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CN210775208U - Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band - Google Patents

Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band Download PDF

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Publication number
CN210775208U
CN210775208U CN201921563386.1U CN201921563386U CN210775208U CN 210775208 U CN210775208 U CN 210775208U CN 201921563386 U CN201921563386 U CN 201921563386U CN 210775208 U CN210775208 U CN 210775208U
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China
Prior art keywords
mounting
test
test tube
top cover
liquid
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Expired - Fee Related
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CN201921563386.1U
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Chinese (zh)
Inventor
李爱东
郑转平
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Xian University of Posts and Telecommunications
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Xian University of Posts and Telecommunications
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Priority to CN201921563386.1U priority Critical patent/CN210775208U/en
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Abstract

The utility model relates to the technical field of chemical testing devices, in particular to a device for measuring the absorption coefficient and the refractive index of a liquid phase substance in a terahertz waveband, which comprises an installation top cover and a plurality of test tubes; a plurality of test tubes are detachably arranged on the lower end face of the mounting top cover, and the tube openings of the test tubes are sealed by the mounting top cover; be equipped with a plurality of notes liquid holes on the installation top cap, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube. Can pour into the liquid that awaits measuring into to the test tube through annotating the liquid hole, annotate the liquid hole very little, can prevent volatilizing of the liquid that awaits measuring, guarantee the accuracy of test. In addition, the device comprises a plurality of test tubes, so that a plurality of liquids to be tested can be tested at one time, and the test efficiency is improved; simultaneously, the test tube is detachably mounted on the mounting top cover, and the test tube is convenient to take down and clean after the test is completed.

