CN218307894U - Stirring mechanism for 8-hydroxyquinoline reaction container - Google Patents
Stirring mechanism for 8-hydroxyquinoline reaction container Download PDFInfo
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- CN218307894U CN218307894U CN202221434478.1U CN202221434478U CN218307894U CN 218307894 U CN218307894 U CN 218307894U CN 202221434478 U CN202221434478 U CN 202221434478U CN 218307894 U CN218307894 U CN 218307894U
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Abstract
The utility model relates to a reaction vessel technical field discloses an rabbling mechanism that 8-hydroxyquinoline reaction vessel was used includes the reaction barrel, the fixed surface of reaction barrel is connected with the base, sealed lid has been cup jointed at the top of reaction barrel, the inner wall fixedly connected with sealing washer of sealed lid, the top fixedly connected with feed nozzle of sealed lid, the stirring hole has been seted up to the surface of sealing washer. The utility model has the advantages of it is following and effect: motor drive motor pivot drives the glass stick and rotates in the inside in stirring hole, the glass ball that makes the surface under the rotation is followed and is rotated, increase and the area of contact of raw materials, the glass ball is under rotating, it mixes to drive the raw materials, it is more even to make it mix, and glass ball and glass stick can not touch the inner wall of retort, chemical reaction efficiency between the messenger raw materials obtains improving, can be when the stirring through the feed inlet, carry out the material loading to the inside of retort, the staff of being convenient for supplements the content of raw materials at any time.
Description
Technical Field
The utility model relates to a reaction vessel technical field, in particular to rabbling mechanism that 8-hydroxyquinoline reaction vessel was used.
Background
During the preparation process of 8-hydroxyquinoline, the 8-hydroxyquinoline is synthesized by taking o-aminophenol, o-nitrophenol, anhydrous glycerin and concentrated sulfuric acid as raw materials, is insoluble in water and ether, is soluble in ethanol, acetone, chloroform, benzene or dilute acid and can be sublimated.
In the prior art, chinese patent publication No. CN210496297U discloses a high temperature resistant reaction vessel, which comprises a reaction vessel made of a metal material, the reaction vessel is provided with a reaction chamber and a material input port, the reaction vessel is connected with a sealing cover which is used for closing the material input port and is made of a metal material, and the sealing cover is connected with a locking member for locking the sealing cover on the reaction vessel.
However, the utility model discloses when in actual use, when being used for preparing 8-hydroxyquinoline, need the staff manual use glass stick to stir the raw materials, the operation is inconvenient, and the glass stick bumps the wall easily, and manual stirring may lead to mixing inhomogeneous between the raw materials, may influence the effect of preparation, and is not convenient for wash reaction vessel's inside, consequently needs to improve.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing an rabbling mechanism that 8-hydroxyquinoline reaction container was used has more even that makes the raw materials mix, and glass ball and glass stick can not touch the inner wall of retort, make the chemical reaction efficiency between the raw materials obtain the effect that improves.
The above technical object of the present invention can be achieved by the following technical solutions: the utility model provides an rabbling mechanism that 8-hydroxyquinoline reaction vessel was used, includes the reaction barrel, the external fixed surface of reaction barrel is connected with the base, sealed lid has been cup jointed at the top of reaction barrel, the inner wall fixedly connected with sealing washer of sealed lid, the top fixedly connected with feed nozzle of sealed lid, the stirring hole has been seted up to the surface of sealing washer, the top fixedly connected with support frame of sealed lid, the top fixedly connected with motor of support frame, the output fixedly connected with motor shaft of motor, the bottom fixedly connected with glass stick of motor shaft, the inside in stirring hole is run through to the glass stick, the external fixed surface of glass stick is connected with the glass ball.
Through adopting above-mentioned technical scheme, the staff is when using, the reaction barrel is put into to the raw materials that will prepare, cover the top at the reaction barrel with sealed lid, the sealing washer makes the sealed effect better, when needs stir the mixture to the raw materials, staff's starter motor, motor drive motor pivot drives the glass stick and rotates in the inside in stirring hole, it follows the rotation to rotate the glass ball that makes the surface down, increase the area of contact with the raw materials, the glass ball is under rotating, it mixes to drive the raw materials, make it mix more even, and glass ball and glass stick can not touch the inner wall of reaction barrel, make the chemical reaction efficiency between the raw materials obtain improving, the material of reaction barrel is glass, the surface is provided with the scale mark, can be when the stirring through the feed inlet, carry out the material loading to the inside of reaction barrel, the staff of being convenient for supplyes at any time supplyes raw materials content, the progress of preparation of being convenient for.
