposition methods
    • C03C2218/15—Deposition methods from the vapour phase
    • C03C2218/152—Deposition methods from the vapour phase by cvd
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/30—Aspects of methods for coating glass not covered above
    • C03C2218/36—Underside coating of a glass sheet

Landscapes

  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Surface Treatment Of Glass (AREA)
  • Chemical Vapour Deposition (AREA)
  • Laminated Bodies (AREA)

Abstract

Le procédé conforme à l'invention se caractérise en ce que : a) on fait circuler le mélange gazeux dans une zone de réaction définie par un trajet des composants réactifs contigu à, parallèle à, et limité par une surface de substrat; b) on dépose, de préférence, un produit de réaction provenant d'un composant plus réactif du mélange sur une partie de la surface venant plutôt en contact avec le mélange gazeux; c) on dépose, de préférence, un produit de réaction provenant d'un composant moins réactif du mélange sur une partie de la surface venant plus tard en contact avec le mélange gazeux; et, d) on déplace la surface du substrat dans la zone de réaction suivant une direction parallèle au trajet de circulation afin d'obtenir une variation de la composition du revêtement le long de l'épaisseur de celui-ci quand le substrat émerge de la zone de réaction.The process according to the invention is characterized in that: a) the gas mixture is circulated in a reaction zone defined by a path of the reactive components contiguous to, parallel to, and limited by a substrate surface; b) preferably depositing a reaction product originating from a more reactive component of the mixture on a part of the surface coming rather in contact with the gas mixture; c) preferably depositing a reaction product from a less reactive component of the mixture on a part of the surface which later comes into contact with the gas mixture; and, d) moving the surface of the substrate in the reaction zone in a direction parallel to the flow path in order to obtain a variation in the composition of the coating along the thickness thereof as the substrate emerges from the coating. reaction zone.

FR7905492A 1978-03-08 1979-03-02 PROCESS FOR DEPOSITING A COATING ON GLASS Granted FR2419335A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/884,432 US4206252A (en) 1977-04-04 1978-03-08 Deposition method for coating glass and the like

Publications (2)

Publication Number Publication Date
FR2419335A1 true FR2419335A1 (en) 1979-10-05
FR2419335B1 FR2419335B1 (en) 1985-03-22

Family

ID=25384616

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7905492A Granted FR2419335A1 (en) 1978-03-08 1979-03-02 PROCESS FOR DEPOSITING A COATING ON GLASS

Country Status (19)

Country Link
JP (2) JPS54127424A (en)
AR (1) AR216975A1 (en)
AU (1) AU526605B2 (en)
BE (1) BE874614A (en)
BR (1) BR7901379A (en)
CA (1) CA1134214A (en)
CH (1) CH638762A5 (en)
DE (1) DE2908412C2 (en)
DK (1) DK94879A (en)
ES (2) ES478393A1 (en)
FI (1) FI790781A (en)
FR (1) FR2419335A1 (en)
GB (1) GB2015983B (en)
IE (1) IE48228B1 (en)
IT (1) IT1119685B (en)
MX (1) MX151883A (en)
NL (1) NL7901875A (en)
NO (1) NO145947C (en)
SE (1) SE445449B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011101572A1 (en) 2010-02-22 2011-08-25 Saint-Gobain Glass France Glass substrate coated with layers having improved mechanical strength
WO2012017162A2 (en) 2010-07-19 2012-02-09 Saint-Gobain Glass France Transparent electrode for a high-yield photovoltaic cell
FR2983350A1 (en) * 2011-11-30 2013-05-31 Saint Gobain Transparent electrode for use in front face substrate of photovoltaic cell, has tin and silicon mixed oxide layer with specific thickness, and positioned between electroconducting layer and photovoltaic material

