CN1817226A - Production of diet fibre with high activity - Google Patents
Production of diet fibre with high activity Download PDFInfo
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- CN1817226A CN1817226A CNA2006100167202A CN200610016720A CN1817226A CN 1817226 A CN1817226 A CN 1817226A CN A2006100167202 A CNA2006100167202 A CN A2006100167202A CN 200610016720 A CN200610016720 A CN 200610016720A CN 1817226 A CN1817226 A CN 1817226A
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- dietary fiber
- alfalfa
- microwave
- citric acid
- grass meal
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Abstract
一种高活性膳食纤维的制备方法,属于保健食品领域。本发明的目的在于利用天然植物,以紫花苜蓿干草为原料,加入柠檬酸和酒石酸来生产高活性膳食纤维的制备方法。本发明首先将苜蓿草切割成草粉洗净,再将湿草粉加入微波加热器中,加入氢氧化钠溶液,用微波进行加热,重复一次加热,所得的中性湿草粉中加入过氧化氢液浸泡后,用纯水洗至中性,放入微波干燥机内进行干燥后进行超微粉碎,加入柠檬酸和酒石酸,搅拌均匀,即得高活性苜蓿膳食纤维。本发明适用范围广泛,即是天然植物源的优质食品添加剂,也是效果良好的功能食品,总膳食纤维含量高达75%以上。可以制作成胶囊、片剂、针剂等。The invention discloses a preparation method of highly active dietary fiber, which belongs to the field of health food. The object of the present invention is to utilize natural plant, take alfalfa hay as raw material, add citric acid and tartaric acid to produce the preparation method of high activity dietary fiber. In the present invention, the alfalfa grass is first cut into grass powder and cleaned, then the wet grass powder is added to a microwave heater, sodium hydroxide solution is added, and the microwave is used to heat, and the heating is repeated once, and the obtained neutral wet grass powder is added with peroxide After soaking in hydrogen solution, wash with pure water until neutral, put it into a microwave dryer for drying, and then perform ultrafine grinding, add citric acid and tartaric acid, and stir evenly to obtain high-activity alfalfa dietary fiber. The invention has a wide application range, not only a high-quality food additive of natural plant source, but also a functional food with good effect, and the total dietary fiber content is as high as 75%. It can be made into capsules, tablets, injections, etc.
Description
技术领域:Technical field:
本发明属于保健食品领域。The invention belongs to the field of health food.
背景技术:Background technique:
近年来,由于国民生活水平的提高,膳食结构的改变,也造成了高蛋白、高脂肪食品摄入量的过多(主要是动物蛋白和脂肪),谷物食品摄取的精细度高,而膳食纤维的摄入比例则相对减少,很多与膳食结构相关的“文明病”明显上升。例如,顽固性便秘、结肠炎、胆结石、糖尿病、动脉硬化、高脂血症、肥胖症等。想要预防这类“文明病”的发生及治疗这类疾病,首先应从膳食配餐着手,增加高活性膳食纤维的摄入量。因为膳食纤维对以上疾病的预防及治疗效果与它们本身的性能及成分均有显著的相关性。In recent years, due to the improvement of national living standards and changes in dietary structure, excessive intake of high-protein and high-fat foods (mainly animal protein and fat) has also been caused. The fineness of grain food intake is high, and dietary fiber The proportion of intake of food is relatively reduced, and many "civilization diseases" related to dietary structure have increased significantly. For example, intractable constipation, colitis, gallstones, diabetes, arteriosclerosis, hyperlipidemia, obesity, etc. In order to prevent the occurrence of such "civilized diseases" and treat such diseases, we should first start with dietary catering and increase the intake of highly active dietary fiber. Because the preventive and therapeutic effects of dietary fiber on the above diseases are significantly related to their own performance and components.