The utility model discloses a further set up to: a water tank is arranged on one side face of the reaction barrel, and a water inlet is formed in the top of the water tank.
Through adopting above-mentioned technical scheme, after the preparation, the staff passes through the water inlet, fills water in the water tank.
The utility model discloses a further set up to: the bottom fixedly connected with water pump of water tank inner wall, the one end fixedly connected with inlet tube of water pump.
Through adopting above-mentioned technical scheme, the staff starts the water pump, produces suction, and the inlet tube begins to absorb water.
The utility model discloses a further set up to: the water pump is characterized in that the other end of the water pump is fixedly connected with a water outlet pipe, the outer surface of the water tank is fixedly connected with a water pressing pipe, and one end of the water pressing pipe is fixedly connected with a clamping sleeve.
Through adopting above-mentioned technical scheme, water flows into the water pipe from the outlet pipe, cutting ferrule and glass pipe joint.
The utility model discloses a further set up to: the outer surface of the reaction barrel is provided with a glass tube, and the outer surface of the glass tube is provided with a valve.
Through adopting above-mentioned technical scheme, the staff opens the valve, and water gets into the reaction barrel through the glass pipe, closes the valve after the water level is suitable, and the staff makes glass stick and glass ball rotate, and rivers produce the revolving force, washs the inside of reaction barrel.
The utility model discloses a further set up to: the glass tube extends to the outer surface of the base, and the glass tube is clamped with the inner wall of the clamping sleeve.
Through adopting above-mentioned technical scheme, wash the back, the staff parts cutting ferrule and glass pipe, opens the valve once more, makes sewage flow from the glass pipe, is convenient for wash reaction barrel inside, can operate repeatedly, makes reaction barrel by abluent more clean.
The beneficial effects of the utility model are that:
1. the utility model discloses, through the reaction vessel, a pedestal, sealed lid, the sealing washer, the feed nozzle, the stirring hole, a supporting fram, including a motor, an end cap, a controller, and a cover plate, motor shaft, cooperation setting between glass stick and the glass ball, can make this device when using, the staff is when using, the reaction vessel is put into to the raw materials that will prepare, cover the top at the reaction vessel with sealed lid, the sealing washer makes the sealed effect of lid better, when needs stir the raw materials and mix, staff starter motor, motor drive motor shaft drives the glass stick and rotates in the inside in stirring hole, it follows the rotation to rotate the glass ball that makes the surface down, increase the area of contact with the raw materials, the glass ball is under rotating, it mixes to drive the raw materials, make its more even that mixes, and glass ball and glass stick can not touch the inner wall of reaction vessel, make the chemical reaction efficiency between the raw materials improve, the material of reaction vessel is glass, the surface is provided with the scale mark, can be in the stirring through the feed nozzle, carry out the material loading to the inside of reaction vessel, the staff of being convenient for at any time, the content of raw materials, be convenient for preparation, the progress.
2. The utility model discloses, through the water tank, a water inlet, a water pump, the inlet tube, the outlet pipe, the pressurized-water pipe, the cutting ferrule, cooperation setting between glass pipe and the valve, can make this device when using, the staff passes through the water inlet, fill up water in the water tank, the staff starts the water pump, produce suction, the inlet tube begins to absorb water, water is from going out the water pipe inflow pressurized-water pipe, cutting ferrule and glass pipe joint, the staff opens the valve, water passes through the glass pipe and gets into the reaction barrel, close the valve after the water level is suitable, the staff makes glass stick and glass ball rotate, rivers produce the revolving force, wash the inside of reaction barrel, after wash, the staff parts cutting ferrule and glass pipe, open the valve once more, make sewage flow from the glass pipe, be convenient for wash the reaction barrel inside, can operate repeatedly, it is more clean to make the reaction barrel wash.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly described below, and it is obvious that the drawings in the description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained without creative efforts.
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged schematic view of the structure of the present invention at A in FIG. 1;
fig. 3 is a schematic structural view of the sealing cover of the present invention;
fig. 4 is a schematic view of the structure of the water tank of the present invention.
In the figure, 1, a reaction barrel; 2. a base; 3. a sealing cover; 4. a seal ring; 5. a feed nozzle; 6. a stirring hole; 7. a support frame; 8. a motor; 9. a motor shaft; 10. a glass rod; 11. a glass ball; 12. a water tank; 13. a water inlet; 14. a water pump; 15. a water inlet pipe; 16. a water outlet pipe; 17. a water pressing pipe; 18. a ferrule; 19. a glass tube; 20. and (4) a valve.
