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EP0364881A3 - Process for preparing granules containing surface-active agents - Google Patents

Process for preparing granules containing surface-active agents Download PDF

Info

Publication number
EP0364881A3
EP0364881A3 EP89118962A EP89118962A EP0364881A3 EP 0364881 A3 EP0364881 A3 EP 0364881A3 EP 89118962 A EP89118962 A EP 89118962A EP 89118962 A EP89118962 A EP 89118962A EP 0364881 A3 EP0364881 A3 EP 0364881A3
Authority
EP
European Patent Office
Prior art keywords
water
insoluble solids
soluble
granulates
ionic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP89118962A
Other languages
German (de)
French (fr)
Other versions
EP0364881A2 (en
Inventor
Elmar Dr. Wilms
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of EP0364881A2 publication Critical patent/EP0364881A2/en
Publication of EP0364881A3 publication Critical patent/EP0364881A3/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065—High-density particulate detergent compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/128—Aluminium silicates, e.g. zeolites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Medicinal Preparation (AREA)
  • Superconductors And Manufacturing Methods Therefor (AREA)
  • Cosmetics (AREA)
  • Glanulating (AREA)
  • Colloid Chemistry (AREA)

Abstract

A process for manufacturing pourable granulates with an apparent density of 650 to 1000 g/l containing non-ionic tensides from the class of polyglycol ether derivatives as well as fine-particle, water-soluble and/or water-insoluble solids and water comprises a first mixing step (A) in which the non-ionic tenside is mixed with water, which may contain a fraction less than 50 wt.% of the total amount of water-soluble or water-insoluble solids in dissolved or dispersed form, to form a viscous gel phase. In a second mixing step (B), the remaining larger fraction of the water-soluble or water-insoluble solids is added in solid powder form and the mixture is processed until granulates are formed and a maximum apparent density is reached. The weight ratio of non-ionic tenside and water in the gel phase to the total solids present referred to the anhydrous substance lies between 25:75 and 65:35. Zeolites and bentonites are particularly suitable as water-insoluble solids.
EP89118962A 1988-10-21 1989-10-12 Process for preparing granules containing surface-active agents Pending EP0364881A3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3835918 1988-10-21
DE3835918A DE3835918A1 (en) 1988-10-21 1988-10-21 METHOD FOR PRODUCING TENSIDE CONTAINING GRANULES

Publications (2)

Publication Number Publication Date
EP0364881A2 EP0364881A2 (en) 1990-04-25
EP0364881A3 true EP0364881A3 (en) 1990-06-06

Family

ID=6365638

Family Applications (2)

Application Number Title Priority Date Filing Date
EP89118962A Pending EP0364881A3 (en) 1988-10-21 1989-10-12 Process for preparing granules containing surface-active agents
EP89911804A Expired - Lifetime EP0536110B1 (en) 1988-10-21 1989-10-12 Process for manufacturing tenside-containing granulates

Family Applications After (1)

Application Number Title Priority Date Filing Date
EP89911804A Expired - Lifetime EP0536110B1 (en) 1988-10-21 1989-10-12 Process for manufacturing tenside-containing granulates

Country Status (11)

Country Link
US (1) US5354493A (en)
EP (2) EP0364881A3 (en)
JP (1) JP2704020B2 (en)
KR (1) KR970001224B1 (en)
AT (1) ATE117718T1 (en)
DE (2) DE3835918A1 (en)
DK (1) DK71791D0 (en)
ES (1) ES2067569T3 (en)
PT (1) PT92060A (en)
TR (1) TR24142A (en)
WO (1) WO1990004629A2 (en)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3943019A1 (en) * 1989-12-27 1991-07-04 Henkel Kgaa GRANULAR, AVIVATING ACTIVITY OF DETERGENT ADDITIVE AND METHOD FOR THE PRODUCTION THEREOF
KR0170424B1 (en) * 1990-07-05 1999-01-15 호르스트 헤를레,요한 글라슬 Process for making washing and cleaning active tensile granulates
US5108646A (en) * 1990-10-26 1992-04-28 The Procter & Gamble Company Process for agglomerating aluminosilicate or layered silicate detergent builders
DE4110510A1 (en) * 1991-03-30 1992-10-01 Henkel Kgaa LOW-ALKALINE, CHLORINE AND PHOSPHATE-FREE MACHINE DISTRIBUTORS IN THE FORM OF HEAVY-DENTAL POWDERS AND GRANULES
DE4127323A1 (en) * 1991-08-20 1993-02-25 Henkel Kgaa METHOD FOR PRODUCING TENSIDE GRANULES
DE4137470A1 (en) * 1991-11-14 1993-05-19 Henkel Kgaa METHOD FOR PRODUCING LOW-ALKALINE, ACTIVE-CHLORINE AND PHOSPHATE-FREE MACHINE DISPERSIVE AGENTS IN THE FORM OF HEAVY GRANULES
CA2083331C (en) * 1991-11-26 1998-08-11 Johannes H. M. Akkermans Detergent compositions
DE4203789A1 (en) * 1992-02-10 1993-08-12 Henkel Kgaa METHOD FOR STABILIZING AQUEOUS ZEOLITE SUSPENSIONS
DE4216629A1 (en) * 1992-05-20 1993-11-25 Henkel Kgaa Process for the production of detergents and cleaning agents containing anionic surfactants
EP0622454A1 (en) * 1993-04-30 1994-11-02 The Procter & Gamble Company Structuring liquid nonionic surfactants prior to granulation process
ES2140498T3 (en) * 1993-09-13 2000-03-01 Procter & Gamble GRANULAR DETERGENT COMPOSITIONS COMPRISING A NON-IONIC SURFACTANT AND PROCEDURE FOR PREPARING SUCH COMPOSITIONS.
GB9324129D0 (en) * 1993-11-24 1994-01-12 Unilever Plc Detergent compositions and process for preparing them
US5496486A (en) * 1994-06-30 1996-03-05 Amway Corporation Process for increasing liquid surfactant loading in free flowing powder detergents
EP0694608A1 (en) * 1994-07-28 1996-01-31 The Procter & Gamble Company Process for making granular detergents and detergent compositions comprising nonionic surfactant
TW326472B (en) * 1994-08-12 1998-02-11 Kao Corp Method for producing nonionic detergent granules
WO1996025482A1 (en) * 1995-02-13 1996-08-22 The Procter & Gamble Company Process for producing detergent agglomerates in which particle size is controlled
US5574005A (en) * 1995-03-07 1996-11-12 The Procter & Gamble Company Process for producing detergent agglomerates from high active surfactant pastes having non-linear viscoelastic properties
US5888419A (en) * 1995-06-07 1999-03-30 The Clorox Company Granular N-alkyl ammonium acetontrile compositions
GB9513327D0 (en) * 1995-06-30 1995-09-06 Uniliver Plc Process for the production of a detergent composition
DE19603760A1 (en) * 1996-02-02 1997-08-07 Henkel Kgaa Solid detergent preparations
GB9605534D0 (en) * 1996-03-15 1996-05-15 Unilever Plc Detergent compositions
GB9711356D0 (en) † 1997-05-30 1997-07-30 Unilever Plc Particulate detergent composition
US7625855B2 (en) * 1999-08-11 2009-12-01 Gonzalez Gustavo M Cleaning compositions for removing organic deposits in hard to reach surfaces
US6057280A (en) 1998-11-19 2000-05-02 Huish Detergents, Inc. Compositions containing α-sulfofatty acid esters and methods of making and using the same
DE19913995A1 (en) 1999-03-29 2000-10-05 Basf Ag Process for the preparation of granular N-alkylamonium acetonitrile salts
DE10008815A1 (en) * 2000-02-25 2001-08-30 Sued Chemie Ag Agglomerates containing layered minerals with non-ionic surfactants
CN108837784A (en) * 2018-06-07 2018-11-20 曾婧 A kind of improved method for producing detergent composition particle

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2369341A1 (en) * 1976-11-02 1978-05-26 Albright & Wilson PROCESS FOR OBTAINING A SOLID POWDERED DETERGENT CONTAINING AN ALCOHOL ALCOHOL
DE2837504A1 (en) * 1978-08-28 1980-03-20 Henkel Kgaa Pourable nonionic surfactant compsn. prodn. - by premixing fatty alcohol condensate with propylene oxide and ethylene oxide with e.g. builder salt
EP0028432B1 (en) * 1979-11-03 1984-01-18 THE PROCTER & GAMBLE COMPANY Granular laundry compositions

