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EP1038096A1 - Feuille metallique comportant des trous - Google Patents

Feuille metallique comportant des trous

Info

Publication number
EP1038096A1
EP1038096A1 EP98965782A EP98965782A EP1038096A1 EP 1038096 A1 EP1038096 A1 EP 1038096A1 EP 98965782 A EP98965782 A EP 98965782A EP 98965782 A EP98965782 A EP 98965782A EP 1038096 A1 EP1038096 A1 EP 1038096A1
Authority
EP
European Patent Office
Prior art keywords
structures
honeycomb body
opening
primary
body according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP98965782A
Other languages
German (de)
English (en)
Other versions
EP1038096B1 (fr
Inventor
Wolfgang Maus
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vitesco Technologies Lohmar Verwaltungs GmbH
Original Assignee
Emitec Gesellschaft fuer Emissionstechnologie mbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Emitec Gesellschaft fuer Emissionstechnologie mbH filed Critical Emitec Gesellschaft fuer Emissionstechnologie mbH
Publication of EP1038096A1 publication Critical patent/EP1038096A1/fr
Application granted granted Critical
Publication of EP1038096B1 publication Critical patent/EP1038096B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
    • F01N3/00—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust
    • F01N3/08—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous
    • F01N3/10—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by thermal or catalytic conversion of noxious components of exhaust
    • F01N3/24—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by thermal or catalytic conversion of noxious components of exhaust characterised by constructional aspects of converting apparatus
    • F01N3/28—Construction of catalytic reactors
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
    • F01N3/00—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust
    • F01N3/08—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous
    • F01N3/10—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by thermal or catalytic conversion of noxious components of exhaust
    • F01N3/24—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by thermal or catalytic conversion of noxious components of exhaust characterised by constructional aspects of converting apparatus
    • F01N3/28—Construction of catalytic reactors
    • F01N3/2803—Construction of catalytic reactors characterised by structure, by material or by manufacturing of catalyst support
    • F01N3/2807—Metal other than sintered metal
    • F01N3/281—Metallic honeycomb monoliths made of stacked or rolled sheets, foils or plates
    • F01N3/2821—Metallic honeycomb monoliths made of stacked or rolled sheets, foils or plates the support being provided with means to enhance the mixing process inside the converter, e.g. sheets, plates or foils with protrusions or projections to create turbulence
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional monoliths
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
    • F01N2330/00—Structure of catalyst support or particle filter
    • F01N2330/30—Honeycomb supports characterised by their structural details
    • F01N2330/32—Honeycomb supports characterised by their structural details characterised by the shape, form or number of corrugations of plates, sheets or foils
    • F01N2330/321—Honeycomb supports characterised by their structural details characterised by the shape, form or number of corrugations of plates, sheets or foils with two or more different kinds of corrugations in the same substrate
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
    • F01N2330/00—Structure of catalyst support or particle filter
    • F01N2330/30—Honeycomb supports characterised by their structural details
    • F01N2330/38—Honeycomb supports characterised by their structural details flow channels with means to enhance flow mixing,(e.g. protrusions or projections)
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/1234—Honeycomb, or with grain orientation or elongated elements in defined angular relationship in respective components [e.g., parallel, inter- secting, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/12361—All metal or with adjacent metals having aperture or cut
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/1241—Nonplanar uniform thickness or nonlinear uniform diameter [e.g., L-shape]

