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CN206772322U - A kind of two-parameter detecting system for surpassing surface based on medium - Google Patents

A kind of two-parameter detecting system for surpassing surface based on medium Download PDF

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Publication number
CN206772322U
CN206772322U CN201720490453.6U CN201720490453U CN206772322U CN 206772322 U CN206772322 U CN 206772322U CN 201720490453 U CN201720490453 U CN 201720490453U CN 206772322 U CN206772322 U CN 206772322U
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China
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medium
super surface
resonance
refractive index
sensitivity
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CN201720490453.6U
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胡杰
郎婷婷
吴梦茹
赵瑞安
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China Jiliang University
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China Jiliang University
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Abstract

The utility model discloses a kind of two-parameter detecting system for surpassing surface based on medium, including the super surface probe of wideband light source, the polarizer, collimation lens, detection platform, medium, spectrometer.The light of wideband light source output is changed into parallel linearly polarized light after the polarizer, collimation lens, vertical normal incidence is to the super surface probe of medium being positioned in detection platform, according to rice formula scattering theory, there are at least two resonance peaks (electric resonance and the magnetic resonance that correspond to different orders respectively) in the transmitted spectrum of the super surface probe of medium.The two resonance peaks have different sensitivity to two kinds of external parameters.Spectrometer receives transmitted light, by analyzing the wavelength amount of movement combination sensitivity matrix of resonance peak, can measure two kinds of external parameter values simultaneously.The utility model is measured based on the super surface of medium to realize while two kinds of external parameters, and the super surface texture of medium is stable, and easily fabricated, cost is low, and size is small, and multi-channel detection is realized beneficial to integration packaging and in smaller size range.

Description

A kind of two-parameter detecting system for surpassing surface based on medium
Technical field
The utility model belongs to field of sensing technologies, is related to a kind of detection system that can measure two kinds of external parameters simultaneously System.
Background technology
In the manufacturing, environmental monitoring, food safety detection etc., often it is related to temperature, concentration, stress, folding The detection of the various parameter of rate, electric current, speed etc. is penetrated, country encourages the research about sensing detection technology.And can be right The sensor-based system that at least two external parameters carry out measurement simultaneously can be not only solved in measurement process between external parameter Influence each other, detection efficiency can also be greatly improved.
In existing two-parameter sensing technology, optical fiber sensing technology is most common, also there is some other two-parameter biographies Sensor.Such as China Measures Institute's on January 15th, 2014 propose Application No. 201420024605.X " be based on long period light Fine grating refractive index temperature biparameter measurement sensor ", the sensor include light supply apparatus, Transmission Fibers, sensor fibre and Spectrometer, two sections are carved with the sensor fibre and is connected with each other but LPFG that the cycle is different, two structures only have One of them has coat, so refractive index and temperature have different sensitivity respectively, flashlight passes through the sense light Fibre can produce two resonance peaks, and as the change of refractive index and temperature produces different degrees of drift respectively, it is same so as to reach When detect the purpose of refractive index and temperature.Such as the Application No. of Central China University of Science and Technology's application on December 29th, 2014 201410834615.4 propose " Fibre Optical Sensor unit and its application for measuring refractive index temperature at the same time ", Fibre Optical Sensor unit Including input single-mode fiber, micro-nano multimode fibre, reflection multimode fibre and a reflection end face.Interference in Fibre Optical Sensor unit Optical signal transmission is demodulated the wavelength that device receives and demodulates interference spectrum to reflection end face generating unit point reflection, interference spectrum With Strength Changes amount, that is, measured while realizing refractive index and temperature.But the material of optical fiber, structure self character determine light Fiber sensor volume can not be made very small, and integrated level is low.And fibre optical sensor performance is unstable, repeatability is poor.2016 1 The moon 7, Zhejiang University proposes a kind of " temperature/refraction based on cascade coupled microcavity of Application No. 201610014723.6 Rate biparameter sensor ", including wideband light source, bus waveguide, the first coupled micro-cavity, the second coupled micro-cavity and photo-detector.The One coupled micro-cavity, the second coupled micro-cavity have different resonance wavelength and different Light Energy distribution proportions, micro- using two kinds Significant difference of the chamber in response of refractive index sensitivity and temperature-responsive sensitivity, just can realize in one-shot measurement while obtain Refractive index, temperature information.But this sensor needs to make a series of micro-cavity structure in waveguide, to processing technology requirement It is very high, it is careless slightly result to be affected greatly, and also work flow is complicated, is not suitable for volume production, and time cost is high.
