CN220861419U - Concentrate preprocessing device in potassium phytate production - Google Patents
Concentrate preprocessing device in potassium phytate production Download PDFInfo
- Publication number
- CN220861419U CN220861419U CN202322497709.4U CN202322497709U CN220861419U CN 220861419 U CN220861419 U CN 220861419U CN 202322497709 U CN202322497709 U CN 202322497709U CN 220861419 U CN220861419 U CN 220861419U
- Authority
- CN
- China
- Prior art keywords
- heat exchanger
- feed inlet
- frame filter
- plate frame
- storage tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 title claims abstract description 23
- 235000002949 phytic acid Nutrition 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 239000011591 potassium Substances 0.000 title claims abstract description 16
- 229910052700 potassium Inorganic materials 0.000 title claims abstract description 16
- 239000012141 concentrate Substances 0.000 title claims abstract description 12
- 238000007781 pre-processing Methods 0.000 title claims description 5
- 230000007062 hydrolysis Effects 0.000 claims abstract description 12
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims description 6
- 239000010865 sewage Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 8
- 238000000746 purification Methods 0.000 abstract description 6
- 238000000926 separation method Methods 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 12
- 239000012535 impurity Substances 0.000 description 8
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 description 4
- 229940068041 phytic acid Drugs 0.000 description 4
- 239000000467 phytic acid Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 240000008042 Zea mays Species 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 235000005822 corn Nutrition 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model belongs to the technical field of phytate production, and discloses a concentrated solution pretreatment device in potassium phytate production, which comprises a concentrated solution storage tank, a heat exchanger, a pre-decolorizing tank, a plate frame filter and a hydrolysis kettle which are sequentially communicated through pipelines, valves and pumps, wherein the discharge port of the concentrated solution storage tank is communicated with the feed inlet of the heat exchanger, the discharge port of the heat exchanger is communicated with the feed inlet of the pre-decolorizing tank, the discharge port of the pre-decolorizing tank is communicated with the feed inlet of the plate frame filter, and the discharge port of the plate frame filter is communicated with the feed inlet of the hydrolysis kettle. The utility model pretreats the potassium phytate concentrate to remove macromolecular organic substances, thereby effectively reducing the separation and purification difficulty of the subsequent procedures and improving the production efficiency.
Description
Technical Field
The utility model belongs to the technical field of phytate production, and particularly relates to a concentrated solution pretreatment device in potassium phytate production.
Background
The corn soaking water is leftover material produced in the wet process of producing corn starch, and has phytic acid in 1-2 wt% and through extraction, separation and purification, phytic acid or phytate may be produced for sale. However, because the corn soaking water has very complex components, besides the phytic acid, the corn soaking water also contains impurities such as protein, starch, lactic acid, sugar, calcium, magnesium and the like, and the content of the impurities is far higher than that of the phytic acid; the potassium phytate raw material liquid obtained in the existing production process is directly separated by a resin column after concentration and hydrolysis, and because of the existence of a large amount of impurities, the resin column is easy to be blocked, the difficulty of separation and purification of the subsequent process is increased, and the production efficiency is seriously affected.
Disclosure of Invention
The technical problems to be solved by the utility model are as follows: the concentrated solution pretreatment device for potassium phytate production overcomes the defects of the prior art, pretreats the concentrated solution of potassium phytate, removes macromolecular organic substances in the concentrated solution, effectively reduces the separation and purification difficulty of subsequent procedures, and improves the production efficiency.
In order to solve the technical problems, the technical scheme of the utility model is as follows:
Concentrate preprocessing device in potassium phytate production includes concentrate storage tank, heat exchanger, the decoloration jar in advance, board frame filter and the cauldron of hydrolysising that communicate in proper order through pipeline, valve and pump, and the discharge gate of concentrate storage tank communicates the feed inlet to the heat exchanger, and the discharge gate of heat exchanger communicates the feed inlet to the decoloration jar in advance, and the discharge gate of decoloration jar in advance communicates the feed inlet to board frame filter, and board frame filter's discharge gate communicates the feed inlet to the cauldron of hydrolysising.