随着现代“文明病”的出现以及对其功能的研究,使人们越来越多的认识到膳食纤维在营养保健上的重要性,对膳食纤维的研究开发也投入了极大的热情,欧、美、日等发达国家和地区已经研制和生产出不少品种的膳食纤维和高活性的膳食纤维食品,颇受消费者的欢迎。近年来,我国有关膳食纤维的提取、生产的报道也不少,但大多数产品的开发还停留在实验室的研究,尚未形成批量生产的规模;另一方面,对膳食纤维的认识,许多人仅理解为粗纤维和纤维素等,因此,开展对膳食纤维和膳食纤维功能食品的研究与开发,对促进人们身体健康,提高食品工业在国内国际市场上的竞争力有重要的现实意义。大量试验证明使用膳食纤维在降低血脂、防止便秘、预防癌症及心血管疾病等均有显著的临床疗效。这已被国内外大量的研究事实与流行病学调查结果所证实,并将其应用于食品工业中。With the emergence of modern "disease of civilization" and the research on its function, more and more people realize the importance of dietary fiber in nutrition and health care, and they have also invested great enthusiasm in the research and development of dietary fiber. Developed countries and regions such as Japan, the United States, and Japan have developed and produced many varieties of dietary fiber and highly active dietary fiber foods, which are quite popular with consumers. In recent years, there have been many reports on the extraction and production of dietary fiber in my country, but the development of most products is still in the laboratory research, and has not yet formed a scale of mass production; on the other hand, many people have little understanding of dietary fiber. It is only understood as crude fiber and cellulose, etc. Therefore, the research and development of dietary fiber and dietary fiber functional food has important practical significance for promoting people's health and improving the competitiveness of the food industry in domestic and international markets. A large number of experiments have proved that the use of dietary fiber has significant clinical effects in reducing blood lipids, preventing constipation, preventing cancer and cardiovascular diseases. This has been confirmed by a large number of research facts and epidemiological findings at home and abroad, and it has been applied in the food industry.
技术内容:Technical content:
本发明的目的在于利用天然植物,以紫花苜蓿干草为原料来生产高活性膳食纤维的制备方法。The object of the present invention is to utilize natural plant, take alfalfa hay as raw material to produce the preparation method of high activity dietary fiber.
本发明的配方是:The formula of the present invention is:
苜蓿膳食纤维99%~97.5%,柠檬酸1.5%~0.5%,酒石酸1%~0.5%Alfalfa dietary fiber 99%-97.5%, citric acid 1.5%-0.5%, tartaric acid 1%-0.5%
本发明高活性膳食纤维的制备方法,其步骤是:The preparation method of high activity dietary fiber of the present invention, its steps are:
a、首先将苜蓿草用切割机切割成草粉,置入水槽中去泥洗净捞出;a. First, cut the alfalfa grass into grass powder with a cutting machine, put it in the water tank, remove the mud, wash it, and take it out;
b、再将湿草粉加入微波加热器中,加入氢氧化钠溶液,用微波进行加热,然后放掉加热液;b. Then add the wet grass powder into the microwave heater, add sodium hydroxide solution, heat with microwave, and then let go of the heating liquid;
c、重复b步骤一次,捞出后放入水槽中,将去杂质和活化处理的湿草粉用纯水洗至中性,捞出后,放入过滤槽中自然漏去水;c. Repeat step b once, take it out and put it in the water tank, wash the impurity-removed and activated wet grass powder with pure water until neutral, take it out, put it in the filter tank to drain the water naturally;
d、将上述所得的中性湿草粉放入塑料桶中,加入过氧化氢液浸泡,捞出后将水分淋出,再用纯水洗至中性,捞出后离心;d. Put the neutral wet grass powder obtained above into a plastic bucket, add hydrogen peroxide solution to soak, remove the water, then wash with pure water until neutral, remove and centrifuge;
e、再将d步骤所得的中性湿草粉放入微波干燥机内进行干燥,超微粉碎后即得高活性苜蓿膳食纤维原料;E, then put the neutral wet grass powder gained in step d into a microwave dryer for drying, and obtain high-activity alfalfa dietary fiber raw material after ultrafine pulverization;
f、在所得的高活性苜蓿膳食纤维原料中加入柠檬酸和酒石酸,搅拌均匀,即得高活性苜蓿膳食纤维。f. Add citric acid and tartaric acid to the obtained high-activity alfalfa dietary fiber raw material, and stir evenly to obtain high-activity alfalfa dietary fiber.
本发明适用范围广泛,即是天然植物源的优质食品添加剂,也是效果良好的功能食品,制备工艺与传统提取生产工艺比较,由于使用了微波加热浸提和微波加热干燥之技术,分别使加热浸提时间和干燥时间大大缩短,这样就节省了能源,从而使提取率显著提高,省工、省时、节省能耗。为了进一步提高加工提取得到的苜蓿膳食纤维在人体内发挥更好的生理活性的作用,使其膳食纤维的微粒表面积最大化,本发明使用了超微粉碎机,对其纤维进行超微粉碎,使苜蓿膳食纤维的最终粒经在40-100微米之间。高活性苜蓿膳食纤维中主要成分为:总膳食纤维和少量蛋白质及脂肪。其中总膳食纤维含量高达75%以上。本发明可以制作成胶囊、片剂、针剂等。The present invention has a wide range of applications. It is not only a high-quality food additive of natural plant sources, but also a functional food with good effects. Compared with the traditional extraction production process, the preparation process uses microwave heating extraction and microwave heating drying techniques, respectively. The extraction time and drying time are greatly shortened, which saves energy, thereby significantly improving the extraction rate, saving labor, time and energy. In order to further improve the alfalfa dietary fiber obtained by processing and extracting to play a better physiologically active role in the human body, and to maximize the particle surface area of the dietary fiber, the present invention uses a superfine pulverizer to pulverize the fiber to make The final particle diameter of alfalfa dietary fiber is between 40-100 microns. The main components of highly active alfalfa dietary fiber are: total dietary fiber and a small amount of protein and fat. Wherein the total dietary fiber content is as high as more than 75%. The present invention can be made into capsules, tablets, injections and the like.
具体实施方式:Detailed ways:
本发明的配方是:The formula of the present invention is:
苜蓿膳食纤维99%~97.5%,柠檬酸1.5%~0.5%,酒石酸1%~0.5%Alfalfa dietary fiber 99%-97.5%, citric acid 1.5%-0.5%, tartaric acid 1%-0.5%
本发明高活性膳食纤维的制备方法,其步骤是:The preparation method of high activity dietary fiber of the present invention, its steps are:
a、首先将含水量在14%以下的苜蓿草用切割机切割成草粉,切割粒径在2.5~3.5mm,置入水槽中去泥洗净捞出,得到湿草粉;a. First, cut the alfalfa with a water content below 14% into grass powder with a cutting machine, and the cutting particle size is 2.5-3.5mm, put it in a water tank to remove mud, wash it, and remove it to obtain wet grass powder;
b、再将湿草粉加入微波加热器中,加入干草粉重量的5~7倍的0.8~1.2%的氢氧化钠溶液,用微波频率为2450MHz的微波进行加热至95℃,然后放掉加热液;b. Then add the wet grass powder into the microwave heater, add 0.8-1.2% sodium hydroxide solution which is 5-7 times the weight of the dry grass powder, and heat it to 95°C with a microwave frequency of 2450MHz, and then let go of the heating liquid;
c、重复b步骤一次,捞出后放入水槽中,将去杂质和活化处理的湿草粉用纯水洗至中性,捞出后,放入过滤槽中自然漏去水;c. Repeat step b once, take it out and put it in the water tank, wash the impurity-removed and activated wet grass powder with pure water until neutral, take it out, put it in the filter tank to drain the water naturally;
d、将上述所得的中性湿草粉放入塑料桶中,加入7%过氧化氢液浸泡10~14小时,捞出后将水分淋出,再将活化处理的湿草粉用纯水洗至中性,PH值为6.5~7.5,捞出后离心;d. Put the above-mentioned neutral wet grass powder into a plastic bucket, add 7% hydrogen peroxide solution and soak for 10-14 hours, remove the water after taking it out, and then wash the activated wet grass powder with pure water until Neutral, PH value is 6.5~7.5, take out and centrifuge;
e、再将d步骤所得的中性湿草粉放入微波干燥机内进行干燥,微波频率为2450MHz,超微粉碎后即得高活性苜蓿膳食纤维原料。粉碎过程首先将干草粉进行粗粉碎,过80目筛,再将过80目筛的干燥粉进行超微粉碎,过150目筛。e, put the neutral wet grass powder gained in step d into a microwave dryer for drying, the microwave frequency is 2450MHz, and after ultrafine pulverization, the high-activity alfalfa dietary fiber raw material is obtained. In the crushing process, the dry grass powder is coarsely crushed and passed through an 80-mesh sieve, and then the dry powder passed through the 80-mesh sieve is ultrafinely crushed and passed through a 150-mesh sieve.
f、在所得的高活性苜蓿膳食纤维原料中加入柠檬酸和酒石酸,搅拌均匀,即得高活性苜蓿膳食纤维。f. Add citric acid and tartaric acid to the obtained high-activity alfalfa dietary fiber raw material, and stir evenly to obtain high-activity alfalfa dietary fiber.
将所得高活性苜蓿膳食纤维汇入胶囊后包装,用60Co或137Csγ进行辐照灭菌,其吸收剂量范围为0.4-1.0kGy。The obtained highly active alfalfa dietary fiber is poured into capsules and packaged, and irradiated and sterilized with 60 Co or 137 Csγ, and the absorbed dose ranges from 0.4 to 1.0 kGy.
实施例1:Example 1:
本发明的配方取苜蓿膳食纤维99%,柠檬酸0.5%,酒石酸0.5%。(方法同上)The formula of the present invention takes 99% of alfalfa dietary fiber, 0.5% of citric acid and 0.5% of tartaric acid. (method same as above)
实施例1:Example 1:
本发明的配方取苜蓿膳食纤维98.25%,柠檬酸1%,酒石酸0.25%。(方法同上)The formula of the present invention takes 98.25% of alfalfa dietary fiber, 1% of citric acid and 0.25% of tartaric acid. (method same as above)
实施例3:Example 3:
本发明的配方取苜蓿膳食纤维97.5%,柠檬酸1.5%,酒石酸1%。(方法同上)The formula of the present invention takes 97.5% of alfalfa dietary fiber, 1.5% of citric acid and 1% of tartaric acid. (method same as above)
本发明采用以下分析测定方法The present invention adopts following analysis and determination method
1、总膳食纤维的测定 AoAc001.431. Determination of total dietary fiber AoAc001.43
2、粗蛋白质的测定 GB/T5009.5-19852. Determination of crude protein GB/T5009.5-1985
3、溶涨性的测定 3. Determination of swelling property
4、持水力的测定 4. Determination of water holding capacity
得出结论:高活性苜蓿膳食纤维中主要成分为:总膳食纤维和少量蛋白质及脂肪。其中总膳食纤维含量高达75%以上。It is concluded that the main components of highly active alfalfa dietary fiber are: total dietary fiber and a small amount of protein and fat. Wherein the total dietary fiber content is as high as more than 75%.
本发明膳食纤维对人体具有以下主要保健作用:Dietary fiber of the present invention has following main health-care effects to human body:
膳食纤维对人体健康具有很多重要的生理功能,已被国内外大量的研究事实与流行病学调查结果所证实,并被现代医学和营养学家确认为是继蛋白质、脂肪、碳水化合物、维生素、矿物质和水之后的第七大营养素,并且还显示出许多特殊生理活性功能。Dietary fiber has many important physiological functions to human health, which has been confirmed by a large number of research facts and epidemiological investigation results at home and abroad, and has been confirmed by modern medicine and nutritionists as the next step in protein, fat, carbohydrates, vitamins, It is the seventh largest nutrient after minerals and water, and also shows many special physiologically active functions.
1、膨胀特性与预防肠道疾病功能1. Expanding properties and the function of preventing intestinal diseases
膳食纤维具有很强的吸水性,进入消化道后,在胃中吸水膨胀,现成高粘度的溶胶,刺激胃肠道蠕动,增加排便速度,降低肠内压,产生通便作用,可用于防止便秘、肠憩室症、横膈膜症及痔疮等疾病。Dietary fiber has strong water absorption. After entering the digestive tract, it absorbs water and swells in the stomach. It is ready-made high-viscosity sol, which stimulates gastrointestinal peristalsis, increases defecation speed, reduces intestinal pressure, and produces laxative effect. It can be used to prevent constipation. , intestinal diverticulosis, diaphragm disease and hemorrhoids and other diseases.
由于膳食纤维在胃肠中吸水膨胀,产生饱腹感,可减少进食量,能量摄入减少,同时,抑制营养物质在肠道的扩散速度,减少小肠对脂肪的吸收率,长期食用可以动用体内储备脂肪,从而达到减肥的目的。Because dietary fiber absorbs water and expands in the gastrointestinal tract, it produces a feeling of fullness, which can reduce food intake and energy intake. At the same time, it inhibits the diffusion rate of nutrients in the intestinal tract and reduces the absorption rate of fat in the small intestine. Long-term consumption can use the fat in the body. Store fat, so as to achieve the purpose of weight loss.
2、吸附有机物特性与预防心脑血管疾病功能2. The characteristics of adsorbing organic matter and the function of preventing cardiovascular and cerebrovascular diseases
膳食纤维具有吸附胆汁酸、胆固醇、变异原等有机分子的性质,进入肠道的膳食纤维能螯合肠道中的胆固醇,减少外源性胆固醇、胆汁酸、盐类的合成与吸收,同时限制胆酸的肠肝循环,阻碍内源性胆固醇、中性脂肪酸的重吸收;膳食纤维还能促进胆固醇转化成胆酸和胆盐,加速胆盐和脂类物质的排泄。所以,膳食纤维可用于预防胆石症、高脂血症、肥胖、动脉粥样硬化、冠心病等疾病的发生。Dietary fiber has the property of adsorbing organic molecules such as bile acid, cholesterol, and mutants. Dietary fiber entering the intestine can chelate cholesterol in the intestine, reduce the synthesis and absorption of exogenous cholesterol, bile acid, and salts, and limit the bile The enterohepatic circulation of acid hinders the reabsorption of endogenous cholesterol and neutral fatty acids; dietary fiber can also promote the conversion of cholesterol into bile acid and bile salt, and accelerate the excretion of bile salt and lipid substances. Therefore, dietary fiber can be used to prevent cholelithiasis, hyperlipidemia, obesity, atherosclerosis, coronary heart disease and other diseases.
3、解毒及降血压功能3. Detoxification and blood pressure lowering function
膳食纤维分子呈弱酸性,具有离子交换树脂的作用,在人体肠道内能够吸附铅、汞、镉等重金属离子,降低有毒重金属离子的吸收,加快有毒离子的排泄,起到解毒作用。膳食纤维还能与胃肠道中的钠离子进行交换,使钠离子随粪便大量排出,血液中Na+/K+比变小,从而产生降血压作用。Dietary fiber molecules are weakly acidic and have the function of ion exchange resins. They can absorb heavy metal ions such as lead, mercury, and cadmium in the human intestinal tract, reduce the absorption of toxic heavy metal ions, accelerate the excretion of toxic ions, and play a detoxification role. Dietary fiber can also exchange with sodium ions in the gastrointestinal tract, so that a large amount of sodium ions are excreted with the feces, and the ratio of Na + /K + in the blood becomes smaller, thereby producing a hypotensive effect.
4、调节糖代谢特性与降血糖功能4. Regulating the characteristics of glucose metabolism and hypoglycemic function
膳食纤维能增加肠液粘度,阻碍葡萄糖的吸收,束缚葡萄糖,降低肠道葡萄糖的有效浓度;影响α-淀粉酶对淀粉的降解作用,延长酶解时间,降低肠液中葡萄糖的释放速度;同时改善外周组织对胰岛素的感受性,降低机体对胰岛素的要求,从而降低糖尿病人的血糖水平。Dietary fiber can increase the viscosity of intestinal juice, hinder the absorption of glucose, bind glucose, and reduce the effective concentration of intestinal glucose; affect the degradation of starch by α-amylase, prolong the enzymatic hydrolysis time, and reduce the release rate of glucose in intestinal juice; Tissue sensitivity to insulin, reduce the body's demand for insulin, thereby reducing blood sugar levels in diabetics.
5、调节肠内菌群、清除自由基特性与抗癌功能5. Regulating intestinal flora, free radical scavenging properties and anti-cancer function
膳食纤维进入大肠后,能被肠道细菌选择性的分解,抑制腐生菌的生长,促进益生菌的繁殖,降低了腐生菌产生的致癌物质,促进益生菌产生丁酸,调节肠道内pH值,抑制肿瘤细胞的生长和促进该细胞的死亡,从而起到预防癌症的发生;膳食纤维在结肠内被微生物利用,促使结合在其中的阿魏酸释放,而阿魏酸具有较强的抗氧化活性和清除自由基的作用,从而预防肠道中发生肿瘤的发生。After dietary fiber enters the large intestine, it can be selectively decomposed by intestinal bacteria, inhibit the growth of saprophytic bacteria, promote the reproduction of probiotics, reduce the carcinogens produced by saprophytic bacteria, promote the production of butyric acid by probiotics, and adjust the pH value in the intestine. Inhibit the growth of tumor cells and promote the death of the cells, thereby preventing the occurrence of cancer; dietary fiber is utilized by microorganisms in the colon, which promotes the release of ferulic acid bound to it, and ferulic acid has strong antioxidant activity and scavenging free radicals, thereby preventing the occurrence of tumors in the intestinal tract.
本发明的应用效果:Application effect of the present invention:
从紫花苜蓿中浓缩提取了在该植物存在的大量活性膳食纤维,其含量高达75%以上,是一种资源丰富,并有多种生理功能的多糖类物质。它对预防某些疾病和保障人们的身体健康,起着极其重要作用,是一种比较理想的功能保健食品原料。除此之外,在焙烤食品应用也比较广泛,比如用在面包、饼干、蛋糕、桃酥等焙烤食品中其用量一般为面粉量的5%-10%,苜蓿膳食纤维可用于制作馒头、面条、方便面中,其用量一般为面粉量的5%-6%,将苜蓿膳食纤维与焦糖色素、动物油脂、山犁酸、微量元素等营养成分以及木糖醇甜味剂混合后,加热制成膳食纤维馅料,可用于牛肉馅饼、点心馅、汉堡包等面食制品中,效果很好。A large amount of active dietary fiber present in the plant is concentrated and extracted from alfalfa, and its content is as high as more than 75%. It is a polysaccharide with rich resources and multiple physiological functions. It plays an extremely important role in preventing certain diseases and protecting people's health, and is an ideal raw material for functional health food. In addition, it is also widely used in baked foods, such as bread, biscuits, cakes, peach cakes and other baked foods, and its dosage is generally 5%-10% of flour. Alfalfa dietary fiber can be used to make steamed bread, noodles , In instant noodles, the dosage is generally 5%-6% of the amount of flour. After mixing alfalfa dietary fiber with caramel pigment, animal fat, behenic acid, trace elements and other nutrients and xylitol sweetener, heating It can be used as a dietary fiber filling, which can be used in pasta products such as beef patties, snack fillings, hamburgers, etc., and the effect is very good.
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CN104247739A (en) * | 2014-09-09 | 2014-12-31 | 秋实草业有限公司 | Sugar-free clover cookie and making method thereof |
CN104799290A (en) * | 2015-05-04 | 2015-07-29 | 程晋生 | Compressed fiber particle and method for absorbing fat, expelling toxin and clearing bowels by use of compressed fiber particle |
CN109793243A (en) * | 2017-11-16 | 2019-05-24 | 镇江市丹徒区南山溪园茶叶专业合作社 | A kind of processing method that microwave assisting method extracts apple skin soluble dietary fiber |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN104247739A (en) * | 2014-09-09 | 2014-12-31 | 秋实草业有限公司 | Sugar-free clover cookie and making method thereof |
CN104799290A (en) * | 2015-05-04 | 2015-07-29 | 程晋生 | Compressed fiber particle and method for absorbing fat, expelling toxin and clearing bowels by use of compressed fiber particle |
CN109793243A (en) * | 2017-11-16 | 2019-05-24 | 镇江市丹徒区南山溪园茶叶专业合作社 | A kind of processing method that microwave assisting method extracts apple skin soluble dietary fiber |
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