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4291167A (en) 1980-07-28 1981-09-22 Nalco Chemical Company Preparation of tetramethyldisilane from 1,2-tetramethyldichlorodisilane
JPS57100942A (en) * 1980-12-10 1982-06-23 Asahi Glass Co Ltd Substrate coated with silicon oxide
US4386117A (en) * 1981-11-20 1983-05-31 Gordon Roy G Coating process using alkoxy substituted silicon-bearing reactant
JPS58112375A (en) * 1981-12-25 1983-07-04 Fuji Electric Corp Res & Dev Ltd Manufacture of photovoltaic device
JPS58112374A (en) * 1981-12-25 1983-07-04 Fuji Electric Corp Res & Dev Ltd Manufacture of photovoltaic device
US4595634A (en) * 1983-08-01 1986-06-17 Gordon Roy G Coating process for making non-iridescent glass
GB8624825D0 (en) * 1986-10-16 1986-11-19 Glaverbel Vehicle windows
US5221352A (en) * 1989-06-19 1993-06-22 Glaverbel Apparatus for pyrolytically forming an oxide coating on a hot glass substrate
US5122391A (en) * 1991-03-13 1992-06-16 Watkins-Johnson Company Method for producing highly conductive and transparent films of tin and fluorine doped indium oxide by APCVD
CH690511A5 (en) * 1994-09-01 2000-09-29 Balzers Hochvakuum An optical component and method for manufacturing such.
DE4433206A1 (en) * 1994-09-17 1996-03-21 Goldschmidt Ag Th Process for the pyrolytic coating of glass, glass ceramic and enamel products
FR2736632B1 (en) * 1995-07-12 1997-10-24 Saint Gobain Vitrage GLAZING PROVIDED WITH A CONDUCTIVE AND / OR LOW-EMISSIVE LAYER
TW328971B (en) * 1995-10-30 1998-04-01 Dow Corning Method for depositing Si-O containing coatings
US5698262A (en) 1996-05-06 1997-12-16 Libbey-Owens-Ford Co. Method for forming tin oxide coating on glass
DE19624838A1 (en) * 1996-06-21 1998-01-08 Schueller Glasbeschichtung Gmb Insulating anti-reflective coating and process for its production
US6303523B2 (en) 1998-02-11 2001-10-16 Applied Materials, Inc. Plasma processes for depositing low dielectric constant films
US6287990B1 (en) 1998-02-11 2001-09-11 Applied Materials, Inc. CVD plasma assisted low dielectric constant films
US6054379A (en) 1998-02-11 2000-04-25 Applied Materials, Inc. Method of depositing a low k dielectric with organo silane
US6159871A (en) 1998-05-29 2000-12-12 Dow Corning Corporation Method for producing hydrogenated silicon oxycarbide films having low dielectric constant
US6667553B2 (en) 1998-05-29 2003-12-23 Dow Corning Corporation H:SiOC coated substrates
FR2787440B1 (en) * 1998-12-21 2001-12-07 Saint Gobain Vitrage TRANSPARENT SUBSTRATE HAVING AN ANTI-REFLECTIVE COATING
US6797388B1 (en) * 1999-03-18 2004-09-28 Ppg Industries Ohio, Inc. Methods of making low haze coatings and the coatings and coated articles made thereby
US6709721B2 (en) 2001-03-28 2004-03-23 Applied Materials Inc. Purge heater design and process development for the improvement of low k film properties
JP4924070B2 (en) * 2007-02-06 2012-04-25 ブラザー工業株式会社 Printing device
US8728634B2 (en) * 2007-06-13 2014-05-20 Ppg Industries Ohio, Inc. Appliance transparency
US20140227512A1 (en) * 2011-09-30 2014-08-14 Arkema Inc. Deposition of silicon oxide by atmospheric pressure chemical vapor deposition

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2962388A (en) * 1954-03-12 1960-11-29 Metallgesellschaft Ag Process for the production of titanium carbide coatings
FR1524729A (en) * 1966-05-27 1968-05-10 Dow Corning Method and apparatus for the continuous production of semiconductor materials
GB1115884A (en) * 1966-03-25 1968-05-29 Standard Telephones Cables Ltd Method for depositing on a substrate coherent solid layers
FR2274572A1 (en) * 1974-06-14 1976-01-09 Pilkington Brothers Ltd GLASS COATING IMPROVEMENTS

