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CN220933400U - A pipeline reactor pressure control device - Google Patents

A pipeline reactor pressure control device Download PDF

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Publication number
CN220933400U
CN220933400U CN202322697404.8U CN202322697404U CN220933400U CN 220933400 U CN220933400 U CN 220933400U CN 202322697404 U CN202322697404 U CN 202322697404U CN 220933400 U CN220933400 U CN 220933400U
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cooling
pipe
connecting pipe
control device
pressure control
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李永富
沈连芳
费强
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Sichuan Huanan Inorganic Salts Co ltd
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Sichuan Huanan Inorganic Salts Co ltd
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Abstract

本实用新型涉及气压调节装置的技术领域,提供了一种管道反应器压力控制装置,包括与反应器上侧连接的第一连接管,与第一连接管连接的第二连接管,与第二连接管连接的压力罐,与压力罐连接的压力检测装置,以及与压力罐连接的泄压装置;压力罐的直径大于第二连接管的直径。本实用新型的管道反应器压力控制装置,其不仅能够很好地调节反应过程的气压,还能够减少反应液被带出所造成的影响。

The utility model relates to the technical field of gas pressure regulating devices, and provides a pipeline reactor pressure control device, comprising a first connecting pipe connected to the upper side of the reactor, a second connecting pipe connected to the first connecting pipe, a pressure tank connected to the second connecting pipe, a pressure detection device connected to the pressure tank, and a pressure relief device connected to the pressure tank; the diameter of the pressure tank is greater than the diameter of the second connecting pipe. The pipeline reactor pressure control device of the utility model can not only well regulate the gas pressure of the reaction process, but also reduce the impact caused by the reaction liquid being carried out.

Description

一种管道反应器压力控制装置A pipeline reactor pressure control device

技术领域Technical Field

本实用新型涉及气压调节装置的技术领域,具体而言,涉及一种管道反应器压力控制装置。The utility model relates to the technical field of air pressure regulating devices, in particular to a pipeline reactor pressure control device.

背景技术Background technique

在化工生产中,对反应过程压力(气压)的控制是其中比较关键的环节,其不仅能够保证反应的正常进行,也能够保证生产设备的安全稳定运行。In chemical production, the control of reaction process pressure (gas pressure) is a key link, which not only ensures the normal progress of the reaction, but also ensures the safe and stable operation of production equipment.

对于一些在溶液中发生的生化反应,有些可能会在反应过程中产生大量的气体,如对硝基苯甲酸的生产过程中,会产生大量的一氧化氮气体,而生产过程中的压力需要控制在2MPa左右,因此需要及时对气压进行检测,并将多余的气体排出(对于连续式反应来说,存在一边进料,一边排料的情况)。For some biochemical reactions that occur in solutions, a large amount of gas may be produced during the reaction. For example, a large amount of nitric oxide gas will be produced during the production of p-nitrobenzoic acid, and the pressure in the production process needs to be controlled at around 2MPa. Therefore, the gas pressure needs to be tested in time and the excess gas needs to be discharged (for continuous reactions, there is a situation where the material is fed and discharged at the same time).

传统的气压控制,一般都是通过设置泄压管或泄压阀,放检测到气压过高时,通过管道或阀门将多余的气体排出,然而当气体突然产生,突然排出的时候,快速喷出的气体会带走一部分反应液,而反应液中的酸(或碱)浓度较高,这样不仅会损失一部分原料,还会对装置的其他部分造成不必要的腐蚀等情况。Traditional gas pressure control is generally achieved by setting up a pressure relief pipe or a pressure relief valve. When the gas pressure is detected to be too high, the excess gas is discharged through the pipe or valve. However, when the gas is suddenly generated and discharged, the rapidly ejected gas will take away a part of the reaction liquid, and the acid (or alkali) concentration in the reaction liquid is relatively high. This will not only cause the loss of part of the raw materials, but also cause unnecessary corrosion to other parts of the device.