Definitions

  • the object of the invention relates to a flat structure and to a honeycomb body.
  • EP-0 454 712 B1 describes a flat structure which is formed from a metal foil.
  • the flat structure has at least two structures spaced apart from one another and at least partially overlapping.
  • the overlapping structures are designed in the form of grooves or grooves.
  • the structures have different dimensions.
  • One structure forms so-called macro structures.
  • the other structures form so-called microstructures.
  • the microstructures overlay the macrostructures.
  • EP-0 454 712 B1 also discloses a honeycomb body which has a plurality of channels through which a fluid can flow in a flow direction.
  • the honeycomb body is formed from at least one flat structure. The channels are limited by the structures of the flat structure.
  • a further embodiment of a flat structure which is particularly suitable for building a honeycomb body, is known from WO 96/09892.
  • the flat structure has partially overlapping structures. Macrostructures and microstructures are also provided for this flat structure.
  • the microstructures run at an angle to the macrostructures. From WO 96/09892 it can also be seen that the microstructures also cross. In particular, the microstructures cross on the wave crests of the macrostructures.
  • the flat structure according to WO 96/09892 consists of a metal foil into which the structures are introduced.
  • problem areas arise which lead to a high material stress on the structure during a forming process.
  • WO 96/09892 also describes a metallic honeycomb body with a plurality of channels made of metal foils through which a fluid can flow in a flow direction and which are at least partially provided with at least one macrostructure forming the channels, which determines the honeycomb shape of the metallic honeycomb body, part of which Sheets are provided with additional microstructures at least in partial areas, and the microstructures run at an angle to the direction of flow and follow one another at intervals, the microstructures crossing one another.
  • a flat structure which has structures.
  • the structures are in the form of webs which are pressed out in a bridge shape from a plane of the flat structure.
  • the webs are arranged next to one another in longitudinal and parallel zones.
  • the webs are protruding out of the plane of the metal foil on both sides.
  • the webs protruding on both sides are produced in that an initially flat metallic smooth band is passed through a pair of embossing cutting rollers through which the band is partially slotted and the webs on both sides of the plane of the Tape are pushed out.
  • the present invention has for its object to provide a flat structure which is easier to manufacture and process. Another object of the invention is to provide a honeycomb body that is easier to manufacture.
  • the flat structure according to the invention which has at least two partially overlapping structures spaced from a reference surface, is characterized in that at least one opening is provided which is formed in an area in which the structures overlap.
  • the structures overlap, for example by crossing or bumping into each other. In these areas, the flat structure is particularly stressed when the structures are produced if the structures are produced by a shaping process. Furthermore, folds, faults or the like can occur in the area of the superimposed structures. This is avoided by forming at least one opening in the area of the superimposed structures.
  • the opening is preferably formed by at least one slot.
  • an embodiment of the opening is preferred, in which at least two slots are provided, which meet, in particular cross, at an angle. This ensures optimal material utilization.
  • the opening be formed by at least one perforation.
  • the at least one opening is preferably introduced into the flat structure before the structures are formed.
  • the formation of the openings and the structures can be synchronized, so that the openings are always produced at a predetermined location of the flat structure.
  • the configuration of the flat structure according to the invention also enables structures which have a similar geometry to be superimposed, in particular if they form relatively large structures within the flat structure, since the perforation removes the possible problem zone before the forming process.
  • a flat structure which has at least two structures spaced apart from one another and at least partially overlapping.
  • the flat structure has at least one opening which is formed in an area in which the overlapping structures have a common one have a theoretical maximum height in relation to the reference surface that is greater than a maximum height of at least one structure in this area.
  • the entire edge of the opening lies at a level related to the reference height, which is smaller than the theoretical maximum height.
  • the distance of the edge of the opening to the reference surface preferably corresponds to the height of the superimposed structure.
  • the flat structure have structures that are essentially wave-shaped.
  • the wavy structures can intersect at an angle, for example.
  • the structure as a whole can assume a wavy configuration, it can be wound due to the perforations within the respective structural surfaces.
  • the wavy structures can also meet at an angle.
  • further processing of the planar structure is simplified by the formation of the openings in the superimposition area of the structures.
  • structures of different cross-sectional geometry can be formed.
  • the configuration of a structure which has an essentially V-shaped cross section is preferred.
  • the perforations also make it possible to form structures which have different geometries when viewed in a longitudinal direction of the structure and / or shape, the opening being formed between two adjacent, different structures.
  • the structures can also be designed such that they have a longitudinal extension, the structures having at least two adjacent longitudinal sections which are directed essentially perpendicularly in the opposite direction to the reference surface. In this way, a simpler, opposite curl of the flat structure can be achieved.
  • a flat structure in which at least one structure forms a primary structure and at least one structure forms a secondary structure, the primary structure having a larger amplitude than the secondary structure.
  • the primary structure can be a macro structure.
  • the secondary structure can be a so-called micro structure.
  • An embodiment of the flat structure is preferred in which secondary structures overlap on the primary structures.
  • secondary structures overlap, in particular cross, on a wave crest or in the wave trough of the primary structures.
  • the flat structure preferably consists of a metallic material.
  • the flat structure can be designed, for example, like a net.
  • a flat structure which is formed by a metal foil is preferred.
  • a honeycomb body with a plurality of channels through which a fluid can flow in a flow direction is proposed.
  • the honeycomb body is formed by at least one flat structure. It has at least two structures which are spaced apart from one another and at least partially overlapping and which form the Limit channels.
  • the honeycomb body is characterized in that at least one opening is provided in at least one area in which the structures overlap. The formation of the opening ensures that the honeycomb body is easier to manufacture, because where structures at least partially overlap, the structure is given a certain elasticity by the at least one opening, which makes it possible, for example, to form the honeycomb body by spirally winding the structure.
  • a further advantage of the configuration can be seen in the fact that the structures in the areas in which the structures overlap are not exposed to increased mechanical stress during the production of the structures.
  • the opening is preferably formed by at least one slot.
  • the openings are expediently formed by a plurality of slots which meet at an angle, in particular intersect, at one another.
  • the opening can also be designed in the form of at least one perforation.
  • a honeycomb body with a plurality of channels through which a fluid can flow in a flow direction which has at least one flat surface
  • the honeycomb body is characterized in that at least one opening is provided, which is formed in an area in which the superimposed structures have a common theoretical maximum height in relation to the reference surface, which is greater than a height of at least one structure therein
  • the honeycomb body has the advantage that layers of the structure lie better against one another, since the tips formed by the superimposition of the structures, as are known, for example, from WO 96/09892, are eliminated.
  • the honeycomb body is configured as a metallic honeycomb body, in which the flat structures are formed by metal foils, simplified soldering of the metal foils to one another and / or to a metal tube is also achieved.
  • the opening also opens up a possibility of connecting the structures by means of suitable connecting means, for example pins, the connecting means extending through the openings. This can also be achieved in an embodiment of the honeycomb body according to claim 15.
  • the honeycomb body is preferably designed such that the structures are essentially undulating.
  • At least one structure form a primary structure and at least one structure form a secondary structure, the primary structure having a larger amplitude than the secondary structure.
  • the structures are preferably designed such that the secondary structures overlap on the primary structures.
  • the superimposition of the secondary structures takes place on the wave crests of the primary structures or in wave troughs of the primary structures.
  • the primary structure forms a macro structure
  • the secondary structure forms a micro structure.
  • it be formed by alternating layers of smooth and structured structures, the structured structures having a primary structure and possibly a secondary structure.
  • the honeycomb body be formed by alternating layers of smooth and structured structures, the smooth structures having a secondary structure.
  • the structure consists at least partially of a metallic material.
  • the structure be a metal foil.
  • FIG. 3 is a plan view of the metal foil according to FIG. 2,
  • 5 is a metal foil with structures and a smooth sheet
  • 6 is a front view of a metal foil with a structure between two smooth sheets
  • FIG. 7 is a plan view of the metal foil with a structure according to FIG. 6.
  • FIG. 1 shows schematically and in perspective a metal foil 1 with structures 3, 4.
  • the structures 3, 4 are formed at a distance from a reference surface 2.
  • the reference surface 2 is formed essentially parallel to the metal foil 1 in the unstructured state.
  • the reference surface 2 is shown in dashed lines in FIG. 1. I.
  • the structures 3, 4 have an essentially rectangular cross section.
  • Other cross sections are possible.
  • the configuration of the cross section can be designed according to the requirements for the metal foil 1.
  • the invention proposes that an opening (not shown) be formed in the region 5.
  • the opening is preferably dimensioned such that it corresponds at least to the area 5, so that the edges 7 lying between the structures 3, 4 are removed, as a result of which the structures 3, 4 are not connected to one another.
  • FIG. 2 shows a metal foil 1 with structures 3, 4 which are essentially V-shaped in cross section.
  • the structures have a longitudinal extension.
  • an opening 6 is formed through which structures 3, 4 have essentially no common edge.
  • FIGS. 1 and 2 have an essentially identical cross section.
  • FIGS. 4 and 5 show metal foils 8, 9 which have primary structures 10, 11.
  • the structures 10, 11 form an essentially corrugated metal foil 8 or 9.
  • the structures 10, 11 together with a smooth metal foil 12 delimit channels 13 through which a fluid flows in the direction R through the channels 13.
  • the metal foil 8 is further provided with a secondary structure 14.
  • the secondary structure 14 is intersecting strip-shaped embossments in the metal foil 8.
  • the amplitude of the secondary structures 14 is smaller than the amplitude of the primary structures 10, 11.
  • the secondary structures 14 intersect on wave crests 15 Primary structures 10, 11. Openings 16 are formed in the area of the intersections of the secondary structures 14.
  • FIG. 5 shows a modification of the arrangement of the structured metal foil and a smooth metal foil 12 shown in FIG. 4.
  • the metal foil 9 differs from the metal foil 8 shown in FIG. 4 in that the secondary structures 14 are not only on the wave crests 15 but also cross in the trough 17 and on the flanks 18 of the primary structures.
  • the intersecting secondary structures are formed at an angle to the flow direction R of a fluid F. Openings 16 are formed in the intersection areas or overlay areas of the secondary structures 14, so that the secondary structures 14 do not have a common connecting edge.
  • the embodiments and arrangements of the metal foils shown in FIGS. 4 and 5 can form part of a metallic honeycomb body.
  • FIG. 6 shows an arrangement of a structured metal foil 21 between two smooth metal foils 22, 23.
  • the structured metal foil 21 has a primary structure 19 and a secondary structure 20 which extends essentially transversely to the longitudinal extent of the primary structure 19.
  • a part of the primary structure 19 and of the secondary structure 20 has been removed by means of a punch-out which forms an opening 24.
  • the course of the secondary structure 20 before the punching out process is shown in broken lines in FIG. 6.
  • the opening 24 is formed in an area 5 in which the overlapping structures 19, 20 have a common theoretical height H with respect to a reference surface 2 which is greater than a height h of the structure 19 in the area 5.
  • the opening 24 has an edge 25 whose distance A from the reference surface 2 is smaller than the theoretical height H.
  • the metal foil 22 lies in the area 5 of the opening 24 on the wall of the primary structure 19 and the secondary structure 20, as a result of which there is good contact between the smooth metal foil 22 and the structured metal foil 21, which is particularly useful for forming a soldered connection between the structured metal foil 21 and the smooth metal foil 22 is suitable.
  • the configurations of the metal foils 8, 9 shown in FIGS. 4 and 5 also enable a good connection to a smooth metal foil arranged thereon.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Toxicology (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Exhaust Gas After Treatment (AREA)
  • Laminated Bodies (AREA)
  • Catalysts (AREA)

Abstract

L'invention concerne, entre autres, un produit plat qui présente au moins deux structures (10, 11, 14) se trouvant à une certaine distance d'une surface de référence et se recouvrant partiellement. Dans une zone (5) dans laquelle les structures (10, 11, 14) se recouvrent est formé un trou (16).
EP98965782A 1997-12-12 1998-12-08 Feuille metallique comportant des trous Expired - Lifetime EP1038096B1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19755354A DE19755354A1 (de) 1997-12-12 1997-12-12 Metallfolie mit Durchbrechungen
DE19755354 1997-12-12
PCT/EP1998/007954 WO1999031362A1 (fr) 1997-12-12 1998-12-08 Feuille metallique comportant des trous

Publications (2)

Publication Number Publication Date
EP1038096A1 true EP1038096A1 (fr) 2000-09-27
EP1038096B1 EP1038096B1 (fr) 2004-03-17

Family

ID=7851746

Family Applications (1)

Application Number Title Priority Date Filing Date
EP98965782A Expired - Lifetime EP1038096B1 (fr) 1997-12-12 1998-12-08 Feuille metallique comportant des trous

Country Status (10)

Country Link
US (1) US6316121B1 (fr)
EP (1) EP1038096B1 (fr)
JP (1) JP2002508469A (fr)
KR (1) KR100528356B1 (fr)
CN (1) CN1107789C (fr)
AU (1) AU2159299A (fr)
DE (2) DE19755354A1 (fr)
PL (1) PL193856B1 (fr)
RU (1) RU2213231C2 (fr)
WO (1) WO1999031362A1 (fr)

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DE10162161A1 (de) 2001-12-17 2003-07-03 Emitec Emissionstechnologie Vorrichtung und Verfahren zur Schalldämpfung im Abgassystem einer Verbrennungskraftmaschine
DE10235767C1 (de) * 2002-08-02 2003-12-04 Emitec Emissionstechnologie Blechlage mit Bereichen unterschiedlicher Materialdicke, Verfahren zur Herstellung einer solchen Blechlage und aus solchen Blechlagen hergestellter Wabenkörper
EP1525378B1 (fr) 2002-08-02 2008-08-13 Emitec Gesellschaft für Emissionstechnologie mbH Couche metallique a parties presentant des epaisseurs de materiau differentes, son procede de production et corps en nid d'abeille produits au moins partiellement a partir desdites couches metalliques
DE10242869B4 (de) * 2002-09-17 2013-08-22 Andreas Stihl Ag & Co. Katalysator
US20050054526A1 (en) * 2003-09-08 2005-03-10 Engelhard Corporation Coated substrate and process of preparation thereof
US7340888B2 (en) * 2005-04-26 2008-03-11 Donaldson Company, Inc. Diesel particulate matter reduction system
WO2007032825A1 (fr) * 2005-08-05 2007-03-22 Engelhard Corporation Article d'echappement des diesels et compositions catalytiques afferentes
US7862640B2 (en) 2006-03-21 2011-01-04 Donaldson Company, Inc. Low temperature diesel particulate matter reduction system
DE102008030754A1 (de) * 2008-06-27 2009-12-31 Emitec Gesellschaft Für Emissionstechnologie Mbh Abgasbehandlungseinheit mit Metallfolien geringer Materialdicke
US8468803B2 (en) 2011-02-26 2013-06-25 International Engine Intellectual Property Company, Llc Soot resistant diesel fuel reformer for diesel engine emissions aftertreatment

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Also Published As

Publication number Publication date
DE19755354A1 (de) 1999-06-17
US6316121B1 (en) 2001-11-13
JP2002508469A (ja) 2002-03-19
CN1107789C (zh) 2003-05-07
KR100528356B1 (ko) 2005-11-15
EP1038096B1 (fr) 2004-03-17
KR20010033060A (ko) 2001-04-25
DE59811018D1 (de) 2004-04-22
WO1999031362A1 (fr) 1999-06-24
CN1281529A (zh) 2001-01-24
PL341477A1 (en) 2001-04-23
RU2213231C2 (ru) 2003-09-27
AU2159299A (en) 1999-07-05
PL193856B1 (pl) 2007-03-30

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