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE841625C (en) * 1942-02-01 1952-06-16 Leitz Ernst Gmbh Process for the production of reflection-reducing layers, e.g. B. on glass
DE742463C (en) * 1942-07-15 1944-01-18 Jenaer Glaswerk Schott & Gen Layer for changing the reflectivity from a plurality of alternately superimposed partial layers made of two substances with different refractive indices
US2602032A (en) * 1946-08-19 1952-07-01 Libbey Owens Ford Glass Co Electrically conducting surface and method for producing same
US2617745A (en) * 1951-12-19 1952-11-11 Pittsburgh Plate Glass Co Method of producing an electroconductive article
US3808035A (en) * 1970-12-09 1974-04-30 M Stelter Deposition of single or multiple layers on substrates from dilute gas sweep to produce optical components, electro-optical components, and the like
FR2210675B1 (en) * 1972-12-15 1978-05-12 Ppg Industries Inc
GB1507996A (en) * 1975-06-11 1978-04-19 Pilkington Brothers Ltd Coating glass
GB1524326A (en) * 1976-04-13 1978-09-13 Bfg Glassgroup Coating of glass

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2962388A (en) * 1954-03-12 1960-11-29 Metallgesellschaft Ag Process for the production of titanium carbide coatings
GB1115884A (en) * 1966-03-25 1968-05-29 Standard Telephones Cables Ltd Method for depositing on a substrate coherent solid layers
FR1524729A (en) * 1966-05-27 1968-05-10 Dow Corning Method and apparatus for the continuous production of semiconductor materials
FR2274572A1 (en) * 1974-06-14 1976-01-09 Pilkington Brothers Ltd GLASS COATING IMPROVEMENTS

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011101572A1 (en) 2010-02-22 2011-08-25 Saint-Gobain Glass France Glass substrate coated with layers having improved mechanical strength
WO2012017162A2 (en) 2010-07-19 2012-02-09 Saint-Gobain Glass France Transparent electrode for a high-yield photovoltaic cell
FR2983350A1 (en) * 2011-11-30 2013-05-31 Saint Gobain Transparent electrode for use in front face substrate of photovoltaic cell, has tin and silicon mixed oxide layer with specific thickness, and positioned between electroconducting layer and photovoltaic material

Also Published As

Publication number Publication date
NO145947C (en) 1982-06-30
IT7967488A0 (en) 1979-03-07
IE790235L (en) 1979-09-08
FI790781A (en) 1979-09-09
JPS62191448A (en) 1987-08-21
GB2015983B (en) 1983-02-02
CH638762A5 (en) 1983-10-14
IE48228B1 (en) 1984-11-14
AU526605B2 (en) 1983-01-20
SE7902052L (en) 1979-09-09
NL7901875A (en) 1979-09-11
JPS635343B2 (en) 1988-02-03
NO790762L (en) 1979-09-11
ES478393A1 (en) 1980-01-16
SE445449B (en) 1986-06-23
DE2908412A1 (en) 1979-09-20
NO145947B (en) 1982-03-22
JPS54127424A (en) 1979-10-03
FR2419335B1 (en) 1985-03-22
MX151883A (en) 1985-04-23
JPH0157061B2 (en) 1989-12-04
AU4401479A (en) 1979-09-20
GB2015983A (en) 1979-09-19
DK94879A (en) 1979-09-09
BE874614A (en) 1979-09-05
ES482440A1 (en) 1980-02-16
DE2908412C2 (en) 1994-01-27
BR7901379A (en) 1979-10-02
IT1119685B (en) 1986-03-10
CA1134214A (en) 1982-10-26
AR216975A1 (en) 1980-02-15

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