Super surface be a kind of engineer can be in the micro-structure that sub-wavelength scope interior focusing is regulated and controled.Due to its chi It is very little it is small, prepare it is simple, there is smaller loss for the large-scale component that can realize said function, attract Numerous researchers are explored.Regulation and control etc. have research before nonlinear optics, small Molecular Detection, light wave is realized. In recent years, the super surface of the medium especially super surface of silicon substrate is due to abundant and with semiconductor fabrication process the compatibility of raw material And get most of the attention, but the sensor for being also not based on super surface texture up to now can realize at least two parameters while carry out Detection.
Utility model content
For in the prior art the defects of and present Research, the utility model provides a kind of surpasses the double of surface based on medium Parameter detecting system.
To achieve these goals, technical solution adopted in the utility model is:
A kind of two-parameter detecting system for surpassing surface based on medium, including wideband light source, the polarizer, collimation lens, detection The super surface probe of platform, medium, spectrometer.The light of wideband light source output is changed into parallel after the polarizer, collimation lens successively Linearly polarized light, vertical normal incidence to the super surface probe of the medium with periodic structure being positioned in detection platform, due to The transmission spectrum of the super surface probe of medium has at least two resonance peaks different to two kinds of external parameter sensitivity, passes through analysis The wavelength amount of movement combination sensitivity matrix of resonance peakIt can measure to obtain two external parameters simultaneouslyWherein A and B represents two external parameters, Δ λ respectively1With Δ λ2It is two selected Resonance peak wavelength shift, sensitivity matrix is before formal measurement, when surpassing surface probe to medium and demarcating Determine, wherein KA, 1And KA, 2It is the sensitivity of two resonance peaks when external parameter A changes, and external parameter B keeps constant, KB, 1And KB, 2It is the sensitivity of two resonance peaks when external parameter B changes, and external parameter A keeps constant.
A kind of two-parameter detecting system for surpassing surface based on medium described in the utility model, it is characterised in that:Described Groove is carved with detection platform, length and width is consistent with the size of the super surface probe of medium, and depth is more than the super surface of medium The thickness of sensor, the detection platform only has groove can be with printing opacity, and light intensity is influenceed to ignore, and other positions are not The light that can export wideband light source passes through.
A kind of two-parameter detecting system for surpassing surface based on medium described in the utility model, it is characterised in that:Described The super surface probe of medium, is made up of periodic cellular construction, and backing material is low refractive index dielectric, and cellular construction material is High refractive index medium, cycle are less than incident wavelength;Also, in its transmission spectrum at least two to two kinds of external parameter sensitivity not Same resonance peak.
A kind of two-parameter detecting system for surpassing surface based on medium described in the utility model, it is characterised in that:Described Spectrometer can measure the light intensity under each wavelength of the wideband light source output, and wavelength resolution is less than 0.1nm.
Compared with prior art, characteristic of the present utility model is with advantage:
1. the utility model is to be measured based on the super surface of medium to realize while two kinds of external parameters, the super surface knot of medium Structure is stable, and size is small, is easily integrated encapsulation, and is advantageous to realize multi-channel detection in less size.
2. the utility model is to be measured based on the super surface of medium to realize while two kinds of external parameters, the super surface of medium with Existing semiconductor fabrication process is fully compatible, prepares simply, is adapted to extensive a large amount of productions, reduces cost.
3. the utility model is to be measured based on the super surface of medium to realize while two kinds of external parameters, because medium surpasses table The material in face, size can be selected arbitrarily so that the spectrum service band of the sensor is almost unrestricted, and limitation is smaller.
Brief description of the drawings
, below will be to embodiment in order to illustrate more clearly of the utility model embodiment or technical scheme of the prior art Or the required accompanying drawing used is briefly described in description of the prior art.It should be evident that drawings in the following description are these Some embodiments of utility model, for those of ordinary skill in the art, on the premise of not paying creative work, also Other accompanying drawings can be obtained according to these accompanying drawings.