Preferably, the concentrated solution storage tank is a cone bottom storage tank, a drain outlet is arranged at the cone bottom, and the drain outlet is communicated with a drain valve; a liquid outlet is arranged on the side wall of the cone bottom of the concentrated solution storage tank on one side of the upper part of the sewage outlet, and the liquid outlet is communicated to the heat exchanger through a pipeline.
Preferably, the heat exchanger is an AM5-MPL/175 model heat exchanger. The manufacturer is Amiteck industrial equipment Inc. Shanghai.
Preferably, the plate frame filter is a HMZG150/1250-V model plate frame filter. The manufacturer is Jingjin equipment and stock limited company.
Due to the adoption of the technical scheme, the utility model has the beneficial effects that:
the concentrated solution is prepared by precipitating insoluble particles in a concentrated solution storage tank and discharging the insoluble particles, heating and denaturing soluble organic matters by a heater, adding activated carbon into a pre-decolorizing tank to adsorb adsorbable matters in the solution, filtering the denatured organic matters, the activated carbon and impurities adsorbed by the activated carbon by a plate-frame filter, conveying the treated filtrate into a hydrolysis kettle for hydrolysis, and effectively removing most of impurities such as protein, insoluble starch, colloid, pigment and the like in the concentrated solution by the treatment, thereby reducing the separation and purification difficulty of subsequent procedures.
In a word, the utility model pretreats the potassium phytate concentrated solution to remove macromolecular organic substances, thereby effectively reducing the separation and purification difficulty of the subsequent procedures and improving the production efficiency.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
In the figure, 1, a concentrated solution storage tank; 2. a heat exchanger; 3. a pre-decoloring tank; 4. a plate frame filter; 5. and (3) a hydrolysis kettle.
Detailed Description
The utility model is further illustrated in the following, in conjunction with the accompanying drawings and examples.
Embodiment one:
As shown in fig. 1, a concentrate preprocessing device in potassium phytate production includes concentrate storage tank 1, heat exchanger 2, pre-decoloration jar 3, plate frame filter 4 and hydrolysis kettle 5 that communicate in proper order through pipeline (not shown), valve (not shown) and pump (not shown), and the discharge gate of concentrate storage tank 1 communicates to the feed inlet of heat exchanger 2, and the discharge gate of heat exchanger 2 communicates to the feed inlet of pre-decoloration jar 3, and the discharge gate of pre-decoloration jar 3 communicates to the feed inlet of plate frame filter 4, and the discharge gate of plate frame filter 4 communicates to the feed inlet of hydrolysis kettle 5.
In actual use, the potassium phytate concentrated solution obtained in the previous step is firstly conveyed into a concentrated solution storage tank 1 for temporary storage, insoluble particles in the concentrated solution can be deposited at the bottom of the cone bottom of the concentrated solution storage tank 1, and the deposited impurities are periodically discharged through a drain valve arranged at the bottom of the cone bottom; the rest concentrated solution is conveyed to the heat exchanger 2 through the liquid outlet of the storage tank, and the heat exchanger 2 heats the concentrated solution by using hot water in the process, so that organic matters (including proteins, colloids and the like) in the concentrated solution are separated out by thermal denaturation; then, the heated concentrated solution is conveyed to a pre-decoloring tank 3, activated carbon is added into the pre-decoloring tank 3 for decoloring and adsorbing (adsorbing impurities such as pigment and the like); after the decoloring is finished, the mixture is pumped into a plate-and-frame filter 4 for filtering, denatured organic matters, activated carbon and impurities adsorbed by the activated carbon are filtered out, and clear liquid enters a hydrolysis kettle 5 for subsequent hydrolysis and other working procedures.
It is to be understood that these examples are illustrative of the present utility model and are not intended to limit the scope of the present utility model. Furthermore, it should be understood that various changes and modifications can be made by one skilled in the art after reading the teachings of the present utility model, and such equivalents are intended to fall within the scope of the utility model as defined in the appended claims.