实用新型内容Utility Model Content

本实用新型的目的在于提供一种管道反应器压力控制装置,其不仅能够很好地调节反应过程的气压,还能够减少反应液被带出所造成的影响。The utility model aims to provide a pipeline reactor pressure control device, which can not only well regulate the gas pressure of the reaction process, but also reduce the influence caused by the reaction liquid being carried out.

本实用新型的实施例通过以下技术方案实现:本实用新型的管道反应器压力控制装置,包括与反应器上侧连接的第一连接管,与所述第一连接管连接的第二连接管,与所述第二连接管连接的压力罐,与所述压力罐连接的压力检测装置,以及与所述压力罐连接的泄压装置;所述压力罐的直径大于所述第二连接管的直径。The embodiment of the utility model is realized through the following technical scheme: the pipeline reactor pressure control device of the utility model includes a first connecting pipe connected to the upper side of the reactor, a second connecting pipe connected to the first connecting pipe, a pressure tank connected to the second connecting pipe, a pressure detection device connected to the pressure tank, and a pressure relief device connected to the pressure tank; the diameter of the pressure tank is larger than the diameter of the second connecting pipe.

进一步地,所述第一连接管与所述第二连接管可拆卸连接。Furthermore, the first connecting pipe and the second connecting pipe are detachably connected.

进一步地,所述压力罐内部下端设有冷却腔,所述冷却腔内设有冷却装置。Furthermore, a cooling cavity is provided at the lower end of the pressure tank, and a cooling device is provided in the cooling cavity.

进一步地,所述冷却装置包括多件水平设于所述冷却腔内的冷却管,以及与所述冷却管连接的循环水装置。Furthermore, the cooling device includes a plurality of cooling pipes horizontally arranged in the cooling cavity, and a circulating water device connected to the cooling pipes.

进一步地,沿竖直方向的截面,多件所述冷却管呈交错分布。Furthermore, along the vertical cross section, the plurality of cooling pipes are staggeredly distributed.

进一步地,所述冷却管采用金属材质制成。Furthermore, the cooling pipe is made of metal material.

进一步地,所述冷却管外套设有冷却套,所述冷却套采用塑料材质制成。Furthermore, a cooling jacket is disposed outside the cooling tube, and the cooling jacket is made of plastic material.

进一步地,所述冷却套外壁设有多件冷却环,多件所述冷却环沿所述冷却套的轴向分布;所述冷却环采用塑料材质制成。Furthermore, a plurality of cooling rings are provided on the outer wall of the cooling jacket, and the plurality of cooling rings are distributed along the axial direction of the cooling jacket; and the cooling rings are made of plastic material.

进一步地,所述循环水装置包括与多件所述冷却管连接筒的进水管,同时与多件所述冷却管连接的出水管,以及与所述进水管和所述出水管连接的泵体。Furthermore, the circulating water device includes a water inlet pipe connected to the plurality of cooling pipes, a water outlet pipe connected to the plurality of cooling pipes, and a pump body connected to the water inlet pipe and the water outlet pipe.