Description

Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band
Technical Field
The utility model relates to a chemistry testing arrangement technical field, concretely relates to liquid phase material is at terahertz wave band absorption coefficient's measuring device now.
Background
Terahertz (THz) waves generally refer to electromagnetic waves with a frequency in the range of 0.1-10 THZ, have a wavelength of 30-3000 μm, and are located at very special positions in the whole electromagnetic spectrum. In terms of frequency, it is between radio waves and light waves; in terms of wavelength, it is between millimeter waves and infrared waves; it is energetically intermediate between electrons and photons. In recent years, with the rapid development of the THz spectrum technology, the research and application of the THz frequency band at home and abroad are more and more. Among them, the field to which the THz spectroscopy can be applied is also becoming wider and wider.
According to research, the Terahertz time-domain spectroscopy (THz-TDS) has been increasingly applied to the fields of medicine, security inspection, material structure detection, transmission communication, biopharmaceutical and the like. The collective vibration of most biological macromolecules is in THz wave band, so that the THz time domain spectrum technology can be used for qualitatively judging substance elements and quantitatively testing substance content, and the terahertz absorption spectrum can determine conformation and configuration through specific characteristic spectrum; in addition, the terahertz wave has penetrability, can easily penetrate substances such as plastics and ceramics, can also detect biological tissue information under epidermis, has very low photon energy, cannot generate ionization effect like X-rays, has no damage to organisms and biological tissues, has very high sensitivity to polar substances, and has better contrast than X-rays in soft tissue tests. However, the application of THz time-domain spectroscopy techniques relies on the comparison of tests on the absorption coefficient of substances in the THz band. Research shows that by comparing the absorption coefficients of substances in the THz wave band, not only solid-phase substances can be distinguished, but also different liquid-phase substances can be distinguished. This is extremely lacking in the medical and safety fields at the present stage and is not achieved by other spectroscopic techniques. The application of the THz time domain spectroscopy technology is more and more close to the drug production, medical treatment and airport safety detection which are closely related to the daily life of human beings, and the THz time domain spectroscopy technology has very important practical significance and immeasurable prospect value for maintaining the social health and safety of human beings.
When the THz time domain spectrum is used for detecting qualitative substances, the key problem is to rapidly and accurately obtain the absorption coefficient of a detected sample in the THz wave band by using a proper device. Compared with liquid phase substances, the detection of solid substances is simpler, and more descriptions are provided for the THz spectrum testing device at home and abroad and the THz spectrum testing device is in a unified trend. However, the liquid phase substance has very rare introduction of the testing device due to the problems of fluidity, volatility, mixed heat dissipation and the like. In the prior art, liquid substance measurement is usually placed in a quartz cuvette, and the problems of large measurement error, difficulty in adjusting the measurement optical distance, low test efficiency and the like exist. In addition, when the liquid substance is repeatedly tested, the light path is influenced and the toxic liquid can cause damage to human body if careless. Therefore, it is important to design a testing device for the liquid phase substance in the THz wave band, which is rapid, safe, high in accuracy and easy to clean.
SUMMERY OF THE UTILITY MODEL
The utility model discloses the main technical problem who solves measures the liquid that awaits measuring among the prior art when terahertz wave band's absorption coefficient and refracting index, and efficiency of software testing is low, inconvenient tube cleaning's technical problem.
A device for measuring the absorption coefficient and the refractive index of a liquid phase substance in a terahertz waveband comprises an installation top cover and a plurality of test tubes;
the test tubes are detachably arranged on the lower end face of the mounting top cover, and the tube openings of the test tubes are sealed by the mounting top cover;
be equipped with a plurality of notes liquid holes on the installation top cap, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube.
Wherein, the installation top cap is the polytetrafluoroethylene board, the test tube is the polytetrafluoroethylene pipe.
The test tube comprises a test tube body, a top cover, a test tube end, a connecting structure and a plurality of mounting grooves, wherein the lower end face of the mounting top cover is provided with the plurality of concave mounting grooves, the outer wall of the tube end of the test tube is provided with the connecting structure, and the connecting structure is detachably mounted in the mounting grooves.
Wherein, the mounting groove is the thread groove, connection structure is the screw thread, the test tube passes through screw thread detachable with the installation top cap.
The polytetrafluoroethylene plate is circular, and a plurality of mounting grooves are uniformly formed in the lower end face of the polytetrafluoroethylene plate along the circumference.
Specifically, evenly be equipped with 12 mounting grooves along the circumference on the installation top cap, install one in every mounting groove the test tube.
Wherein, the length of a plurality of test tubes of installation on the installation top cap increases along a diameter direction of this installation top cap in proper order, wherein about the length of two test tubes of diameter symmetry is the same.
Furthermore, the center of the mounting top cover is also provided with a mounting hole for fixedly mounting the mounting top cover.
The diameter of the mounting top cover is 80mm, and the thickness of the mounting top cover is 6 mm; the diameter of the mounting groove is 6mm, and the depth of the mounting groove is 4 mm; the diameter of the liquid injection hole is 0.5 mm.
Wherein the longest length of the plurality of test tubes is 65mm and the shortest length is 5 mm.
According to above-mentioned embodiment's testing arrangement, it is including installation top cap and a plurality of test tube, the lower terminal surface at the installation top cap is installed to a plurality of test tubes are detachable, after the test is accomplished, the dismantlement of convenient test tube is washd, and the mouth of pipe of test tube is sealed by the installation top cap, be equipped with a plurality of notes liquid holes on the installation top cap, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube, can pour into the liquid that awaits measuring into in to the test tube through annotating the liquid hole, it is very little to annotate the liquid hole, can prevent the volatilization of the liquid that awaits measuring, the accuracy. In addition, the device comprises a plurality of test tubes, so that a plurality of liquids to be tested can be tested at one time, and the test efficiency is improved; simultaneously, the test tube is detachably mounted on the mounting top cover, and the test tube is convenient to take down and clean after the test is completed.
Drawings
FIG. 1 is a schematic diagram of an overall structure of a testing apparatus according to an embodiment of the present disclosure;
FIG. 2 is a cross-sectional view of a test apparatus along a diameter according to an embodiment of the present application;