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2874123A (en) * 1954-09-07 1959-02-17 Colgate Palmolive Co Process for the preparation of granular compositions
US3769222A (en) * 1971-02-09 1973-10-30 Colgate Palmolive Co Free flowing nonionic surfactants
ZA734721B (en) 1972-07-14 1974-03-27 Procter & Gamble Detergent compositions
AT330930B (en) 1973-04-13 1976-07-26 Henkel & Cie Gmbh PROCESS FOR THE PRODUCTION OF SOLID, SPILLABLE DETERGENTS OR CLEANING AGENTS WITH A CONTENT OF CALCIUM BINDING SUBSTANCES
US4166039A (en) * 1973-10-15 1979-08-28 The Proctor & Gamble Company Detergent composition and process
AT335035B (en) * 1974-10-10 1977-02-25 Henkel & Cie Gmbh STABLE SUSPENSIONS OF WATER-INSOLUBLE, SILICATES CAPABLE OF BINDING CALCIUMIONS AND THEIR USE FOR THE MANUFACTURE OF DETERGENTS AND DETERGENTS
US4169075A (en) * 1974-10-10 1979-09-25 Henkel Kommanditgesellschaft Auf Aktien Process for the production of powdery washing agents by spray-drying
DE3069768D1 (en) * 1979-09-29 1985-01-17 Procter & Gamble Ltd Detergent compositions
AU549000B2 (en) 1981-02-26 1986-01-09 Colgate-Palmolive Pty. Ltd. Base beads for detergent compositions
GB8329880D0 (en) 1983-11-09 1983-12-14 Unilever Plc Particulate adjuncts
DE3444311A1 (en) * 1984-12-05 1986-06-05 Degussa Ag, 6000 Frankfurt AQUEOUS, STABLE SUSPENSION OF WATER-INSOLUBLE SILICATES CAPABLE OF CALCIUMIONS AND THE USE THEREOF FOR THE PRODUCTION OF DETERGENT AND CLEANING AGENTS
DE3444960A1 (en) * 1984-12-10 1986-06-12 Henkel KGaA, 4000 Düsseldorf GRAINY ADSORPTION
US4970017A (en) * 1985-04-25 1990-11-13 Lion Corporation Process for production of granular detergent composition having high bulk density
DE3526405A1 (en) * 1985-07-24 1987-02-05 Henkel Kgaa LAYERED SILICATES WITH RESTRICTED SOURCE, PROCESS FOR THEIR PRODUCTION AND THEIR USE IN DETERGENT AND CLEANING AGENTS
US4894117A (en) * 1988-04-28 1990-01-16 Colgate-Palmolive Company Process for manufacturing high bulk density particulate fabric softening synthetic anionic organic detergent compositions
US4925585A (en) * 1988-06-29 1990-05-15 The Procter & Gamble Company Detergent granules from cold dough using fine dispersion granulation

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2369341A1 (en) * 1976-11-02 1978-05-26 Albright & Wilson PROCESS FOR OBTAINING A SOLID POWDERED DETERGENT CONTAINING AN ALCOHOL ALCOHOL
DE2837504A1 (en) * 1978-08-28 1980-03-20 Henkel Kgaa Pourable nonionic surfactant compsn. prodn. - by premixing fatty alcohol condensate with propylene oxide and ethylene oxide with e.g. builder salt
EP0028432B1 (en) * 1979-11-03 1984-01-18 THE PROCTER & GAMBLE COMPANY Granular laundry compositions

Also Published As

Publication number Publication date
DK71791A (en) 1991-04-19
WO1990004629A2 (en) 1990-05-03
EP0536110B1 (en) 1995-01-25
ATE117718T1 (en) 1995-02-15
KR900701988A (en) 1990-12-05
US5354493A (en) 1994-10-11
JPH04501129A (en) 1992-02-27
DE58908952D1 (en) 1995-03-09
PT92060A (en) 1990-04-30
KR970001224B1 (en) 1997-02-04
WO1990004629A3 (en) 1991-05-30
JP2704020B2 (en) 1998-01-26
DE3835918A1 (en) 1990-04-26
ES2067569T3 (en) 1995-04-01
TR24142A (en) 1991-04-09
EP0364881A2 (en) 1990-04-25
EP0536110A1 (en) 1993-04-14
DK71791D0 (en) 1991-04-19

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XX Miscellaneous (additional remarks)

Free format text: VERFAHREN ABGESCHLOSSEN INFOLGE VERBINDUNG MIT 89911804.6/0536110 (EUROPAEISCHE ANMELDENUMMER/VEROEFFENTLICHUNGSNUMMER) VOM 22.06.93.