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CN207153661U - A kind of chemical experiment kipp gas generator - Google Patents

A kind of chemical experiment kipp gas generator Download PDF

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Publication number
CN207153661U
CN207153661U CN201720556558.7U CN201720556558U CN207153661U CN 207153661 U CN207153661 U CN 207153661U CN 201720556558 U CN201720556558 U CN 201720556558U CN 207153661 U CN207153661 U CN 207153661U
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CN
China
Prior art keywords
partition
fixedly connected
retort
hole
gas generator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720556558.7U
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Chinese (zh)
Inventor
黄依铃
吴大珍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo University
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Ningbo University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ningbo University filed Critical Ningbo University
Priority to CN201720556558.7U priority Critical patent/CN207153661U/en
Application granted granted Critical
Publication of CN207153661U publication Critical patent/CN207153661U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of chemical experiment kipp gas generator, including retort, first partition is fixedly connected with inside the retort, some first through hole are offered in the first partition, second partition is fixedly connected with the downside of first partition, some second through holes are offered on the second partition, first through hole is staggered with the second through hole, retort right side central is fixedly connected with escape pipe, the first valve is fixedly connected with the middle part of the escape pipe, feeding-in solid body pipe is fixedly connected with the left of retort, the feeding-in solid body pipe lower end is located above first partition.Compared with prior art, the beneficial effects of the utility model are:The utility model is simple in construction, easy to operate, can be in reaction toward adding solid reactant inside device, device can discharge the liquid reactants of desaturation by bottom discharge pipe simultaneously, and highly concentrated liquid reactants are added from top, reaction speed can be accelerated, gas is improved and prepare speed.

Description

A kind of chemical experiment kipp gas generator
Technical field
A kind of kipp gas generator is the utility model is related to, specifically a kind of chemical experiment kipp gas generator.
Background technology
Kipp gas generator, it is a kind of gas generator, also known as Qi Shi gas generators or hydrogen generator.It is commonly used for With preparing gas in the experiment of solid particle and liquid reactions.Typical experiment is exactly to utilize dilute sulfuric acid and zinc granule hydrogen making. It is Dutch scientist Qi Pu inventions, and named with his surname.
Traditional kipp gas generator adds solid in reaction by escape pipe, is inconvenient, and can not be in reaction Add solid and reach the purpose of sustained response, in addition traditional kipp gas generator in reaction with the carry out reaction solution concentration of reaction It can gradually reduce, be continuously added reaction solution to improve reaction solution concentration eventually so that generator fills liquid, be finally difficult to reality Existing sustained response.
For this, those skilled in the art propose a kind of chemical experiment kipp gas generator, to solve to propose in above-mentioned background The problem of.
Utility model content
The purpose of this utility model is to provide a kind of chemical experiment kipp gas generator, to solve in above-mentioned background technology The problem of proposition.
To achieve the above object, the utility model provides following technical scheme:
A kind of chemical experiment kipp gas generator, including retort, first partition is fixedly connected with inside the retort, Some first through hole are offered in the first partition, second partition, the second partition are fixedly connected with the downside of first partition On offer some second through holes, first through hole is staggered with the second through hole, and retort right side central is fixedly connected with outlet Pipe, the escape pipe middle part are fixedly connected with the first valve, are fixedly connected with feeding-in solid body pipe on the left of retort, the solid enters Expects pipe lower end is located above first partition;Sealing-plug is fixedly connected with the top of retort, liquid separation leakage is connected with the sealing-plug Bucket, first partition are located on the downside of third through-hole with offering third through-hole, the separatory funnel lower end in the middle part of second partition, reaction Pot bottom is fixedly connected with discharge nozzle, and the second valve is fixedly connected with the middle part of the discharge nozzle.
As further program of the utility model:The first through hole is identical with the second through-hole aperture.
As the utility model further scheme:The feeding-in solid body pipe slant setting, angle of inclination be 30 °- 45°。
As the utility model further scheme:The reaction pot bottom is in funnel-form.
As the utility model further scheme:The retort is glass material.
As the utility model further scheme:The feeding-in solid body tube top portion is provided with seal cover board.
Compared with prior art, the beneficial effects of the utility model are:The utility model is simple in construction, easy to operate, can With in reaction toward adding solid reactant inside device, while device can be discharged by bottom discharge pipe desaturation liquid it is anti- Thing is answered, and highly concentrated liquid reactants are added from top, reaction speed can be accelerated, gas is improved and prepares speed.
Brief description of the drawings
Fig. 1 is a kind of structural representation of chemical experiment kipp gas generator.
In figure:1- retort, 2- first partitions, 3- first through hole, 4- second partitions, the through holes of 5- second, 6- escape pipes, 7- First valve, 8- feeding-in solid bodies pipe, 9- sealing-plugs, 10- separatory funnels, 11- third through-holes, 12- discharge nozzles, the valves of 13- second, 14- seal cover boards.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Referring to Fig. 1, a kind of chemical experiment kipp gas generator, including retort 1, the inside of retort 1 is fixed to be connected First partition 2 is connected to, some first through hole 3 are offered in the first partition 2, the downside of first partition 2 is fixedly connected with second Dividing plate 4, some second through holes 5 is offered on the second partition 4, first through hole 3 is staggered with the second through hole 5, retort 1 Right side central is fixedly connected with escape pipe 6, and the middle part of escape pipe 6 is fixedly connected with the first valve 7, and the left side of retort 1 is fixed Feeding-in solid body pipe 8 is connected with, the lower end of feeding-in solid body pipe 8 is located at the top of first partition 2;
The top of retort 1 is fixedly connected with sealing-plug 9, and separatory funnel 10, first partition 2 are connected with the sealing-plug 9 Third through-hole 11 is offered in the middle part of 4 plates with second, the lower end of separatory funnel 10 is located at the downside of third through-hole 11, retort 1 Bottom is fixedly connected with discharge nozzle 12, and the middle part of discharge nozzle 12 is fixedly connected with the second valve 13.
The first through hole 3 is identical with the aperture of the second through hole 5.
The slant setting of feeding-in solid body pipe 8, angle of inclination are 30 ° -45 °.
The bottom of retort 1 is in funnel-form.
The retort 1 is glass material.
The top of feeding-in solid body pipe 8 is provided with seal cover board 14.
Seal cover board 14 is opened during use, then toward solid reactant is added inside device, closes seal cover board 14, reaction Thing falls in gravity and inertia double action and the segment distance of side roll one to the right is then proceeded in first partition 2, afterwards by dividing Liquid funnel 10 is gradually increasing, opened when being contacted with solid reactant toward addition liquid reactions liquid in device reaction tank 1, reaction liquid level Begin to react, and gas is discharged by escape pipe 6, close the first valve 7 when needing and stopping and preparing, liquid is pushed back separatory funnel In 10;
If needing to add solid reactants during the course of the reaction, liquid is first added so that liquid level is promoted to solid charging The top of pipe 8, now solid addition tube 8 is closed, and will not also be produced gas leakage even if seal cover board 14 is opened, be added afterwards solid Precursor reactant agent covers seal cover board 14, and with the progress of reaction, reaction solution concentration can gradually dilute, and be continuously added reaction solution It can make it that liquid is excessive, final liquid can fill device, thus it is finally infeasible to be continuously added liquid, when strength of fluid drops Low, reacting gas opens the second valve 13 when reducing, reaction solution outflow, ensure that reaction solution liquid level is higher than the mouth of pipe of discharge nozzle 12 Ensure that gas is not revealed, then add high concentration reaction solution.
Operation principle of the present utility model is:The utility model opens seal cover board 14 when in use, then toward in device Portion adds solid reactant, closes seal cover board 14, and reactant falls in first partition 2 so in gravity and inertia double action After continue to roll a segment distance to the right, afterwards by separatory funnel 10 toward adding liquid reactions liquid, reaction in device reaction tank 1 Liquid level is gradually increasing, and starts to react when contacting with solid reactant, and discharges gas by escape pipe 6, is made when needing stopping The first valve 7 is closed when standby, liquid is pushed back in separatory funnel 10, if needing to add solid reactants during the course of the reaction, First add liquid so that liquid level is promoted to the top of solid addition tube 8, and now solid addition tube 8 is closed, even if opening closure Plate 14 will not also produce gas leakage, add solid reactants afterwards and cover seal cover board 14, with the progress of reaction, instead Liquid concentration is answered gradually to dilute, being continuously added reaction solution can make it that liquid is excessive, and final liquid can fill device, thus constantly add It is finally infeasible to enter liquid, and when strength of fluid reduces, reacting gas opens the second valve 13 when reducing, and reaction solution flows out, Ensure that reaction solution liquid level can ensure that gas is not revealed higher than the mouth of pipe of discharge nozzle 12, then add high concentration reaction solution.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and And in the case of without departing substantially from spirit or essential attributes of the present utility model, it can realize that this practicality is new in other specific forms Type.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and is nonrestrictive, this practicality is new The scope of type limits by appended claims rather than described above, it is intended that the equivalency fallen in claim is contained All changes in justice and scope are included in the utility model.Any reference in claim should not be considered as limitation Involved claim.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims (6)

1. a kind of chemical experiment kipp gas generator, including retort, it is characterised in that be fixedly connected with inside the retort First partition, some first through hole are offered in the first partition, second partition is fixedly connected with the downside of first partition, it is described Some second through holes are offered on second partition, first through hole is staggered with the second through hole, and retort right side central, which is fixed, to be connected Escape pipe is connected to, the first valve is fixedly connected with the middle part of the escape pipe, feeding-in solid body pipe, institute are fixedly connected with the left of retort Feeding-in solid body pipe lower end is stated to be located above first partition;Sealing-plug is fixedly connected with the top of retort, is connected in the sealing-plug There is separatory funnel, for first partition with offering third through-hole in the middle part of second partition, the separatory funnel lower end is located at third through-hole Downside, reaction pot bottom are fixedly connected with discharge nozzle, the second valve are fixedly connected with the middle part of the discharge nozzle.
A kind of 2. chemical experiment kipp gas generator according to claim 1, it is characterised in that the first through hole and the Two through-hole apertures are identical.
A kind of 3. chemical experiment kipp gas generator according to claim 1 or 2, it is characterised in that the feeding-in solid body Pipe slant setting, angle of inclination are 30 ° -45 °.
A kind of 4. chemical experiment kipp gas generator according to claim 3, it is characterised in that it is described reaction pot bottom be in Funnel-form.
5. a kind of chemical experiment kipp gas generator according to claim 4, it is characterised in that the retort is glass Material.
A kind of 6. chemical experiment kipp gas generator according to claim 5, it is characterised in that the feeding-in solid body tube top Portion is provided with seal cover board.
CN201720556558.7U 2017-05-18 2017-05-18 A kind of chemical experiment kipp gas generator Expired - Fee Related CN207153661U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720556558.7U CN207153661U (en) 2017-05-18 2017-05-18 A kind of chemical experiment kipp gas generator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720556558.7U CN207153661U (en) 2017-05-18 2017-05-18 A kind of chemical experiment kipp gas generator

Publications (1)

Publication Number Publication Date
CN207153661U true CN207153661U (en) 2018-03-30

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Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252207A (en) * 2019-05-27 2019-09-20 陈祖友 A kind of chemical reaction filter device convenient for extracting gas
CN115855603A (en) * 2023-01-03 2023-03-28 成都理工大学 Device and method for efficiently extracting pyrite sulfur in ancient sediments

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252207A (en) * 2019-05-27 2019-09-20 陈祖友 A kind of chemical reaction filter device convenient for extracting gas
CN110252207B (en) * 2019-05-27 2021-07-27 山东沾化天元精细化工有限公司 Chemical reaction filter equipment convenient to extract gas
CN115855603A (en) * 2023-01-03 2023-03-28 成都理工大学 Device and method for efficiently extracting pyrite sulfur in ancient sediments

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180330

Termination date: 20180518

CF01 Termination of patent right due to non-payment of annual fee