Claims (4)
1. Concentrate preprocessing device in potassium phytate production, its characterized in that: including concentrate storage tank, heat exchanger, the decoloration jar in advance, plate frame filter and the hydrolysis kettle of communicating in proper order through pipeline, valve and pump, the feed inlet to the heat exchanger is linked together to the discharge gate of concentrate storage tank, and the feed inlet to the decoloration jar in advance is linked together to the discharge gate of heat exchanger, and the feed inlet to the plate frame filter is linked together to the discharge gate of decoloration jar in advance, and the feed inlet to the hydrolysis kettle is linked together to the discharge gate of plate frame filter.
2. The pretreatment device for concentrated solutions in potassium phytate production as claimed in claim 1, wherein: the concentrated solution storage tank is a cone bottom storage tank, a drain outlet is arranged at the cone bottom, and the drain outlet is communicated with a drain valve; the side wall of the cone bottom at one side of the upper part of the sewage outlet is provided with a liquid outlet which is communicated with the heat exchanger through a pipeline.
3. The pretreatment device for concentrated solutions in potassium phytate production as claimed in claim 1, wherein: the heat exchanger is an AM5-MPL/175 type heat exchanger.
4. The pretreatment device for concentrated solutions in potassium phytate production as claimed in claim 1, wherein: the plate frame filter is an HMZG150/1250-V model plate frame filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322497709.4U CN220861419U (en) | 2023-09-14 | 2023-09-14 | Concentrate preprocessing device in potassium phytate production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322497709.4U CN220861419U (en) | 2023-09-14 | 2023-09-14 | Concentrate preprocessing device in potassium phytate production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220861419U true CN220861419U (en) | 2024-04-30 |
Family
ID=90816307
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322497709.4U Active CN220861419U (en) | 2023-09-14 | 2023-09-14 | Concentrate preprocessing device in potassium phytate production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220861419U (en) |
-
2023
- 2023-09-14 CN CN202322497709.4U patent/CN220861419U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101864002B (en) | Method for extracting sodium heparin | |
| CN103805665B (en) | A kind of preparation method of deep-sea fish skin collagen polypeptide | |
| CN111793145A (en) | Process for improving quality and yield of sodium chondroitin sulfate co-produced collagen peptide | |
| CN102146144B (en) | Method for extracting and refining inulin | |
| CA3109770C (en) | Method for extracting antibacterial peptides and albumin from pea whey wastewater | |
| CN104593446A (en) | Preparation method of pure xylooligosaccharide powder | |
| CN103626836A (en) | Extraction process for polypeptide from waste liquid obtained in production of crude heparin sodium product | |
| CN107011457B (en) | A method of extracting preparation non-starch polysaccharide and small molecule nutrient molecule from sweet potato waste water | |
| CN103232362B (en) | Process for extracting L-glutamine | |
| CN220861419U (en) | Concentrate preprocessing device in potassium phytate production | |
| CN105441520A (en) | Method adopting rice residues as raw material for enzyme-membrane combined preparation of rice polypeptides | |
| CN106220521B (en) | A kind of method of full film extraction L isoleucines | |
| WO2023000578A1 (en) | Protein recovery system and method in production process of ultra-high maltose syrup | |
| CN104045551A (en) | Recycling method of unqualified sodium citrate mother liquor | |
| CN113151382B (en) | Method for producing wheat oligopeptide by precipitation method | |
| CN105148557B (en) | A kind of syrup decolorization system | |
| CN113861236B (en) | Method for preparing calcium phytate by purifying phytic acid | |
| CN210560185U (en) | Device for purifying and recovering protein peptide by membrane method | |
| CN221681002U (en) | Corn protein separating device | |
| CN208949005U (en) | Primary reverse osmosis water system for preparing ergothioneine through biological fermentation synthesis | |
| CN1308130A (en) | Method of extracting nucleic and from microbe cell | |
| CN204874353U (en) | Device of cystine waste liquid production leucine | |
| CN204874354U (en) | Device of feather production cystine | |
| CN220939196U (en) | Crystallization mother liquor processing apparatus in potassium dihydrogen phosphate production | |
| CN214183017U (en) | One set of device of preparation acid type sophorolipid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |