CN205683600U - The vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary - Google Patents
The vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary Download PDFInfo
- Publication number
- CN205683600U CN205683600U CN201620522409.4U CN201620522409U CN205683600U CN 205683600 U CN205683600 U CN 205683600U CN 201620522409 U CN201620522409 U CN 201620522409U CN 205683600 U CN205683600 U CN 205683600U
- Authority
- CN
- China
- Prior art keywords
- ultrasound bath
- exhaust tube
- sample bottle
- vacuum pump
- thermal drivers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses the vacuum concentrating apparatus of a kind of ultrasonic combined thermal drivers auxiliary, to solve tradition concentrator, to concentrate speed slow and would generally cause reducing or the problem of loss of its activity.It includes that ultrasound bath, glass fill sample bottle, vacuum pump, the bottom of ultrasound bath is provided with recirculated water entrance, the upper side of ultrasound bath is provided with circulating water outlet, glass dress sample bottle is placed in ultrasound bath, the bottleneck of glass dress sample bottle is fixed on exhaust tube by heat insulation seal washer, the other end of exhaust tube connects vacuum pump, and exhaust tube is provided with heating mantle at vacuum pump.This device at low pressure, ultrasonic cavitation effect and steam molecule by under the synergy of thermal drivers, it is achieved that water extract rapid concentration at normal temperatures.Convenient operation, adaptability scope is wide, rapidly and efficiently low cost.
Description
Technical field
This utility model belongs to concentrator field, particularly relates to being concentrated in vacuo of a kind of ultrasonic combined thermal drivers auxiliary
Device.
Background technology
In the extraction preparation field of natural bioactivity substance, the extraction cost of water solubility extract is minimum, and operation is the most
Convenience and safety, and due to its water-soluble character, the application of this kind of natural active matter is the most extensive, using value
Also maximum.But compared with other lower boiling organic extraction solvent, the boiling point of this solvent of water is higher, so extract
Concentrating and removal process cost is high, difficulty is big.And for the water extract of some thermal sensitivitys, traditional concentration technique speed
And reduction or the loss of its activity would generally be caused slowly,.And freezing vacuum concentration technique is due to its apparatus expensive, applied sample amount is little
Feature, limits its sizable application and popularization.
Utility model content
The purpose of this utility model is a kind of convenient operation, and adaptability scope is wide, rapidly and efficiently the ultrasound wave connection of low cost
Closing the vacuum concentrating apparatus of thermal drivers auxiliary, to solve tradition concentrator, to concentrate speed slow and would generally cause the fall of its activity
Problem that is low or that lose.
The purpose of this utility model can be by realizing by the following technical solutions: a kind of ultrasonic combined thermal drivers is auxiliary
The vacuum concentrating apparatus helped, including ultrasound bath, glass dress sample bottle, vacuum pump, the bottom of ultrasound bath is provided with recirculated water
Entrance, the upper side of ultrasound bath is provided with circulating water outlet, and glass dress sample bottle is placed in ultrasound bath, glass dress sample bottle
Bottleneck be fixed on exhaust tube by heat insulation seal washer, the other end of exhaust tube connects vacuum pump, near true on exhaust tube
It is provided with heating mantle at empty pump.By the steam in its heating exhaust tube, that accelerates steam extracts process.
As improving further, recirculated water entrance and circulating water outlet form one by heat radiation comb and water circulating pump and follow
Ring water loop.
As improving further, the bottleneck of glass dress sample bottle is fixed on exhaust tube by holder.
This device at low pressure, ultrasonic cavitation effect and steam molecule by under the synergy of thermal drivers, it is achieved that water
Extract rapid concentration at normal temperatures.
Ultrasound bath system provides ultrasound wave, and recirculated water keeps water-bath by fin and is concentrated water extract
Temperature near room temperature, it is to avoid extract temperature is too high.Which solves the technology barrier that ultrasound wave can not be propagated in vacuum, super
Sound wave reaches extract system by containing the glass medium of the container of extract, improves ultrasonic cavitation effect, Qi Zhongrong
Agent water preferential absorption and transmission ultrasonic energy, hydrone rapid evaporation under the low pressure of vacuum pump.Rise through at hydrone
During the thermal treatment zone, accepting heat energy further, molecular motion aggravation is also extracted rapidly by vacuum pump, improves thing liquid level to be concentrated with true
Hydrone Concentraton gradient between empty pump interface, thereby results in hydrone steam bigger between the thermal treatment zone and the extract page
Pressure reduction, this pressure reduction accelerates hydrone from extract system to the transfer in vacuum pump district, it is achieved the purpose of rapid concentration.This device
Effectively overcome ultrasound wave in prior art to propagate in region of no pressure and cause the open defect that can not realize cavitation effect, real
Show effective combination of ultrasound wave and vacuum technique.Further, since recirculated water is by the heat exchange of the comb that dispels the heat, it is ensured that whole
In concentration process, the temperature being concentrated thing is in near-ambient temperature all the time, it is achieved that extract concentration at a temperature of near-ambient,
Avoid heat damage effect.