Fig. 1 is a kind of schematic diagram for the two-parameter detecting system for surpassing surface based on medium of the utility model
Fig. 2 is length of side 600nm, thickness 220nm silicon square (refractive index 3.7), is periodic arrangement in dioxy using 800nm The transmitted light spectrogram of the super surface texture formed in SiClx (refractive index 1.48) substrate
Fig. 3 is length of side 600nm, thickness 220nm silicon square (refractive index 3.7), is periodic arrangement in dioxy using 800nm The super surface texture formed in SiClx (refractive index 1.48) substrate is when occurring magnetic resonance and electric resonance, the electricity at silico briquette section Field distribution and Distribution of Magnetic Field.
Fig. 4 is a kind of Jie of two-parameter detecting system for surpassing surface based on medium in the utility model specific embodiment 1 The structure and illumination schematic diagram of the super surface probe of matter
Fig. 5 is a kind of two-parameter detecting system (a) inspection for surpassing surface based on medium in the utility model specific embodiment 1 Transmitted spectrum, (b) variations in refractive index for surveying the solution of different refractivity are linear with the relation curve of resonance peak wavelength shift Transmitted spectrum, (d) temperature change and the relation curve of resonance peak wavelength shift that fitting, (c) are obtained at different temperatures Linear fit
Fig. 6 is a kind of the another of two-parameter detecting system for surpassing surface based on medium in the utility model specific embodiment 2 A kind of structure and illumination schematic diagram of the super surface probe of medium
Fig. 7 is a kind of two-parameter detecting system (a) inspection for surpassing surface based on medium in the utility model specific embodiment 2 Transmitted spectrum, (b) variations in refractive index for surveying the solution of different refractivity are linear with the relation curve of resonance peak wavelength shift Transmitted spectrum, (d) temperature change and the relation curve of resonance peak wavelength shift that fitting, (c) are obtained at different temperatures Linear fit
Embodiment
Below in conjunction with the accompanying drawings and specific embodiment the utility model is described in further detail.
As shown in figure 1, a kind of two-parameter detecting system for surpassing surface based on medium, including wideband light source (1), the polarizer (2), collimation lens (3), detection platform (4), the super surface probe of medium (5), spectrometer (6);The light of wideband light source (1) output It is changed into parallel linearly polarized light after the polarizer (2), collimation lens (3) successively, vertical normal incidence is to being positioned in detection platform (4) The super surface probe of the medium with periodic structure (5), due to medium surpass surface probe (5) transmission spectrum have at least Two resonance peaks different to two kinds of external parameter sensitivity, by analyzing the wavelength amount of movement of resonance peak and combining sensitivity square Battle arrayTwo external parameters can be obtained simultaneouslyWherein A and B points Two external parameters, Δ λ are not represented1With Δ λ2It is the wavelength shift of two selected resonance peaks, sensitivity matrix is formal Before measurement, surface probe (5) is surpassed to medium and carries out marking timing determination, wherein KA, 1And KA, 2It is to work as external parameter A to change, The sensitivity of two resonance peaks, K when external parameter B keeps constantB, 1And KB, 2It is that external parameter A is kept when external parameter B changes The sensitivity of two resonance peaks when constant.
In addition, being carved with groove on detection platform (4) described in the utility model, length and width senses with the super surface of medium The size of device (5) is consistent, and depth is more than the thickness of the super surface probe of medium (5);The detection platform (4) only has groove can With printing opacity, and light intensity is influenceed to ignore, the light that other positions can not export wideband light source (1) passes through.
The super surface probe of medium (5) described in the utility model, is made up of, backing material is periodic cellular construction Low refractive index dielectric, cellular construction material are high refractive index medium, and the cycle is less than incident wavelength;Also, in its transmission spectrum at least There are two resonance peaks different to two kinds of external parameter sensitivity.
Spectrometer (6) described in the utility model can measure the light intensity under each wavelength of the wideband light source (1) output, Wavelength resolution is less than 0.1nm.