本实用新型实施例的技术方案至少具有如下优点和有益效果:本实用新型的管道反应器压力控制装置,在使用时反应器内部所产生的气体通弄个第一连接管和第二连接管进入到压力罐中,由于压力罐的直径显著大于第二连接管的直径,因此气体再由第二连接管进入到压力罐中时,其会迅速膨胀,流速迅速降低,此时裹挟在气体中的液体(呈水滴状或雾状等)失去了气体的的支撑,会逐渐回落下去,通弄个压力检测装置对压力罐中的压力进行实时检测,来调节泄压装置的动作,能够很好地实时调节压力罐以及反应器中的压力,使得反应器中保持较为平衡的压力,使得在加入新的原料,迅速发生反应产生大量的气体时,压力罐能够很好地将突然产生的大量气体排出,但是又不会使反应液排出,因此能够不影响原有反应液的浓度,且全过程可自动化运行,无需人工的干预。The technical solution of the embodiment of the utility model has at least the following advantages and beneficial effects: the pipeline reactor pressure control device of the utility model, when in use, the gas generated inside the reactor enters the pressure tank through the first connecting pipe and the second connecting pipe. Since the diameter of the pressure tank is significantly larger than the diameter of the second connecting pipe, when the gas enters the pressure tank through the second connecting pipe, it will expand rapidly and the flow rate will decrease rapidly. At this time, the liquid (in the form of water droplets or mist, etc.) entrained in the gas loses the support of the gas and will gradually fall back. The pressure in the pressure tank is detected in real time through a pressure detection device to adjust the action of the pressure relief device, which can well adjust the pressure in the pressure tank and the reactor in real time, so that a relatively balanced pressure is maintained in the reactor, so that when new raw materials are added and a rapid reaction occurs to produce a large amount of gas, the pressure tank can well discharge the suddenly generated large amount of gas, but will not discharge the reaction liquid, so that it can not affect the concentration of the original reaction liquid, and the whole process can be automatically operated without manual intervention.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

为了更清楚地说明本实用新型实施例的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,应当理解,以下附图仅示出了本实用新型的某些实施例,因此不应被看作是对范围的限定,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他相关的附图。In order to more clearly illustrate the technical solutions of the embodiments of the utility model, the drawings required for use in the embodiments will be briefly introduced below. It should be understood that the following drawings only show certain embodiments of the utility model and therefore should not be regarded as limiting the scope. For ordinary technicians in this field, other relevant drawings can be obtained based on these drawings without paying creative work.

图1为本实用新型实施例提供的管道反应器压力控制装置的结构示意图;FIG1 is a schematic structural diagram of a pipeline reactor pressure control device provided by an embodiment of the utility model;

图2为本实用新型实施例提供的冷却管部分的结构示意图。FIG. 2 is a schematic structural diagram of a cooling pipe portion provided in an embodiment of the present utility model.

图标:10-反应器,11-第一连接管,12-第二连接管,13-压力罐,14-气压检测装置,15-泄压装置,21-冷却腔,22-冷却管,23-冷却套,24-冷却环,25-进水管,26-出水管。Icons: 10-reactor, 11-first connecting pipe, 12-second connecting pipe, 13-pressure tank, 14-air pressure detection device, 15-pressure relief device, 21-cooling chamber, 22-cooling pipe, 23-cooling jacket, 24-cooling ring, 25-water inlet pipe, 26-water outlet pipe.

具体实施方式Detailed ways

为使本实用新型实施例的目的、技术方案和优点更加清楚,下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本实用新型一部分实施例,而不是全部的实施例。通常在此处附图中描述和示出的本实用新型实施例的组件可以以各种不同的配置来布置和设计。In order to make the purpose, technical solution and advantages of the embodiment of the utility model clearer, the technical solution in the embodiment of the utility model will be clearly and completely described below in conjunction with the drawings in the embodiment of the utility model. Obviously, the described embodiment is a part of the embodiment of the utility model, not all of the embodiments. Generally, the components of the embodiment of the utility model described and shown in the drawings here can be arranged and designed in various different configurations.

因此,以下对在附图中提供的本实用新型的实施例的详细描述并非旨在限制要求保护的本实用新型的范围,而是仅仅表示本实用新型的选定实施例。基于本实用新型中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。Therefore, the following detailed description of the embodiments of the present invention provided in the accompanying drawings is not intended to limit the scope of the present invention to be protected, but merely represents selected embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

应注意到:相似的标号和字母在下面的附图中表示类似项,因此,一旦某一项在一个附图中被定义,则在随后的附图中不需要对其进行进一步定义和解释。It should be noted that similar reference numerals and letters denote similar items in the following drawings, and therefore, once an item is defined in one drawing, it does not require further definition and explanation in the subsequent drawings.

在本实用新型的描述中,需要说明的是,若出现术语“中心”、“上”、“下”、“左”、“右”、“竖直”、“水平”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,或者是该申请产品使用时惯常摆放的方位或位置关系,仅是为了便于描述本实用新型和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本实用新型的限制。In the description of the present invention, it should be noted that if the terms "center", "up", "down", "left", "right", "vertical", "horizontal", "inside", "outside", etc. appear, the orientation or position relationship indicated is based on the orientation or position relationship shown in the accompanying drawings, or is the orientation or position relationship in which the product of the application is usually placed when used. It is only for the convenience of describing the present invention and simplifying the description, and does not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

在本实用新型的描述中,还需要说明的是,除非另有明确的规定和限定,若出现术语“设置”、“安装”、“相连”、“连接”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以具体情况理解上述术语在本实用新型中的具体含义。In the description of the present invention, it is also necessary to explain that, unless otherwise clearly specified and limited, the terms "set", "install", "connect", and "connect" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

实施例Example

以下结合具体实施例进一步说明,如附图1-附图2所示,本实施例的管道反应器10压力控制装置,包括与反应器10上侧连接的第一连接管11,与第一连接管11连接的第二连接管12,与第二连接管12连接的压力罐13,与压力罐13连接的压力检测装置,以及与压力罐13连接的泄压装置15;压力罐13的直径大于第二连接管12的直径。具体的,在使用时反应器10内部所产生的气体通弄个第一连接管11和第二连接管12进入到压力罐13中,由于压力罐13的直径显著大于第二连接管12的直径,因此气体再由第二连接管12进入到压力罐13中时,其会迅速膨胀,流速迅速降低,此时裹挟在气体中的液体(呈水滴状或雾状等)失去了气体的的支撑,会逐渐回落下去,通弄个压力检测装置对压力罐13中的压力进行实时检测,来调节泄压装置15的动作,能够很好地实时调节压力罐13以及反应器10中的压力,使得反应器10中保持较为平衡的压力,使得在加入新的原料,迅速发生反应产生大量的气体时,压力罐13能够很好地将突然产生的大量气体排出,但是又不会使反应液排出,因此能够不影响原有反应液的浓度,且全过程可自动化运行,无需人工的干预。The following is further described in conjunction with specific embodiments. As shown in Figures 1-2, the pressure control device of the pipeline reactor 10 of this embodiment includes a first connecting pipe 11 connected to the upper side of the reactor 10, a second connecting pipe 12 connected to the first connecting pipe 11, a pressure tank 13 connected to the second connecting pipe 12, a pressure detection device connected to the pressure tank 13, and a pressure relief device 15 connected to the pressure tank 13; the diameter of the pressure tank 13 is greater than the diameter of the second connecting pipe 12. Specifically, when in use, the gas generated inside the reactor 10 enters the pressure tank 13 through the first connecting pipe 11 and the second connecting pipe 12. Since the diameter of the pressure tank 13 is significantly larger than the diameter of the second connecting pipe 12, when the gas enters the pressure tank 13 through the second connecting pipe 12, it will expand rapidly and the flow rate will decrease rapidly. At this time, the liquid (in the form of water drops or mist, etc.) entrained in the gas loses the support of the gas and will gradually fall back. The pressure in the pressure tank 13 is detected in real time through a pressure detection device to adjust the action of the pressure relief device 15. The pressure in the pressure tank 13 and the reactor 10 can be well adjusted in real time, so that a relatively balanced pressure is maintained in the reactor 10, so that when new raw materials are added and a large amount of gas is generated by a rapid reaction, the pressure tank 13 can well discharge the large amount of gas suddenly generated, but will not discharge the reaction liquid, so that it can not affect the concentration of the original reaction liquid, and the whole process can be automatically operated without manual intervention.

本实施例中的第一连接管11与第二连接管12可拆卸连接。具体的,这样便于将本装置拆下进行清洗维护。In this embodiment, the first connecting pipe 11 and the second connecting pipe 12 are detachably connected, which makes it easy to disassemble the device for cleaning and maintenance.

本实施例中的压力罐13内部下端设有冷却腔21,冷却腔21内设有冷却装置。冷却装置包括多件水平设于冷却腔21内的冷却管22,以及与冷却管22连接的循环水装置。具体的,反应器10中反应时会产生一定的高温,此时使用冷却装置将气体和水蒸气冷却,能够更好地使液体回流到反应器10中。A cooling chamber 21 is provided at the lower end of the pressure tank 13 in this embodiment, and a cooling device is provided in the cooling chamber 21. The cooling device includes a plurality of cooling pipes 22 horizontally arranged in the cooling chamber 21, and a circulating water device connected to the cooling pipes 22. Specifically, a certain high temperature is generated during the reaction in the reactor 10, and at this time, the cooling device is used to cool the gas and water vapor, so that the liquid can flow back into the reactor 10 better.

本实施例中的沿竖直方向的截面,多件冷却管22呈交错分布。具体的,这样能够增大热气与冷却管22的接触面积,提高冷却效果。In the cross section along the vertical direction of this embodiment, the plurality of cooling tubes 22 are staggeredly distributed, which can increase the contact area between the hot gas and the cooling tubes 22 and improve the cooling effect.

本实施例中的冷却管22为金属材质制成。冷却管22外套设有冷却套23,冷却套23为塑料材质制成。冷却套23外壁设有多件冷却环24,多件冷却环24沿冷却套23的长度方向分布;冷却环24为塑料材质制成。具体的,如附图2所以,反应器10中具有大量的酸,因此如果直接使用金属材质的冷却管22并裸露在压力罐13中,那么就会导致冷却管22被腐蚀的情况,因此在冷却管22外套设有一层冷却套23就能够很好地保护冷却管22,其中冷却套23可以是聚四氟乙烯材质。而冷却环24则是为了增大气体与冷却装置的接触面积,提高冷却效果。The cooling tube 22 in this embodiment is made of metal. A cooling jacket 23 is provided on the outer surface of the cooling tube 22, and the cooling jacket 23 is made of plastic. A plurality of cooling rings 24 are provided on the outer wall of the cooling jacket 23, and the plurality of cooling rings 24 are distributed along the length direction of the cooling jacket 23; the cooling rings 24 are made of plastic. Specifically, as shown in FIG2 , there is a large amount of acid in the reactor 10, so if a metal cooling tube 22 is directly used and exposed in the pressure tank 13, the cooling tube 22 will be corroded, so a cooling jacket 23 is provided on the outer surface of the cooling tube 22 to protect the cooling tube 22 well, wherein the cooling jacket 23 can be made of polytetrafluoroethylene. The cooling ring 24 is to increase the contact area between the gas and the cooling device and improve the cooling effect.

本实施例中的循环水装置包括同时与多件冷却管22连接筒的进水管25,同时与多件冷却管22连接的出水管26,以及与进水管25和出水管26连接的泵体。The circulating water device in this embodiment includes a water inlet pipe 25 connected to multiple cooling pipes 22, a water outlet pipe 26 connected to multiple cooling pipes 22, and a pump body connected to the water inlet pipe 25 and the water outlet pipe 26.

综上,本实施例的管道反应器10压力控制装置,在使用时反应器10内部所产生的气体通弄个第一连接管11和第二连接管12进入到压力罐13中,由于压力罐13的直径显著大于第二连接管12的直径,因此气体再由第二连接管12进入到压力罐13中时,其会迅速膨胀,流速迅速降低,此时裹挟在气体中的液体(呈水滴状或雾状等)失去了气体的的支撑,会逐渐回落下去,通弄个压力检测装置对压力罐13中的压力进行实时检测,来调节泄压装置15的动作,能够很好地实时调节压力罐13以及反应器10中的压力,使得反应器10中保持较为平衡的压力,使得在加入新的原料,迅速发生反应产生大量的气体时,压力罐13能够很好地将突然产生的大量气体排出,但是又不会使反应液排出,因此能够不影响原有反应液的浓度,且全过程可自动化运行,无需人工的干预。In summary, the pressure control device of the pipeline reactor 10 of this embodiment, when in use, the gas generated inside the reactor 10 enters the pressure tank 13 through the first connecting pipe 11 and the second connecting pipe 12. Since the diameter of the pressure tank 13 is significantly larger than the diameter of the second connecting pipe 12, when the gas enters the pressure tank 13 from the second connecting pipe 12, it will expand rapidly and the flow rate will decrease rapidly. At this time, the liquid (in the form of water droplets or mist, etc.) entrained in the gas loses the support of the gas and will gradually fall back. The pressure in the pressure tank 13 is detected in real time through a pressure detection device to adjust the action of the pressure relief device 15, which can well adjust the pressure in the pressure tank 13 and the reactor 10 in real time, so that a relatively balanced pressure is maintained in the reactor 10, so that when new raw materials are added and a large amount of gas is generated by a rapid reaction, the pressure tank 13 can well discharge the large amount of gas suddenly generated, but will not discharge the reaction liquid, so that it can not affect the concentration of the original reaction liquid, and the whole process can be automatically operated without manual intervention.

以上仅为本实用新型的优选实施例而已,并不用于限制本实用新型,对于本领域的技术人员来说,本实用新型可以有各种更改和变化。凡在本实用新型的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本实用新型的保护范围之内。The above are only preferred embodiments of the present invention and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and variations. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims (9)

1. A pipeline reactor pressure control device, characterized by: comprises a first connecting pipe (11) connected with the upper side of the reactor (10), a second connecting pipe (12) connected with the first connecting pipe (11), a pressure tank (13) connected with the second connecting pipe (12), a pressure detection device connected with the pressure tank (13) and a pressure relief device (15) connected with the pressure tank (13);
The diameter of the pressure tank (13) is larger than the diameter of the second connecting pipe (12).
2. The pipe reactor pressure control device according to claim 1, wherein: the first connecting pipe (11) is detachably connected with the second connecting pipe (12).
3. The pipe reactor pressure control device according to claim 1, wherein: the lower end in the pressure tank (13) is provided with a cooling cavity (21), and a cooling device is arranged in the cooling cavity (21).
4. A pipeline reactor pressure control device as claimed in claim 3, wherein: the cooling device comprises a plurality of cooling pipes (22) horizontally arranged in the cooling cavity (21), and a circulating water device connected with the cooling pipes (22).
5. The pipe reactor pressure control device according to claim 4, wherein: the cooling pipes (22) are staggered in the vertical cross section.
6. The pipe reactor pressure control device according to claim 4, wherein: the cooling pipe (22) is made of metal materials.
7. The pipe reactor pressure control device according to claim 6, wherein: the cooling pipe (22) is sleeved with a cooling sleeve (23), and the cooling sleeve (23) is made of plastic materials.
8. The pipe reactor pressure control device according to claim 7, wherein: the outer wall of the cooling sleeve (23) is provided with a plurality of cooling rings (24), and the cooling rings (24) are distributed along the axial direction of the cooling sleeve (23); the cooling ring (24) is made of plastic materials.
9. The pipe reactor pressure control device according to claim 4, wherein: the circulating water device comprises a water inlet pipe (25) connected with a plurality of cooling pipes (22), a water outlet pipe (26) connected with the cooling pipes (22) at the same time, and a pump body connected with the water inlet pipe (25) and the water outlet pipe (26).
CN202322697404.8U 2023-10-08 2023-10-08 A pipeline reactor pressure control device Active CN220933400U (en)

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CN202322697404.8U CN220933400U (en) 2023-10-08 2023-10-08 A pipeline reactor pressure control device

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PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: A pressure control device for pipeline reactors

Granted publication date: 20240510

Pledgee: China Construction Bank Co.,Ltd. Hejiang Branch

Pledgor: SICHUAN HUANAN INORGANIC SALTS Co.,Ltd.

Registration number: Y2024980058682