Detailed Description
The technical solution of the present invention will be clearly and completely described below with reference to the specific embodiments. It is obvious that the described embodiments are only some of the embodiments of the present invention, and not all of them. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.
Referring to fig. 1-4, an agitating mechanism for an 8-hydroxyquinoline reaction vessel comprises a reaction vessel 1, a base 2 is fixedly connected to the outer surface of the reaction vessel 1, a sealing cover 3 is sleeved on the top of the reaction vessel 1, a sealing ring 4 is fixedly connected to the inner wall of the sealing cover 3, a feeding nozzle 5 is fixedly connected to the top of the sealing cover 3, an agitating hole 6 is formed in the outer surface of the sealing ring 4, a supporting frame 7 is fixedly connected to the top of the sealing cover 3, a motor 8 is fixedly connected to the top of the supporting frame 7, a motor rotating shaft 9 is fixedly connected to the output end of the motor 8, a glass rod 10 is fixedly connected to the bottom of the motor rotating shaft 9, the glass rod 10 penetrates through the agitating hole 6, a glass ball 11 is fixedly connected to the outer surface of the glass rod 10, when a worker uses the agitating mechanism, prepared raw materials are put into the reaction vessel 1, the sealing cover 3 is covered on the top of the reaction vessel 1, the sealing ring 4 enables the sealing effect of the sealing cover 3 to be better, when raw materials need to be stirred and mixed, a worker starts the motor 8, the motor 8 drives the motor rotating shaft 9 to drive the glass rod 10 to rotate in the stirring hole 6, the glass ball 11 on the surface rotates along with the rotation under the rotation, the contact area with the raw materials is increased, the glass ball 11 drives the raw materials to be mixed under the rotation, the raw materials are mixed more uniformly, the glass ball 11 and the glass rod 10 cannot touch the inner wall of the reaction barrel 1, the chemical reaction efficiency between the raw materials is improved, the reaction barrel 1 is made of glass, the surface is provided with scale marks, the feeding can be carried out on the inner part of the reaction barrel 1 while stirring through the feeding nozzle 5, the content of the raw materials can be supplemented by the worker at any time, the preparation process is convenient, a water tank 12 is arranged on one side surface of the reaction barrel 1, and a water inlet 13 is formed in the top of the water tank 12, after preparation is finished, a worker fills water in the water tank 12 through the water inlet 13, the water pump 14 is fixedly connected to the bottom of the inner wall of the water tank 12, one end of the water pump 14 is fixedly connected with the water inlet pipe 15, the worker starts the water pump 14 to generate suction, the water inlet pipe 15 starts to absorb water, the other end of the water pump 14 is fixedly connected with the water outlet pipe 16, the outer surface of the water tank 12 is fixedly connected with the water pressing pipe 17, one end of the water pressing pipe 17 is fixedly connected with the clamping sleeve 18, water flows into the water pressing pipe 17 from the water outlet pipe 16, the clamping sleeve 18 is clamped with the glass pipe 19, the outer surface of the reaction barrel 1 is provided with the glass pipe 19, the outer surface of the glass pipe 19 is provided with the valve 20, the worker opens the valve 20 after the water level is proper, the worker rotates the glass rod 10 and the glass ball 11 to generate water flow to clean the interior of the reaction barrel 1, the glass pipe 19 extends to the outer surface of the base 2, the glass pipe 19 is clamped with the inner wall of the clamping sleeve 18, after cleaning, the cutting sleeve 18 is separated from the glass pipe 19, the valve 20 is opened again to enable sewage to flow out from the glass pipe 19, the interior to be convenient for cleaning of the reaction barrel 1, and the barrel to be cleaned, and the barrel to be capable of repeated reaction barrel to be cleaned.