It is illustrated in figure 2 length of side 600nm, thickness 220nm silicon square (refractive index 3.7), using 800nm as periodic arrangement The transmitted light spectrogram of the super surface texture formed in silica (refractive index 1.48) substrate.It is from figure 2 it can be seen that each The transmissivity of individual wavelength is related to wavelength, and the transmissivity near 1.42 μm and 1.63 mum wavelengths is extremely low, close to 0, this be because For the incident electromagnetic wave near the two wavelength, there occurs magnetic resonance (1.42 μm) and electric resonance respectively with super surface texture (1.63 μm), form two resonance peaks;And the transmissivity of wavelength is higher beyond the two resonance peaks, the super table of medium is embodied The smaller loss in face.
Length of side 600nm is illustrated in figure 3, thickness 220nm silico briquette (refractive index 3.7), is existed by periodic arrangement of 800nm The super surface texture formed in silica (refractive index 1.48) substrate is when occurring magnetic resonance and electric resonance, at silico briquette section Electric Field Distribution and Distribution of Magnetic Field.Fig. 3 (a) is partly and (c) part is that the electric field at section during magnetic resonance occurs for silico briquette respectively Distribution and Distribution of Magnetic Field, it can be seen that magnetic field is enriched in inside silico briquette and parallel to x-axis, and electric field is in be vortexed in y-z plane Shape, show the characteristic of magnetic dipole.Fig. 3 (b) is partly and (d) part is that the electricity at section during electric resonance occurs for silico briquette respectively Field distribution and Distribution of Magnetic Field, it can be seen that electric field is enriched in inside silico briquette and parallel to y-axis, and magnetic field is in be vortexed in x-z-plane Shape, show the characteristic of electric dipole.
Below by taking two external parameters of refractive index and temperature as an example, illustrate the utility model proposes biparameter sensor Operation principle.
In measurement process, the change of refractive index and the change of temperature, it can all cause the skew of resonance peak wavelength, i.e.,:
Wherein i represents the resonance peak 1 (magnetic resonance) or resonance peak 2 (electric resonance) in transmitted spectrum.In order to realize refractive index, Temperature biparameter senses, it would be desirable to uses the wavelength shift of the two resonance peaks.Formula (1) is by arranging, after transposition, i.e., For:
Here KN, 1, KN, 2, KT, 1, KT, 2The sensitivity of sensor response when being all refractive index and the single change of temperature.
The position of two resonance peak wavelength of (certain temperature and refractive index) is first demarcated under certain reference state, then measures two Resonance peak wavelength is respectively with the variation relation of single parameter (refractive index or temperature), i.e. variations in refractive index sensitivity KN, 1、 KN, 2With temperature change sensitivity KT, 1、KT, 2, it is finally immersed in certain testing sample, measures the offset of two resonance peak wavelength Δλ1With Δ λ2, the refractive index and temperature demarcated at the beginning can be contrasted in the hope of the variable quantity of refractive index and temperature by formula (2) Reference value, it is possible to obtain current refractive index and temperature.
It is illustrated with reference to specific embodiment.
Embodiment 1:
A kind of super surface probe of silicon substrate is devised, as shown in figure 4, silico briquette array periodicity is arranged in silica substrate On, a branch of parallel linearly polarized light kiNormal incidence surpasses on surface to silicon substrate, transmitted light ktIt is collected and is analyzed.Incident electromagnetic wave edge Z-axis normal incidence, direction of an electric field is parallel to y-axis, and magnetic direction is parallel to x-axis.The refractive index of silica is at 20 DEG C 1.48, the refractive index of silico briquette is 3.7 at 20 DEG C.Fig. 4 lower right corner is the partial enlarged drawing of super surface texture, and the arrangement of silico briquette is all Phase PxAnd PyAll it is 800nm, the length of side a of silico briquette is 600nm, and the thickness of silico briquette is 220nm.
It is placed on super surface texture is smooth in the groove of detection platform, surface adds the solution (1.33- of different refractivity 1.49) super surface texture is totally submerged, and it is 20 DEG C to control temperature constant, obtains sensor and is immersed in different refractivity liquid Transmitted spectrum, as shown in Fig. 5 (a) part, it can be seen that the wavelength of two resonance peaks is all with the increase of refractive index and to length Different degrees of skew occurs for ripple direction.Resonance peak wavelength shift corresponding to different refractivity is subjected to linear fit, such as Fig. 5 (b) shown in part, magnetic resonance and electric resonance are 243.44nm/RIU and 159.43nm/ for the response sensitivity of variations in refractive index RIU, linearity R2Also all close to 1, reflecting between them has preferable linear relationship.
