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ES2186551A1 - Procedure for the spontaneous resolution by direct crystallisation of racemic compounds. - Google Patents

Procedure for the spontaneous resolution by direct crystallisation of racemic compounds.

Info

Publication number
ES2186551A1
ES2186551A1 ES200101591A ES200101591A ES2186551A1 ES 2186551 A1 ES2186551 A1 ES 2186551A1 ES 200101591 A ES200101591 A ES 200101591A ES 200101591 A ES200101591 A ES 200101591A ES 2186551 A1 ES2186551 A1 ES 2186551A1
Authority
ES
Spain
Prior art keywords
procedure
racemic compounds
resolution
direct crystallisation
compounds
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES200101591A
Other languages
Spanish (es)
Other versions
ES2186551B1 (en
Inventor
Molero Cristobal Viedma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Universidad Complutense de Madrid
Original Assignee
Universidad Complutense de Madrid
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Universidad Complutense de Madrid filed Critical Universidad Complutense de Madrid
Priority to ES200101591A priority Critical patent/ES2186551B1/en
Publication of ES2186551A1 publication Critical patent/ES2186551A1/en
Application granted granted Critical
Publication of ES2186551B1 publication Critical patent/ES2186551B1/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)

Abstract

Procedure for the spontaneous resolution by direct crystallisation of racemic compounds. The procedure for the spontaneous resolution by direct crystallisation of racemic compounds consists of a technique through which the racemic compounds that normally cannot spontaneously crystallise at its two enantiomers, can do so without difficulty. The basis of this procedure is the mass transfer, by capillary action, in a porous medium that provides the appropriate conditions so that a solution of these compounds crystallise in its enantiomer phases. This avoids the traditional techniques that require biological treatments or chiral media, allowing, with our procedure, achievement of a resolution of the racemic compounds in its two enantiomer phases for industrially leveraging its peculiar physiochemical properties, in a quick, economical and easy manner.
ES200101591A 2001-07-06 2001-07-06 PROCEDURE FOR THE SPONTANEOUS RESOLUTION BY DIRECT CRYSTALLIZATION OF RACEMIC COMPOUNDS. Expired - Fee Related ES2186551B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
ES200101591A ES2186551B1 (en) 2001-07-06 2001-07-06 PROCEDURE FOR THE SPONTANEOUS RESOLUTION BY DIRECT CRYSTALLIZATION OF RACEMIC COMPOUNDS.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES200101591A ES2186551B1 (en) 2001-07-06 2001-07-06 PROCEDURE FOR THE SPONTANEOUS RESOLUTION BY DIRECT CRYSTALLIZATION OF RACEMIC COMPOUNDS.

Publications (2)

Publication Number Publication Date
ES2186551A1 true ES2186551A1 (en) 2003-05-01
ES2186551B1 ES2186551B1 (en) 2004-11-16

Family

ID=8498332

Family Applications (1)

Application Number Title Priority Date Filing Date
ES200101591A Expired - Fee Related ES2186551B1 (en) 2001-07-06 2001-07-06 PROCEDURE FOR THE SPONTANEOUS RESOLUTION BY DIRECT CRYSTALLIZATION OF RACEMIC COMPOUNDS.

Country Status (1)

Country Link
ES (1) ES2186551B1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2310131B1 (en) 2007-06-04 2009-12-04 INSTITUTO NACIONAL DE TECNICA AEROESPACIAL "ESTEBAN TERRADAS" CRYSTALLIZATION PROCEDURE FROM SOLUTION.

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB921075A (en) * 1961-07-21 1963-03-13 Ajinomoto Kk Process for optical resolution of racemic glutamic acid
EP0225503A1 (en) * 1985-11-12 1987-06-16 Yeda Research And Development Company Limited Resolution system

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB921075A (en) * 1961-07-21 1963-03-13 Ajinomoto Kk Process for optical resolution of racemic glutamic acid
EP0225503A1 (en) * 1985-11-12 1987-06-16 Yeda Research And Development Company Limited Resolution system

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MIZOGUCHI, N. Resolution of Racemic Glutamic Acid by Preferential Crystallization. I. Solubility, Supersaturation and Crystal Growth of Optically Active Glutamic Acid in Solutions Containing the Antipode. Nippon Nogei Kagaku Kaishi, 1967, 41 (11), pßginas 607-615. HCAPLUS, resumen, AN 1969:32319. *

Also Published As

Publication number Publication date
ES2186551B1 (en) 2004-11-16

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