In the utility model, through the matching arrangement between the reaction barrel 1, the base 2, the sealing cover 3, the sealing ring 4, the feeding mouth 5, the stirring hole 6, the supporting frame 7, the motor 8, the motor rotating shaft 9, the glass rod 10 and the glass ball 11, when the device is used, a worker puts the prepared raw materials into the reaction barrel 1 and covers the sealing cover 3 at the top of the reaction barrel 1, the sealing ring 4 enables the sealing effect of the sealing cover 3 to be better, when the raw materials are required to be stirred and mixed, the worker starts the motor 8, the motor 8 drives the motor rotating shaft 9 to drive the glass rod 10 to rotate in the stirring hole 6, the glass ball 11 on the surface rotates to follow the rotation, the contact area with the raw materials is increased, the glass ball 11 drives the raw materials to be mixed under the rotation, the mixing is more uniform, and the glass ball 11 and the glass rod 10 can not touch the inner wall of the reaction barrel 1, the chemical reaction efficiency among the raw materials is improved, the reaction barrel 1 is made of glass, the surface of the reaction barrel 1 is provided with scale marks, the feeding nozzle 5 can be used for feeding the inside of the reaction barrel 1 while stirring, so that a worker can supplement the content of the raw materials at any time, the preparation progress is facilitated, the water tank 12, the water inlet 13, the water pump 14, the water inlet pipe 15, the water outlet pipe 16, the water pressure pipe 17, the clamping sleeve 18, the glass pipe 19 and the valve 20 are matched, when the device is used, the worker fills water in the water tank 12 through the water inlet 13, the worker starts the water pump 14 to generate suction, the water inlet pipe 15 starts to absorb water, the water flows into the water pressure pipe 17 from the water outlet pipe 16, the clamping sleeve 18 is clamped with the glass pipe 19, the worker opens the valve 20, the water enters the reaction barrel 1 through the glass pipe 19, and closes the valve 20 when the water level is proper, the staff makes glass stick 10 and glass ball 11 rotate, and rivers produce the revolving force, washs the inside of retort 1, and after the washing, the staff parts cutting ferrule 18 and glass pipe 19, opens valve 20 once more, makes sewage follow glass pipe 19 and flows out, is convenient for wash 1 inside of retort, can operate repeatedly, makes retort 1 more totally by the abluent.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides an rabbling mechanism that 8-hydroxyquinoline reaction vessel used, includes reaction barrel (1), its characterized in that: the outer fixed surface of reaction barrel (1) is connected with base (2), sealed lid (3) have been cup jointed at the top of reaction barrel (1), inner wall fixedly connected with sealing washer (4) of sealed lid (3), top fixedly connected with feed nozzle (5) of sealed lid (3), stirring hole (6) have been seted up to the surface of sealing washer (4), top fixedly connected with support frame (7) of sealed lid (3), top fixedly connected with motor (8) of support frame (7), the output fixedly connected with motor shaft (9) of motor (8), the bottom fixedly connected with glass stick (10) of motor shaft (9), the inside in stirring hole (6) is run through to glass stick (10), the outer fixed surface of glass stick (10) is connected with glass ball (11).
2. The stirring mechanism for an 8-hydroxyquinoline reaction vessel according to claim 1, wherein: a water tank (12) is arranged on one side face of the reaction barrel (1), and a water inlet (13) is formed in the top of the water tank (12).
3. The stirring mechanism for an 8-hydroxyquinoline reaction vessel as claimed in claim 2, wherein: the bottom fixedly connected with water pump (14) of water tank (12) inner wall, the one end fixedly connected with inlet tube (15) of water pump (14).
4. The stirring mechanism for an 8-hydroxyquinoline reaction vessel according to claim 3, wherein: the water pump is characterized in that the other end of the water pump (14) is fixedly connected with a water outlet pipe (16), the outer surface of the water tank (12) is fixedly connected with a water pressing pipe (17), and one end of the water pressing pipe (17) is fixedly connected with a clamping sleeve (18).
5. The stirring mechanism for an 8-hydroxyquinoline reaction vessel as claimed in claim 1, wherein: the outer surface of the reaction barrel (1) is provided with a glass tube (19), and the outer surface of the glass tube (19) is provided with a valve (20).
6. The stirring mechanism for an 8-hydroxyquinoline reaction vessel according to claim 5, wherein: the glass tube (19) extends to the outer surface of the base (2), and the glass tube (19) is clamped with the inner wall of the clamping sleeve (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221434478.1U CN218307894U (en) | 2022-06-11 | 2022-06-11 | Stirring mechanism for 8-hydroxyquinoline reaction container |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221434478.1U CN218307894U (en) | 2022-06-11 | 2022-06-11 | Stirring mechanism for 8-hydroxyquinoline reaction container |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN218307894U true CN218307894U (en) | 2023-01-17 |
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ID=84867499
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202221434478.1U Active CN218307894U (en) | 2022-06-11 | 2022-06-11 | Stirring mechanism for 8-hydroxyquinoline reaction container |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN218307894U (en) |
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2022
- 2022-06-11 CN CN202221434478.1U patent/CN218307894U/en active Active
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