FIG. 3 is a top view of a testing device according to an embodiment of the present disclosure.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings. Wherein like elements in different embodiments are numbered with like associated elements. In the following description, numerous details are set forth in order to provide a better understanding of the present application. However, those skilled in the art will readily recognize that some of the features may be omitted or replaced with other elements, materials, methods in different instances. In some instances, certain operations related to the present application have not been shown or described in detail in order to avoid obscuring the core of the present application from excessive description, and it is not necessary for those skilled in the art to describe these operations in detail, so that they may be fully understood from the description in the specification and the general knowledge in the art.
Furthermore, the features, operations, or characteristics described in the specification may be combined in any suitable manner to form various embodiments. Also, the various steps or actions in the method descriptions may be transposed or transposed in order, as will be apparent to one of ordinary skill in the art. Thus, the various sequences in the specification and drawings are for the purpose of describing certain embodiments only and are not intended to imply a required sequence unless otherwise indicated where such sequence must be followed.
The numbering of the components as such, e.g., "first", "second", etc., is used herein only to distinguish the objects as described, and does not have any sequential or technical meaning. The term "connected" and "coupled" when used in this application, unless otherwise indicated, includes both direct and indirect connections (couplings).
The utility model provides a testing arrangement, it is including installation top cap and a plurality of test tube, the lower terminal surface at the installation top cap is installed to a plurality of test tube detachablely, after the test is accomplished, the dismantlement of conveniently testing the test tube is washd, and the mouth of pipe of test tube is sealed by the installation top cap, be equipped with a plurality of notes liquid holes on the installation top cap, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube, can pour into the liquid that awaits measuring into in to the test tube through annotating the liquid hole, it is very little to annotate the liquid hole, can prevent volatilizing of the liquid that awaits measuring, the. In addition, this device includes a plurality of test tubes, once can test the multiple liquid that awaits measuring, has improved efficiency of software testing.
Referring to fig. 1, the present embodiment provides a device for measuring an absorption coefficient and a refractive index of a liquid substance in a terahertz waveband, the device includes a mounting top cover 21 and a plurality of test tubes 24, wherein the plurality of test tubes 24 are detachably mounted on a lower end surface of the mounting top cover 21, and a tube opening of the test tube 24 is sealed by the mounting top cover 21, so that the liquid substance to be detected placed in the test tube 24 can be volatilized, which affects the accuracy of measurement.
Wherein, be equipped with a plurality of notes liquid holes on installation top cap 21, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube 24, can adopt the syringe to pour into the liquid phase material that awaits measuring into the test tube through the liquid hole of annotating that corresponds like this.
Wherein, the installation top cap 21 of this embodiment is the polytetrafluoroethylene board, and test tube 24 is the polytetrafluoroethylene pipe, because polytetrafluoroethylene has very high transmissivity at the terahertz wave band, and it can be under aqueous solution environment refractive index remain unchanged basically moreover, compares with other materials, and it can show the test information of sample at the terahertz wave band more, consequently in this embodiment, installation top cap 21 chooses for use the polytetrafluoroethylene board, and test tube 24 is the polytetrafluoroethylene pipe.
In the embodiment shown in fig. 1, the mounting form of each test tube is the same, and in the embodiment, one test tube is taken as an example for illustration, the mounting top cover 21 is disc-shaped, a plurality of concave mounting grooves 22 are arranged on the lower end surface of the mounting top cover 21, a connecting structure is arranged on the outer wall of the pipe orifice end of the test tube 24, the connecting structure is detachably mounted in the mounting grooves, wherein the mounting groove 22 and the connecting structure have various forms, such as a snap and a slot, as long as the test tube 24 can be detachably connected, and can be sealed by the mounting top cover 21 after being mounted on the mounting top cover 21, the test tube 24 can be detachably mounted on the mounting top cover 21, after the test is accomplished, can conveniently dismantle test tube 24 and wash, compare than the mode that current adoption wooden plug etc. sealed test tube, the sealed mode of this embodiment is more high-efficient.
Wherein, as shown in fig. 2 and fig. 3, 12 mounting grooves 22 are uniformly arranged on the mounting top cover 21 along the circumference, one test tube 24 is mounted in each mounting groove 22, and the central angle of every two adjacent test tubes 24 spaced in the circumferential direction is 30 °. And the plurality of test tubes 24 degrees on the mounting top cover 21 are sequentially increased along one diameter direction of the mounting top cover 21, wherein the two test tubes symmetrical about the diameter have the same length. As shown in figure 1, serial numbers 1-12 are the notes liquid hole that every test tube corresponds respectively, 1 number notes liquid hole corresponding test tube length design is 65mm, 2 numbers and 3 numbers annotate the test tube length that the liquid hole corresponds and be 55mm, 4 numbers and 5 numbers annotate the test tube length that the liquid hole corresponds and be 45mm, 6 numbers and 7 numbers annotate the test tube length that the liquid hole corresponds and be 35mm, 8 numbers and 9 numbers annotate the test tube length that the liquid hole corresponds and be 25mm, 10 numbers and 11 numbers annotate the test tube length that the liquid hole corresponds and be 15mm, last 12 numbers annotate the test tube length that the liquid hole corresponds and be 5mm, the design can make the result of detection more accurate can not waste the sample simultaneously. In addition, the upper part of the mounting top cover 21 is provided with a liquid injection hole corresponding to each test tube for adding another sample to detect the mixed substance in the detection process, so that the contact between the detected sample and air is reduced, the relatively good sealing performance is ensured, and the detection precision is improved. This allows the test tube 24 to be designed to be removable, again to facilitate cleaning of the device after testing.
Specifically, in the embodiment, the diameter of the mounting top cover is 80mm, and the thickness is 6 mm; the diameter of the mounting groove is 6mm, and the depth of the mounting groove is 4 mm; the diameter of the liquid injection hole is 0.5 mm.
Specifically, the mounting groove 22 that sets up on installation top cap 21 in this embodiment is the thread groove, and the connection structure that sets up in test tube 24 upper end is the screw thread, and test tube 24 passes through screw thread detachable connection with installation top cap 21.
Further, a mounting hole 23 is formed in the center of the mounting top cover 21, the mounting hole 23 in this embodiment is a threaded hole, the mounting hole 23 is used for connecting with a mounting mechanism, fixing the testing device on the mounting mechanism, and then irradiating by terahertz waves.
The testing device of this embodiment includes a plurality of test tubes, once can test a plurality of liquid that await measuring, has improved efficiency of software testing, can pour into the liquid that awaits measuring into to the test tube through annotating the liquid hole, annotate the liquid hole very little, can prevent volatilizing of the liquid that awaits measuring, has guaranteed the accuracy of test.
It is right to have used specific individual example above the utility model discloses expound, only be used for helping to understand the utility model discloses, not be used for the restriction the utility model discloses. To the technical field of the utility model technical personnel, the foundation the utility model discloses an idea can also be made a plurality of simple deductions, warp or replacement.