It is placed on super surface texture is smooth in the groove of detection platform, surface is air (refractive index 1).Consulting literatures It is 1.84 × 10 respectively that data, which obtains silicon and the thermo-optical coeffecient of silica,-4/ K and 8.6 × 10-6The heat of/K, silicon and silica The coefficient of expansion is 2.59 × 10 respectively-6/ K and 0.55 × 10-6/K.Temperature is increased to 100 DEG C from 0 DEG C, obtains super surface texture Transmitted light spectrogram at different temperatures, as shown in Fig. 5 (c) part, two vignettes beside resonance peak are two respectively The enlarged drawing of resonance peak wavelength change, it can be seen that the wavelength of two resonance peaks all occurs in various degree with the change of temperature Change.Temperature change and the relation of resonance peak wavelength shift are subjected to linear fit, as shown in Fig. 5 (d) part, magnetic is humorous It is 51.83pm/ DEG C and 76.35pm/ DEG C for the response sensitivity of variations in refractive index to shake with electric resonance, linearity R2Also it is all close In 1, reflecting between them has preferable linear relationship.Bring the above results into formula (2), we can obtain:
Formula (3) is the sensitivity square of the refractive index of detecting system described in embodiment 1, temperature biparameter while measurement Battle array.
Embodiment 2:
The super surface probe of silicon substrate of another structure is devised, as shown in fig. 6, silico briquette array periodicity is arranged in two Aoxidize in silicon base, a branch of parallel linearly polarized light kiNormal incidence surpasses on surface to silicon substrate, transmitted light ktIt is collected and is analyzed.Two The refractive index of silica is 1.48 at 20 DEG C, and the refractive index of silico briquette is 3.7 at 20 DEG C.It is super surface texture on the right of Fig. 6 Partial enlarged drawing, the arrangement period P of silico briquettexAnd PyAll it is 800nm, the length of side a of silico briquette is 600nm, and the thickness of silico briquette is 220nm, 4 apertures are symmetrically hollowed out on each silico briquette, the length of side of each aperture is 130nm, between aperture and aperture Interval be 140nm, form a kind of sphere of movements for the elephants shape structure.
It is placed on super surface texture is smooth in the groove of detection platform, surface adds the solution (1.33- of different refractivity 1.49) super surface texture is totally submerged, and it is 20 DEG C to control temperature constant, is collected into the sensing being immersed in different refractivity liquid The transmitted spectrum of device, as shown in Fig. 7 (a) part, it can be seen that the wavelength of two resonance peaks all with the increase of refractive index and Different degrees of skew occurs to long wave direction.Resonance peak wavelength shift corresponding to different refractivity is subjected to linear fit, such as Shown in Fig. 7 (b) part, magnetic resonance and electric resonance for variations in refractive index response sensitivity for 306.71nm/RIU and Also all close to 1, reflecting between them has preferable linear relationship by 204.27nm/RIU, linearity R2.
It is placed on super surface texture is smooth in the groove of detection platform, surface is air (refractive index 1).Consulting literatures It is 1.84 × 10 respectively that data, which obtains silicon and the thermo-optical coeffecient of silica,-4/ K and 8.6 × 10-6The heat of/K, silicon and silica The coefficient of expansion is 2.59 × 10 respectively-6/ K and 0.55 × 10-6/K.Temperature is increased to 100 DEG C from 0 DEG C, obtains super surface texture Transmitted light spectrogram at different temperatures, as shown in Fig. 7 (c) part, two vignettes beside resonance peak are two respectively The enlarged drawing of resonance peak wavelength change, it can be seen that the wavelength of two resonance peaks all occurs in various degree with the change of temperature Change.Temperature change and the relation of resonance peak wavelength shift are subjected to linear fit, as shown in Fig. 7 (d) part, magnetic is humorous It is 35.01pm/ DEG C and 69.1pm/ DEG C for the response sensitivity of variations in refractive index to shake with electric resonance, linearity R2Also it is all close In 1, reflecting between them has preferable linear relationship.Bring the above results into formula (2), we can obtain:
Formula (4) is the sensitivity square of the refractive index of detecting system described in embodiment 2, temperature biparameter while measurement Battle array.