Accompanying drawing explanation
Fig. 1 is the structural representation of the vacuum concentrating apparatus of a kind of ultrasonic combined thermal drivers auxiliary.
Reference implication is as follows: 1 vacuum pump；2 heating mantles；3 exhaust tubes；4 holders；5 adiabatic sealings
Packing ring；6 glass dress sample bottles；7 ultrasound baths, 8 recirculated water entrances；9 water circulating pumps, 10 heat radiation combs；11—
Circulating water outlet.
Detailed description of the invention
Below in conjunction with the accompanying drawings this utility model is further illustrated.
The vacuum concentrating apparatus of a kind of ultrasonic combined thermal drivers auxiliary, including ultrasound bath 7, glass dress sample bottle 6, true
Empty pump 1, the bottom of ultrasound bath 7 is provided with recirculated water entrance 8, and the upper side of ultrasound bath 7 is provided with circulating water outlet 11,
Glass dress sample bottle 6 is placed in ultrasound bath 7, and the bottleneck of glass dress sample bottle 6 is fixed on exhaust tube 3 by heat insulation seal washer 5
On, the other end of exhaust tube 3 connects vacuum pump 1, and exhaust tube 3 is provided with heating mantle 2 at vacuum pump.Heating mantle is by outside
Power supply is heated by resistance.
Recirculated water entrance 8 and circulating water outlet 11 form a circulating water loop by heat radiation comb 10 and water circulating pump 9.
The bottleneck of glass dress sample bottle 6 is fixed on exhaust tube 3 by holder 4.
During use, being placed in by extract to be concentrated in glass dress sample bottle 6, its bottleneck is fixed by heat insulation seal washer 5
Device 4 is fixed on exhaust tube 3, and the bottle of glass dress sample bottle 6 is placed in ultrasound bath 7, and its water body is by heat radiation comb 10 He
Water circulating pump 9 forms a circulating water loop, switches on power and makes ultrasound bath 7 start working, and water circulating pump 9 makes water body simultaneously
Bottom in and top out starts the cycle over, and heat radiation comb 10 guarantees that water temperature is close to ambient temperature；Vacuum pump 1 is started working, low pressure and ultrasonic
Ripple cavitation effect makes hydrone rapid evaporation, and is extracted by vacuum pump, and water vapour molecule is provided energy to accelerate by heating mantle simultaneously
Its motion, rapidly enters vacuum pump, improves the vapor water molecular concentration gradient between thing liquid level to be concentrated and vacuum pump, accelerate
Hydrone from liquid level end to the transfer of vacuum pump end, it is achieved the purpose of rapid concentration.
Claims (3)
1. the vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary, it is characterised in that: it include ultrasound bath (7),
Glass dress sample bottle (6), vacuum pump (1), the bottom of ultrasound bath (7) is provided with recirculated water entrance (8), ultrasound bath (7)
Upper side is provided with circulating water outlet (11), and glass dress sample bottle (6) is placed in ultrasound bath (7), the bottle of glass dress sample bottle (6)
Mouth is fixed on exhaust tube (3) by heat insulation seal washer (5), and the other end of exhaust tube (3) connects vacuum pump (1), exhaust tube
(3) it is provided with heating mantle (2) at upper close vacuum pump.
The vacuum concentrating apparatus of ultrasonic combined thermal drivers the most according to claim 1 auxiliary, it is characterised in that: recirculated water
Entrance (8) and circulating water outlet (11) are by heat radiation comb (10) and water circulating pump (9) one circulating water loop of composition.
The vacuum concentrating apparatus of ultrasonic combined thermal drivers the most according to claim 1 and 2 auxiliary, it is characterised in that: glass
The bottleneck of glass dress sample bottle (6) is fixed on exhaust tube (3) by holder (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620522409.4U CN205683600U (en) | 2016-06-01 | 2016-06-01 | The vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620522409.4U CN205683600U (en) | 2016-06-01 | 2016-06-01 | The vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205683600U true CN205683600U (en) | 2016-11-16 |
Family
ID=57263391
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620522409.4U Expired - Fee Related CN205683600U (en) | 2016-06-01 | 2016-06-01 | The vacuum concentrating apparatus of ultrasonic combined thermal drivers auxiliary |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205683600U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021082448A1 (en) * | 2020-06-05 | 2021-05-06 | 广州理文科技有限公司 | Apparatus for ultrasonic wave-assisted drying of lithium battery electrolyte, and drying method |
-
2016
- 2016-06-01 CN CN201620522409.4U patent/CN205683600U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021082448A1 (en) * | 2020-06-05 | 2021-05-06 | 广州理文科技有限公司 | Apparatus for ultrasonic wave-assisted drying of lithium battery electrolyte, and drying method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161116 Termination date: 20170601 |