Claims (10)

1. The device for measuring the absorption coefficient and the refractive index of the liquid phase substance in the terahertz waveband is characterized by comprising an installation top cover and a plurality of test tubes;
the test tubes are detachably arranged on the lower end face of the mounting top cover, and the tube openings of the test tubes are sealed by the mounting top cover;
be equipped with a plurality of notes liquid holes on the installation top cap, wherein every notes liquid hole corresponds a test tube respectively and communicates with this test tube.
2. The measurement device of claim 1, wherein the mounting cap is a teflon plate and the test tube is a teflon tube.
3. The measuring device according to claim 2, wherein the lower end surface of the mounting top cover is provided with a plurality of concave mounting grooves, and the outer wall of the tube orifice end of the test tube is provided with a connecting structure which is detachably mounted in the mounting grooves.
4. The measuring device according to claim 3, wherein the mounting groove is a threaded groove, the connecting structure is a thread, and the test tube is detachably connected with the mounting top cover through the thread.
5. The measuring device as claimed in claim 4, wherein the teflon plate is circular, and a plurality of mounting grooves are uniformly formed on the lower end surface along the circumference.
6. The measuring device of claim 5, wherein the mounting top cover is uniformly provided with 12 mounting slots along the circumference, and each mounting slot is provided with one test tube.
7. A measuring device according to claim 6, wherein the length of the test tubes mounted on the mounting cap increases in sequence along a diameter of the mounting cap, wherein the length of two test tubes symmetrical about the diameter is the same.
8. The measuring device of claim 1, wherein the mounting cap further comprises a mounting hole in the center thereof for fixedly mounting the mounting cap.
9. A measuring device according to claim 5, wherein the mounting cap has a diameter of 80mm and a thickness of 6 mm; the diameter of the mounting groove is 6mm, and the depth of the mounting groove is 4 mm; the diameter of the liquid injection hole is 0.5 mm.
10. A measuring device according to claim 7, wherein the longest length of the plurality of test tubes is 65mm and the shortest length is 5 mm.
CN201921563386.1U 2019-09-19 2019-09-19 Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band Expired - Fee Related CN210775208U (en)

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Application Number Priority Date Filing Date Title
CN201921563386.1U CN210775208U (en) 2019-09-19 2019-09-19 Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921563386.1U CN210775208U (en) 2019-09-19 2019-09-19 Device for measuring absorption coefficient and refractive index of liquid phase substance in terahertz wave band

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CN210775208U true CN210775208U (en) 2020-06-16

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113101999A (en) * 2021-04-28 2021-07-13 廊坊师范学院 Three-dimensional fluorescence detection device for industrial wastewater treatment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113101999A (en) * 2021-04-28 2021-07-13 廊坊师范学院 Three-dimensional fluorescence detection device for industrial wastewater treatment

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Granted publication date: 20200616

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