It is pointed out that above-described embodiment is only to illustrate technical concept and feature of the present utility model, its object is to Allow person skilled in the art to understand content of the present utility model and implement according to this, this practicality can not be limited according to this New protection domain.All equivalent transformations made according to the utility model Spirit Essence or modification, should all cover in this practicality Within new protection domain.

Claims (4)

1. a kind of two-parameter detecting system for surpassing surface based on medium, including wideband light source (1), the polarizer (2), collimation lens (3), detection platform (4), the super surface probe of medium (5), spectrometer (6);The light of wideband light source (1) output is successively through the polarizer (2), it is changed into parallel linearly polarized light after collimation lens (3), vertical normal incidence is to being positioned over having periodically in detection platform (4) The super surface probe of medium (5) of structure, because the transmission spectrum that medium surpasses surface probe (5) has outside at least two pairs two kinds The different resonance peak of boundary's parametric sensitivity, by the wavelength amount of movement combination sensitivity matrix for analyzing resonance peak It can measure to obtain two external parameters simultaneouslyWherein A and B represents two respectively External parameter, Δ λ1With Δ λ2The wavelength shift of two selected resonance peaks, sensitivity matrix be before formal measurement, Surpass surface probe (5) to medium to carry out marking timing determination, wherein KA, 1And KA, 2It is as external parameter A changes, external parameter B The sensitivity of two resonance peaks, K when keeping constantB, 1And KB, 2It is when external parameter B changes, and external parameter A keeps constant two The sensitivity of individual resonance peak.
A kind of 2. two-parameter detecting system for surpassing surface based on medium according to claim 1, it is characterised in that:Described Groove is carved with detection platform (4), length and width is consistent with the size of the super surface probe of medium (5), and depth is more than medium The thickness of super surface probe (5);The detection platform (4) only has groove can be with printing opacity, and light intensity is not influenceed, other The light that position can not export wideband light source (1) passes through.
A kind of 3. two-parameter detecting system for surpassing surface based on medium according to claim 1, it is characterised in that:Described The super surface probe of medium (5), is made up of periodic cellular construction, and backing material is low refractive index dielectric, cellular construction material Expect to be less than incident wavelength for high refractive index medium, cycle;Also, in its transmission spectrum at least two it is sensitive to two kinds of external parameters Spend different resonance peaks.
A kind of 4. two-parameter detecting system for surpassing surface based on medium according to claim 1, it is characterised in that:Described Spectrometer (6) can measure the light intensity under each wavelength of the wideband light source (1) output, and wavelength resolution is less than 0.1nm.
CN201720490453.6U 2017-04-28 2017-04-28 A kind of two-parameter detecting system for surpassing surface based on medium Expired - Fee Related CN206772322U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107340004A (en) * 2017-04-28 2017-11-10 中国计量大学 A kind of two-parameter detecting system for surpassing surface based on medium
CN109085667A (en) * 2018-07-05 2018-12-25 华中科技大学 A kind of super surface achromatism line polarisation lens
CN117571818A (en) * 2023-12-01 2024-02-20 广州航海学院 Reverse transmission aqueous solution dielectric function test method and sensor thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107340004A (en) * 2017-04-28 2017-11-10 中国计量大学 A kind of two-parameter detecting system for surpassing surface based on medium
CN107340004B (en) * 2017-04-28 2023-09-22 中国计量大学 Double-parameter detection system based on medium super surface
CN109085667A (en) * 2018-07-05 2018-12-25 华中科技大学 A kind of super surface achromatism line polarisation lens
CN117571818A (en) * 2023-12-01 2024-02-20 广州航海学院 Reverse transmission aqueous solution dielectric function test method and sensor thereof
CN117571818B (en) * 2023-12-01 2024-08-20 广州航海学院 Reverse transmission aqueous solution dielectric function test method and sensor thereof

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